• 대한조선학회논문집
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• 제44권4호
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• pp.417-424
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• 2007

With regard to corrosion fatigue crack initiation life (Nc), it has been treated ambiguously for the member which doesn't have stress concentration area. In this research, in order to clarify the corrosion fatigue crack initiation life (Nc), corrosion fatigue tests were carried out. Reasonable and universal corrosion fatigue crack initiation life (Nc) was defined and corrosion fatigue crack initiation/propagation model was suggested also. As the fatigue crack which emanates from the pit is usually small, accordingly it is treated as a small crack. In addition, the observation of the corrosion fatigue fracture surfaces using SEM was conducted. And the fracture mechanics analysis using an intrinsic crack model was conducted for the treatment of the small crack. Finally, the followings were obtained. When there is no clear stress concentration point which seems to fall into a corrosion fatigue crack initiation life, the significance of the definition and suggestion of the moment of the reasonable and universal corrosion fatigue crack initiation life (Nc), at which the fatigue crack propagation rate becomes faster than the corrosion pit growth rate so that the fatigue crack initiates from the pit and propagates in earnest, has been clarified.

• 한국음향학회지
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• 제43권4호
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• pp.466-475
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• 2024

수중 음원 위치를 추정하기 위한 음향 모델 기반의 정합장 처리 방법은 해양 환경과 수신 배열 기울기에 대한 정확한 정보를 필요로 하므로, 음향 모델 불일치에 매우 민감하다. 반면, 도파관 불변성(배열 불변성) 기반의 음원 거리 추정 방법은 빔-시간 영역에서 분리된 다중경로 신호의 빔각도와 상대적 도달 시간 정보만을 활용하므로 음향 모델이 필요 없는 강인한 거리 추정 방법을 제공한다. 본 논문에서는 도파관 불변성 기반 음원 거리 추정 방법을 얕은 웅덩이가 있는 천해 환경으로 확장하였다. 실제 해상실험 데이터와 수치 시뮬레이션 결과를 통해 해당 환경에서의 수중 음원 거리 추정 성능을 분석하였다.

• Corrosion Science and Technology
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• 제23권4호
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• pp.315-323
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• 2024

This work examined pitting corrosion failure of a copper heat-return pipe used in a district heating system. The copper pipe was corroded with a 48% reduction in thickness due to localized corrosion on the inner surface exposed to heating water of 20 ~ 40 ℃. Fe and Si elements as corrosion products were found around pits. Cl element was also observed, which accelerated oxidation of copper inside pits. Cu₂O deposits on the pit's bottom surface decreased the pH inside the pit. X-ray diffraction analysis revealed hematite, cuprite, malachite and brochantite as corrosion products. Chemical analysis demonstrated that Fe and Si elements did not exist in the copper, supply water, or heating water, indicating that Fe and Si species might have entered into the pipe from the exterior. These results indicated that pits were initiated due to ion concentration gradient near Fe and Si species. Moreover, the interior of pits had lower pH due to Cl^- concentration and Cu₂O reactions, which accelerated the pit's growth and led to formation of pinholes. Additionally, we confirmed that the type of pitting corrosion was a complex combination of types I and II based on the HCO₃^-/SO₄^2- ratio, pH, temperature, and corrosion products.

• 한국전기전자재료학회논문지
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• 제35권5호
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• pp.504-508
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• 2022

Single crystal gallium oxide (Ga₂O₃) has been an emerging material for power semiconductor applications. However, the defect distribution of Ga₂O₃ substrates needs to be carefully characterized to improve crystal quality during crystal growth. We analyzed the type and the distribution of defects on commercial (-201) Ga₂O₃ substrates to get a basic standard prior to growing Ga₂O₃ crystals. Etch pit technique was employed to expose the type of defects on the Ga₂O₃ substrates. Synchrotron white beam X-ray topography was also utilized to observe the defect distribution by a nondestructive manner. We expect that the observation of defect distribution with three-dimensional geometry will also be useful for other crystal planes of Ga₂O₃ single crystals.

• 치위생과학회지
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• 제18권6호
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• pp.367-373
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• 2018

시판 중인 어린이 음료가 레진계 치면열구전색제에 미치는 물리 화학적 영향을 알아보기 위해 판매량이 높은 3종의 어린이 음료와 대조군으로 생수를 선정하였다. 제조사의 지시에 따라 레진 시편을 제작하여 시편의 초기 거칠기 값(Ra)를 측정하였고, 각 음료의 pH를 측정한 후, 레진 시편을 각각의 음료에 침지시켜 $37^{\circ}C$ 배양기에서 72시간 보관하였다. 72시간 후 레진 시편의 표면 거칠기를 측정하였고 시편 표면의 형태변화 관찰을 위해 주사전자현미경으로 관찰하였다. 레진 시편에서 용출된 단량체의 종류 및 용출량은 HPLC를 이용하여 비교 분석하였다. 생수를 제외한 모든 실험음료에 구연산이 첨가되어 있었고 어린이 음료의 평균 pH는 $3.25{\pm}0.17$로 '아이키커'에서 $3.03{\pm}0.01$로 가장 낮았고 '뽀로로'에서 $3.47{\pm}0.02$로 가장 높았다. 어린이 음료에 침지 후 시간 경과에 따른 표면 거칠기가 증가하였고 레진 시편의 표면에 기질의 탈락을 관찰하였다. 모든 실험음료에서 bis-GMA는 유출되지 않았으나 생수를 제외한 어린이 음료에서는 TEGDMA가 유출되었다. 이상의 결과 어린이 음료는 치면열구전색제의 열화와 단량체의 유리를 촉진할 수 있으며 유리된 단량체는 성장 중인 어린이에게 더 큰 영향을 미칠 수 있으므로 어린이 음료를 빈번히 음용하는 것은 주의가 필요하다.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2002년도 하계학술대회 논문집
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• pp.67-73
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• 2002

The development of high performance HTS wire is a key factor for various electrical applications of coils and cables. The purpose of this paper is to review and consider the main manufacturing technologies of HTS wire and its current status. A lot of efforts have been focused on the optimization of PIT parameters for Bi-2223/Ag wire. According to this, long Bi-2223 wires having Ic of 130 A were recently produced and their mass production has been underway in US. The current status performance of Bi-2223 wire is supposed to be used in power transmission cable because of its lower self-field property. Y-123 second generation conductor is extensively being developed throughout the world and many fabrication processes are competed with each other. 30 m-long Y-123 wire with Ic of 0.8 MA/$\textrm{cm}^2$ was recently fabricated using IBAD and PLD techniques in Japan. This result offers promise of scalable processing of practical multi-layer coated conductor.

• 한국결정성장학회지
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• 제5권2호
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• pp.87-93
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• 1995

Floating zone법으로 strontium titanate 단결정을 육성하였다. 성장조건은 공기 분위기하에서 성장속도 3mm/hr, 상부축 회전속도 20~25rpm, 하부축 회전속도 15~20rpm이었으며 육성한 단결정은 옅은 갈색을 띄고 있었으며 투명하였고 annealing 후 색깔이 옅어짐을 확인할 수 있었다. 성장방위는 [112] 방향이었으며 XRD, EDS로 화학양론적인 조성은 $SrTiO_3$단일 결정상임을 알 수 있었다. $350^{\circ}C$, KOH용액에서 5분동안 chemical etching하여 etch pit pattern을 조사하였으며 상온하에서$350^{\circ}C$의 온도 범위에서 유전상수 값을 조사하였다.

• 한국분말재료학회지
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• 제14권4호
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• pp.238-244
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• 2007

The electrophoretic deposition process of Ni nano-particles in organic suspension was employed for self-repairing of heat exchanger tubes. For this purpose, Ni nano-particles prepared by levitational gas condensation method were dispersed into the solution of ethanol with the addition of dispersant Hypermer KD2. For electrophoretic deposition of Ni nano-particles on the Ni alloy specimen, constant electric fields of 20 and 100 V $cm^{-1}$ were applied to the specimen in Ni-dispersed solution. It was found that as electrophoretic deposition proceeds, the size of the pit or crack remarkably decreased due to the agglomeration of Ni nano-particles at the pit or crack. This strongly suggests that the electrophoretic mobility of the charged particles is larger for the damaged part with a higher current value rather than outer surfaces with a lower current value.

• 한국치위생학회지
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• 제22권5호
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• pp.347-354
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• 2022

Objectives: This study aimed to evaluate the relationship between pit and fissure sealants of the molars, and caries prevalence and experience to assess the effect of sealants on caries prevention. Methods: Data from 16,119 people were extracted from the seventh Korean national health and nutrition examination survey, which was conducted from 2016 to 2018. Demographic, socioeconomic, oral health-related behavioral, and oral examination survey data were collected as independent variables. SAS statistics for complex samples and multiple logistic regression analysis (Windows ver. 9.4) was used for the statistical analyses. Results: Caries prevalence and experience were significantly associated with age, sex, daily toothbrushing frequency, interdental cleaning, and having molar sealant. Multiple logistic regression analysis revealed a significant association between having molar sealants and the caries prevalence and experience among participants under 30 years of age after adjusting socio-economic variables and toothbrushing-related factors. Conclusions: This study confirmed the effect of molar sealants on caries prevention in Korea. Our results support that the application of molar sealants in children, adolescents, and young individuals is effective in preventing caries.

• Corrosion Science and Technology
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• 제22권3호
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• pp.137-152
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• 2023

Polarization behavior and corrosion inhibition of copper in acidic chloride solutions containing benzotriazole were studied. Pourbaix diagrams constructed for copper in NaCl solutions with different BTAH concentrations were used to understand the polarization behavior. Open circuit potential (OCP) depended not only on chloride concentration, but also on whether a CuBTA layer was formed on the copper surface. Only when the (pH, OCP) was located well in the CuBTA region of the Pourbaix diagram, a stable corrosion inhibiting CuBTA layer was formed, which was confirmed by X-ray Photoelectron Spectroscopy (XPS) and a long-term corrosion test. The OCP for the CuBTA layer decreased logarithmically with increasing [Cl^-] activity in the solution. A minimum BTAH concentration required to form a CuBTA layer for a given NaCl concentration and pH were determined from the Pourbaix diagram. It was found that 320 ppm BTAH solution could be used to form a corrosion-inhibiting CuBTA layer inside the corrosion pit in the sprinkler copper tube, successfully reducing water leakage rate of copper tubes. These experimental results could be used to estimate water chemistry inside a corrosion pit.