• Journal of the Korean Crystal Growth and Crystal Technology
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• v.14 no.5
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• pp.187-192
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• 2004

We try to use isopropanol which has low boiling point to prepare ZnO thin films at low temperature. ZnO thin films were prepared by sol-gel spin-coating method using zinc acetate dehydrate-isopropanol-monoethanolamine (MEA) solution. The c-axis preferred orientation and optical properties of ZnO films with preheating temperature have been investigated. ZnO thin films were preheated at 200 to $300^{\circ}C$ with an interval of $25^{\circ}C$ and post-heated at $650^{\circ}C$. The ZnO film preheated at $275^{\circ}C$ and post-heated at $650^{\circ}C$ was highly oriented along c-axis (002) plane, and the surface with homogeneous and dense microstructures was formed having nano-sized grains. The optical transmittance was above 90 % in the visible range and exhibited absorption edges at 368 nm wavelength.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.23 no.6
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• pp.458-463
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• 2010

MLCC (multi-layer ceramic capacitor) is usually fabricated by lamination of predetermined number of single layers. Often, the state of MLCC before sintering is called the green state, whose strength comes from the adhesion between the dielectric material and the polymer binder. Therefore the lamination of a single layer before sintering can be easily deformed by environment due to the relatively lower strength. After the compression process, which helps single sheets cohereto with adjacent sheets, the MLCC green bar is preheated to resolve the probable internal stress. Unfortunately, unexpected deformation after preheating resulted in problems during cutting of the MLCC green bar. In this study, one of 2 primary hypotheses which were proposed to resolve the unexpected deformation after preheating was examined by quantitative experiment with GC/MS (gas chromatograpy/mass spectrometer). The proportion of deformation caused by DOP evaporation, which was primarily evaporated componet during preheating, to the total deformation of the MLCC green bar was found to be 53%.

• Korean journal of food and cookery science
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• v.6 no.2
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• pp.1-6
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• 1990

The purpose of this study was to investigate the effects of preheating and salt concentration on the fermentation rate and firmness of cucumber kimchi, and the relationship between firmness and the contents of pectin fractions, hemicellulose and cellulose during fermentation. For this purpose, pH, acidity, firmness and the contents of pectic fractions, hemicellulose and cellulose were studied. 1. The changes of pH and titratable acidity indicated that preheating and high salt concentration delayed the fermentation rate in cucumber kimchi. 2. After 9 days, preheated cucumber kimchi was firmer than nonpreheated cucumber kimchi. 3. During fermentation, the cucumber kimchi fermented at 5% NaCl was firmer than that femented at 2% NaCl. 4. After 9 days, preheated cucumber kimchi was higher in insoluble pectin (HCISP)content and lower in soluble pectin (HWSP & HXSP) content than nonpreheated cucumberkimchi and hese results in accord with those of firmness measurements. 5. During fermentation, the cucumber kimchi fermented at 5% NaCl was higher in insoluble pectin content and lower in soluble pectin content than nonpreheated cucumber kimchi, and these results were in accord with those of firmness measurement. 6. During fermentation, cellulose content decreased.

• Proceedings of the IEEK Conference
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• 2001.10a
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• pp.571-575
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• 2001

To examine the grinding effect through preheating of waste concrete as a way of retrieving coarse aggregates from waste concrete, the removal rates of cement mortar and paste of both recycled aggregates and heated and grinded ones were investigated. As the preheating temperature increased, the removal rate of cement mortar from waste concrete was raised, and this kind of removal hardly affected the abrasion rate and specific gravity of aggregates. On the other hand, when it was treated over 40$0^{\circ}C$ of preheating temperature, the absorptance was reduced to less than 2.17, and cement mortar was effectively separated from waste concrete. It could meet the Korean Standards on recycled aggregates for concrete, and it is expected to expand the scope of utilization by making it possible to retrieve the aggregates which have the properties close to natural aggregates.

• 한국지구물리탐사학회:학술대회논문집
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• 2003.11a
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• pp.695-702
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• 2003

In this study, an experimental apparatus has been designed and set-up to analyse the dissociating phenomena of hydrate in porous rock using electric heating method supplied at downhole. The electric heat injecting experiments have been performed to investigate the heat transfer within the core, the dissociating phenomena of hydrate, and the productivities of dissociated gas and water. These experiments were under constant heat injecting method as well as preheating methods. From the experimental results, it is seen that the hydrates is dissociated along the phase equilibrium curve and dissociation of hydrate is accelerated with heat. The injected heat is consumed for the dissociation and also it is lost together with outflow of the dissociated gas and water. From the investigation of gas producing behavior for various heat injecting methods, as the injected heat is greater, dissociation is accelerated faster at outlet and hence the initial gas production becomes higher. Also, it is shown that the initial gas productivity under the constant heating method is better, however, the energy efficiency is low because of smaller amount of the produced gas comparing to the amount of heat injected. In the experiments of preheating method, it was seen that gas production only initial stage is different with the preheating time, but the producing behaviors of gas production are similar.

• Journal of the Korean Society of Manufacturing Technology Engineers
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• v.21 no.6
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• pp.988-997
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• 2012

Laser surface hardening is one of core technologies to enhance various characteristics such as the strength, hardness, toughness, abrasion resistance, and fatigue resistance for the mold material. This paper focuses on testing characteristics of the laser heat treatment according to the preheating parameters in case of the SM45C medium carbon steel. In this paper, we assume that the power and travel speed of the laser are 1,800W and 0.5m/min, respectively, and the range of the preheating temperature is $50^{\circ}C{\sim}300^{\circ}C$. From the result of the test, we observed that the hardness width and depth are enhanced as the temperature is increased. Also, the best average hardness was 751.7Hv for the temperature of $100^{\circ}C$.

• Plant Journal
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• v.7 no.1
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• pp.49-55
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• 2011

This study analyzed causes and status of cracks to suggest preventives for welding cracks generated on fillet welding zone of atmosphere corrosion resisting steel box girder. Penetrant testing, a sort of non-destructive testing, was conducted for inspection of crack status on welding zone. As a result of test, welding cracks were found on the point of start, center and end to fillet welding zone of 32 mm-thickness. The result of carbon equivalent composition of materials was 0.452%. According to welding specification, to preheat prevent welding crack, preheat temperature of $100{\sim}200^{\circ}C$ should be kept before welding execution. It was failed to keep preheat temperature because it had been executed on winter season and the structure of box girder had wide heat transfer area. As a result of examination of time varying preheating temperature of 32mm-thickness material, it was understood that preheat temperature of above $230^{\circ}C$ on both 130mm-long sides of welded joint can prevent welding crack.

• Journal of Korea Foundry Society
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• v.22 no.2
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• pp.75-81
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• 2002

The main objectives were to investigate the suitability of CaO crucible for melting TiAl alloys and to develop investment mold for investment casting of TiAl alloys. TiAl alloy specimen were prepared by plasma arc furnace under argon atmosphere. After melting of TiAl alloy using CaO crucible, the results showed that there is little contamination of oxygen in the TiAl bulk. Conventional vacuum induction furnaces can be readily adaptable to produce cast parts of TiAl without high skilled techniques. The determination of optical metallography and microhardness profiles in investment cast TiAl alloy rods has allowed the gradation of the relative thermal stability of the oxides examined. The molds used for the present study were $ZrO_2$, $Al_2O_3$, CaO stabilized $ZrO_2$ and $ZrSiO_4$. Even although high temperature of mold preheating, $Al_2O_3$ mold is a promising mold material for investment casting of TiAl alloys in terms of thermal stability, cost and handling strength. It is important to take thermal stability and preheating temperature of mold into consideration for investment casting of TiAl alloys.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2004.07a
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• pp.445-448
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• 2004

Radio frequency and microwave dielectric heating are well-known electroheating methods, used in industrial applications where non electrically conducting materials are to be heated, dried or otherwise processed. The major reason for considering this technique for any process is based on its unique ability to transfer heat into the volume of an electrically non conducting material such as insulator directly, rather than, via a surface. Conventional heating must first bring heat to the product surface and there after it depends on the physical characteristics and condition of the material as to how effectively this heat is transmitted into the mass. The product would suffer surface damage before the main body is adequately processed. Dielectric heating is applied to enhance conventional heating methods and to drastically shorten the required processing duration. Although the use of dielectric heating has been a well proven technique for several years in some industries, its application in the preheating of FRP has been limited by the insufficient experience. In this paper a method is described for uniform radio frequency heating of preheating of FRP.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.21 no.8
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• pp.99-109
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• 2022

In this study, an electric resistance-heated surface friction spot-welding process was proposed and tested for the spot-welding ability of copper and aluminum dissimilar metal sheets using electric resistance heating and surface friction heating. This process has welding variables, such as the current value, energizing cycles, rotational speed, and friction time. The current value and energizing cycle can affect the resistance heat, and the rotational speed of the rotating pin and friction time influence frictional heat generation. Resistance heating before friction heating has a preheating effect on the Cu-Al contact interface and a positive effect on preventing friction heat loss during the friction stage. However, because resistance preheating can soften the copper sheet and affect the contact stress and friction coefficient, it has difficulties that may adversely affect frictional heat generation. Therefore, the optimal combination of welding variables should be determined through simulations and experiments of the spot-welding process to determine the effects of electric resistance preheating on the suggested process. Through this procedure, it is known that the proposed spot-welding process can improve the welding quality during the spot welding of Cu-Al sheets.