• Korean Chemical Engineering Research
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• v.49 no.5
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• pp.577-581
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• 2011

Silicon nanoparticles have attracted a great deal of scientific interests due to its intense photoluminescence in the visible spectral region and its potential applications in biological fluorescence maker, RGB (red, green, blue) display, photonics and photovoltaics etc. Practical applications making use of optical and physicochemical properties of Si nanoparticles requires an efficient synthetic method which allows easy modulation of their size, size distribution as well as surface functionalities etc. In this study, a one-pot solution reduction scheme is attempted to prepare alkyl-terminated Si nanoparticles (<10 nm) with Si precursors, (Octyl)$SiCl_3$ or mixture of (Octyl)$SiCl_3$ and $SiCl_4$, containing alkyl-groups using Na(naphthalide) as reducing agent. The surface capping of Si nanoparticles with octyl-groups as well as Si nanoparticle formation was achieved in one-pot reaction. The hexane soluble Si nanoparticles with octyl-termination were in the range of 2-10 nm by TEM and some oxide groups (Si-O-Si) was present on the surface by EDS/FTIR analyses. The optical properties of Si nanoparticles measured by UV-vis and PL evidenced that photoluminescent Si nanoparticles with alkyl-termination was successfully synthesized by solution reduction of alkyl-containing Si precursors in one-pot reaction.

• Journal of Korean Society of Coastal and Ocean Engineers
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• v.28 no.2
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• pp.92-100
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• 2016

Reliability analysis of tripod support structure for offshore wind turbine was performed. Extreme distribution function of peak response due to wind and wave loads was estimated by applying peak over threshold(POT) method. Then, stress based limit state function was defined by using maximum stress of support structure which was obtained by multiplying beam stress and concentration factor. The reliability analysis result was compared when maximum stress was calculated from shell element. Reliability index was evaluated using first order reliability method(FORM).

• Journal of the Earthquake Engineering Society of Korea
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• v.9 no.1 s.41
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• pp.43-50
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• 2005

Many highway bridges in Korea need seismic retrofit because only one decade has passed since the seismic design criteria was introduced. For the highway bridges of which bearings are worn and dysfunctional, the validity of seismic retrofit method using laminated rubber bearings was discussed in this study. Real scale RC pier specimens without seismic details were constructed. And then, Pot bearing, Rubber bearing (RB), Lead-rubber bearing (LRB) were applied to these specimens. Through pseudo dynamic test method, dynamic behavior of these RC piers under earthquake was simulated and compared. From the test results, proposed seismic retrofit method was found to be valid.

• Korean Journal of Community Nutrition
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• v.14 no.5
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• pp.531-544
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• 2009

This study was conducted to survey multiple factors of aversion to vegetables and preferences for vegetable-related recipes in school meal services among elementary school children in order to help develop various menus and recipes for school meal services. Questionnaire survey was carried out with the study subjects, who were 401 children in 6th grade attending elementary schools in Chonnam and Kwangju metropolitan regions. Results from the survey can be summarized as follows: 65.1% of respondents answered they try to eat vegetables and other namul side dishes served in school meal service for health. As for the frequency of taking vegetables and namul side dishes out of daily meals, 47.4% of respondents chose 'once or twice'. The reasons for aversion to vegetables in boys were taste and cooking method, while girls were taste and feeling between teeth. In boys there were no differences between regions of Kwangju and Chonnam but the tendency of aversion to vegetables was significantly high in girls. As for the aspects of vegetable aversion of subjects, 46.9% of respondents took up 'black & purple' in the unfavorable color of vegetables. 49.1% in 'bitterness' and 39.2% in 'greasiness' were in terms of the aversive taste of vegetables. The aversive vegetable recipes were 58.6% in 'raw & seasoned' and the unfavorable feeling of vegetables were 53.1% in 'squashiness'. There were differences between regions of Kwangju and Chonnam with boys in color and cooking method in girls. Results from the survey on their preferences for vegetable recipes showed that leafy vegetables like crown daisy (raw/slightly seasoned) and pak choi (broth/pot stew) fell to the most aversive category, while bean sprouts (broth/pot stew) were chosen as the most favorable one. Among root vegetables bell-flowers were found to belong to the least preferred recipe, while potatoes were proven to be most preferable in terms of recipes. As for fruit vegetables and other vegetables, all respondents didn't like 'fatsia shoots' vegetable and it's cooking method and they preferred 'green pumpkins (broth/pot stew)'. In respect of mushrooms, enoki mushroom (broth/pot stew) was found most preferred and had high tendency of preferences in boys and girls in Kwangju compared with Chonnam region. The study results indicated that respondents did not show big differences in factors influencing them to be averse to vegetables and their preferences for vegetable recipes depending on regions. In order to have high preference and intake in children's diets, it needs to study in reform of menu about using namul or vegetables mixed with meats and fruits that children preferred or applying roasted and fried other less than namul.

• Current Research on Agriculture and Life Sciences
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• v.5
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• pp.59-67
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• 1987

The pot experiment was conducted using soils with varying contents of available phosphorus to select the reasonable method for determination of the available phosphorus content in soils for Nak-Dong rice cultivation. On a basis of the responses to the phosphorus tertilizer applied, the linear correlation coefficients by Bray No.1, Bray No.2, Lancaster, North Carolina and Olsen methods were 0.887, 0.868, 0.879, 0.952 and 0.911 for Nak-Dong rice yield, respectively. Of the methods tested, North Carolina method was the most suitable for determining, the phosphorus content in soils for Nak-Dong rice. The phosphorus application promoted the growth of Nak-Dong rice in pots for culm, tiller number, available stem and grain number per ear. Based on this experiment it could be presumed that the recommanded quantity of phosphorus fertilizer should attain to 5kg per 10a to promote the growth of Nak-Dong rice in A-soil and 10kg per 10a in B -, C - and D-soil. The results from the pot experiment will be somewhat different from those from the field experiment. Therefore, field experiment should be carried out for further information.

• Journal of Biosystems Engineering
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• v.42 no.1
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• pp.56-61
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• 2017

Purpose: High energy requirement and long cooking time are limiting consumption of pigeon pea (Cajanus cajan), a nutritious food. This study was performed to estimate energy and time demand by different methods of cooking pigeon pea. Methods: Pigeon pea (150 g) was soaked in 2.0 L of water at ambient temperature ($29{\pm} 2^{\circ}C$) to determine hydration behavior. Cooking experiments were conducted using aluminum and pressure-cooking pots. Efficiency of cooking was evaluated using four types of cooking appliances (kerosene, liquefied petroleum gas (LPG), electric, and charcoal stoves). Normal (continuous heating until the food was satisfactorily cooked) and control (controlling the energy input to closely match the actual energy required) cooking were conducted. Energy requirement and duration of cooking were determined using standard procedures. Results: Soaking increased moisture content from 11.99 to 30.01% in 90 min, while water absorption rate decreased with soaking duration. In cooking 150 g of pigeon pea using kerosene stove, presoaked normal pressure-pot cooking method consumed the least energy (10 800 kJ) and time (205 min), while unsoaked normal cooking consumed the highest energy (18 450 kJ) and time (336 min). Using LPG stove, unsoaked normal cooking method required the highest energy (52 470 kJ), while presoaked control pressure-pot required the least energy (14 405 kJ). For electric stove, the lowest energy (15 560 kJ) and shortest duration (105 min) were recorded during control cooking of presoaked sample in the pressure-pot. Conclusions: Control cooking was not practicable using charcoal stove. Generally, kerosene stove consumed the least energy, while electric stove was found to have the shortest duration of cooking.

• Journal of the Korean Institute of Intelligent Systems
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• v.20 no.6
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• pp.748-754
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• 2010

To reduce the computational cost required for assembling vessel fragments using surface geometry, this paper proposes a fast axis estimation method. Using circular constraint of pottery and local planar patch assumption, it finds the axis of the symmetry. First, the circular constraint on each cylinder is used. A circular symmetric pot can be thought of unions of many cylinders with different radii. It selects one arbitrary point on the pot fragment surface and searches a path where a circumference exists on that point. The variance of curvature will be calculated along the path and the path with the minimum variance will be selected. The symmetric axis will pass through the center of that circle. Second, the planar patch assumption and profile curve is used. The surface of fragment is divided into small patches and each patch is assumed as plane. The surface normal of each patch will intersects the axis in 3D space since each planar patch faces the center of the pot. A histogram method and minimization of the profile curve error are utilized to find the probability distribution of the axis location. Experimental results demonstrate the improvement in speed and robustness of the algorithms.

• Journal of Soil and Groundwater Environment
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• v.26 no.1
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• pp.8-16
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• 2021

This study has evaluated the stabilization of As contaminated paddy and cultivated soils by pot experiments for rice and lettuce. Various ratios of limestone (L) and steel slag (S) were mixed with the soils in each pot. The soils were taken from before and after pot experiments, and analyzed for As extracted by sequentially (Wenzel method) and totally (aqua regia method).. Paddy soils amended with L (0.5%) and L (1.0%) + S (1.0%) showed increasing fraction 2 (specifically bound As) compared with control soil. Arsenic concentrations in rice grain grown on the amended soils decreased 14% and 12% compared with those on the control soil, respectively. According to sequential extraction of As in cultivated soils, the fractions 1~3 were decreased due to stabilization of As by the soil amendment, especially for S (1.0%), S (3.0%) and L (1.0%) + S (1.0%). In addition, relatively low As concentrations were found in lettuce grown on amended soils with L (0.5%) and L (1.0%) + S (1.0%). Therefore, it can be suggested that soil amendments with L (0.5%) or L (1.0%) + S (1.0%) were suitable for enhancing stabilization of As in the study area.

• Bulletin of the Korean Chemical Society
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• v.33 no.8
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• pp.2679-2682
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• 2012

A simple one-pot synthesis of two derivatives of 1,4-dihydropyridines has been described under reflux conditions using copper iodide nanoparticles (CuI NPs) as a catalyst in high yields. This method demonstrated four-component coupling reactions of aldehydes and ammonium acetate via two pathways. In one route, the reaction was performed using 2 eq ethyl acetoacetate while in the other one 1 eq ethyl acetoacetate and 1 eq malononitrile were used. The CuI NPs was reused and recycled without any loss of activity and product yield. It is noteworthy to state that wide range of the 1,4-dihydropyridines have attracted large interest due to pharmacological and biological activities.

• Journal of the Korean Chemical Society
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• v.58 no.5
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• pp.445-449
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• 2014

A convenient and efficient method has been developed for the one-pot synthesis of dihydropyrimidinones (DHPMs) compounds. Dihydropyrimidinone derivatives were synthesized in good yields using ethyl acetoacetate, aldehyde (aromatic and aliphatic) and urea or thiourea in the presence of ZnO nanoparticles as a catalyst in $H_2O$ as solvent at $80^{\circ}C$. This green chemistry procedure applied to the Biginelli reaction using ZnO nanoparticles as catalyst and illustrated as a rapid preparation of DHPMs in water as solvent. The products were identified by physical data (mp) by comparison with those reported in the literatures.