• 대한치과보철학회지
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• 제29권2호
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• pp.177-194
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• 1991

The purpose of this study was to analyze the magnitude and distribution of stress using a photoelastic model from a distal extension removable partial dentures with three kinds of mandibular major connectors, that is, lingual bar, linguoplate, and swing-lock attachment. A photoelastic model was made of the epoxy resin(PC-1) and hardener(PCH-1) and coated with plastic cement-1 (PC-1) at the lingual surface of the epoxy model and set with three kinds of chrome-cobalt removable partial dentures. A bilateral vertical load of 15kg to the middle portion of the metal bar crossing both the first molars of the right and the left, and a unilateral vertical load of 12.5kg to the right first molar were applied with the use of specially designed loading device and the reflective circular polariscope was used to analyze the photoelastic model under each condition. The following results were obtained : 1. When the bilateral vertical load was applied, the magnitude and distribution of the stress concentration of the edentulous area and the terminal abutment or adjacent teeth was in the order of lingual bar, linguoplate, swing-lock attachment. 2. When the unilateral vertical load was applied, the magnitude and distribution of the stress concentration of the edentulous area and the terminal abutment or adjacent teeth was in the order of lingual bar, linguoplate, swing-lock attachment. 3. When the unilateral vertical load was applied, the magnitude and distribution of the stress concentration of the termial abutment or adjacent teeth on the non-loaded side showed the least stress distribution in case of swing-lock attachment. 4. When the bilateral vertical load and the unilateral vertical load were applied the swing-lock attachment showed the mildest uniform stress distribution on the edentulous area and the alveolar bone around the abutment teeth.

• Design & Manufacturing
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• 제13권4호
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• pp.57-62
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• 2019

In this study, we investigated the halo surface defection of various phenomenon occurred during the injection molding process which is caused by the thinning of the product thickness and the importance of the appearance. Surface analysis was performed to observe the difference between the surface where defects appeared and the surface which did not appear. Based on these results, we analyzed the phenomenon of halo surface defects was caused by unstable flow of resin generated in injection molding and velocity change of flow front. Furthermore, we will conduct a clear analysis of halo surface defects through observations through optical microscopy and subsequent observations with atomic force microscope. It has been analyzed that halo in PP is due to the rheological difference between the crystalline and amorphous regions while that in PC/ABS is due to shear separation of PC and ABS.

• 한국식품과학회지
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• 제31권1호
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• pp.30-35
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• 1999

기존의 PC나 TLC에 의한 타르색소의 정성은 많은 시간이 소요되고 회수율이 낮아 혼합색소의 경우 주 색소만이 검출되는 단점이 있고, 많은 표준용액이 동시에 전개되어질 수 없다는 단점이 있어 분 실험에서는 Polyamide와 Photodiode array 검출기가 장착된 HPLC를 이용하여 타르색소의 추출, 정제 및 정량을 여러 각도로 검토하여 정량분석의 최적 조건을 확립하였다. 검출 파장은 각 타르색소마다 고유의 최대흡수부가 있으나 동시분석을 위해서는 254 nm의 파장에서 가장 광범위한 타르색소의 검출이 가능하였으며 적색 계통은 $520{\sim}540\;nm$, 청색이나 녹색계통은 620 nm에서 최소검출한계가 낮음을 알 수 있었다. 따라서 타르색소의 분석에는 photodiode array detector가 장착된 HPLC를 이용함으로써 220 nm에서 800 nm까지의 넓은 영역의 파장에 걸쳐 일시에 분석하므로서 시간 절약과 함께 타르색소 피크마다 3차원 스펙트럼을 제공함으로서 실험의 정확도를 높일 수 있었다. 한편 Polyamide column을 사용하였을 때의 회수율을 측정한 결과 청색 1호가 가장 낮은 94.4%를 보였으며, 전체적으로 100% 부근의 아주 높은 만족할만한 회수율을 얻었다. 타르색소를 사용한 국내산 빙과류, 캔디류, 청량음료류를 시료로 하여 타르색소의 정량을 시도한 결과 허용의 타르색소는 검출되지 않았으며, 주로 적색 계통의 적색 2호와 40호가, 황색계통의 황색 4호, 5호가 많이 사용되고 있음을 알 수 있었고 타르색소의 사용량도 200 ppm을 초과하는 것은 발견되지 않았다. 한편 녹색은 황색 4호에 청색 1호를, 보라색은 적색과 청색을 혼합한 혼합색소를 사용되어지고 있는 것을 알 수 있었다.

• 접착 및 계면
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• 제23권2호
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• pp.44-52
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• 2022

에폭시 수지는 높은 유리전이 온도 (T_g; glass transition temperature)와 우수한 물성에도 불구하고 높은 가교밀도로 인해 순간적인 충격에 쉽게 파괴되는 단점을 가지고 있다. 이를 보완하기 위해 본 연구에서는 폴리프로필렌 글리콜 (PPG; poly(propylene glycol)) 구조 기반의 diamine 물질인 Jeffamine D 2000과 프로필렌 카보네이트 (PC; propylene carbonate)의 개환중합으로 폴리올을 합성하고 이를 이용하여 우레탄 변성 에폭시를 합성하였다. 합성한 우레탄 변성 에폭시의 특성은 FT-IR, ¹H-NMR로 확인하였고 접착제로서 내충격성 향상 정도를 확인하기 위해 시중에서 사용되고 있는 비스페놀계 에폭시인 DGEBA (diglycidyl ether bisphenol A)와 경화제, 경화촉진제와 배합하여 우레탄 변성 에폭시 접착제를 만들고 전단강도, 인장강도, 충격강도 실험을 통해 우레탄 변성 에폭시의 특성을 분석하였다. 그 결과 DGEBA와 우레탄 변성 에폭시의 비율이 8:2 일 때, 접착제 내 수소결합에 의한 최적의 시너지 효과로 향상된 기계적 물성을 달성할 수 있었다.

• 폴리머
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• 제38권2호
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• pp.193-198
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• 2014

렌즈 그리고 DVD 등과 같은 성형품들은 우수한 광학적 특성을 필요로 한다. 일반사출성형 공정은 캐비티 내에 압력이 높고 큰 온도변화를 포함하게 되어 성형품에 큰 잔류응력이 남아 광학적 품질이 저하된다. 따라서 이와 같은 제품들은 성형 시 잔류응력을 최소화하기 위해 캐비티 내의 압력을 낮게 그리고 균일하게 조절할 수 있는 사출압축성형 공정을 사용하는 경우가 많다. 본 연구에서는 실험을 통하여 사출압축 성형품에 영향을 주는 성형인자를 분석하였다. 다수 캐비티 금형을 이용하여 캐비티 간 품질편차도 고찰하였다. 실험에 사용한 재료는 투명수지인 PC와 PS이었다. 사출압축성형의 실험에서 공정변수로는 압축거리, 압축속도, 압축력 그리고 압축지연시간을 이용하였다. 실험결과, 사출압축성형 공정 변수 중 압축력과 압축지연시간 그리고 압축거리가 광학적 특성에 크게 영향을 미쳤으며 그 정도는 수지에 따라 다르게 나타났다. 이러한 현상은 사출압축성형 시 수지마다 유동성에 따라 최적의 성형조건이 있음을 의미하는 것이다.

• The Journal of Advanced Prosthodontics
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• 제16권2호
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• pp.126-138
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• 2024

PURPOSE. The aim of this study was to evaluate the influence of different 3D dental resins, using a manufacturer recommended printer and a third-party printer, on cellular responses of human gingival cells. MATERIALS AND METHODS. Three NextDent resins (Denture 3D+, C&B MFH and Crowntec) were used to produce specimens on printers NextDent 5100 (groups ND, NC and NT, respectively) and Phrozen Sonic Mini 4K (groups PD, PC and PT, respectively). Human gingival fibroblasts were cultured and biocompatibility was evaluated on days 1, 3 and 7. IL-6 and IL-8 concentrations were evaluated at 3 days using ELISA. Surface roughness was evaluated by a contact profilometer. SEM and fluorescence micrographs were analyzed at days 1 and 7. Statistical analyses were performed using SPSS and mean differences were tested using ANOVA and post-hoc Tukey tests (P < .05). RESULTS. There was an increase in cellular viability after 7 days in groups PC and PT, when compared to group PD. ND group resulted in higher concentration of IL-6 when compared to PT group. SEM and fluorescence micrographs showed less adhesion and thinner morphology of fibroblasts from group PD. No significant differences were found regarding surface roughness. CONCLUSION. The use of different printers or resins did not seem to influence surface roughness. NextDent 5100 and Phrozen Sonic Mini 4K produced resins with similar cellular responses in human gingival fibroblasts. However, Denture 3D+ resin resulted in significantly lower biocompatibility, when compared to C&B MFH and Crowntec resins. Further testing is required to support its long-term use, required for complete dentures.

• 대한치과기공학회지
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• 제41권4호
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• pp.255-262
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• 2019

Purpose: Recently, the production technology of dental prosthesis using 3D Printer workpeices has been developed. However, the lack of information on the work processes and casting techniques of materials for 3D printing casting is expected to require research. Therefore, in this study, we intend to cast a Dental DLP 3D Printer workpiece, which is being commercialized, to identify its appearance and internal clearance, and to observe its castability. Methods: Castability of the 3D Printer workpiece was evaluated. The specimen is prepared in a cylindrical shape and in a 1 mm thick coping shape. The control specimen is made of wax and the experimental specimen is made of resin using two types of 3D printers. After casting, the appearance of the casting body was observed and the internal clearance of the coping was measured. Results: RP1 and RP2, cylindrical specimens, were partially cast or fin. When coping-type specimens were measured before casting, the internal clearance of PE2 was more accurate than that of PC and PE1. When coping-type specimens were measured after casting, CE1 was the most accurate in occlusal clearance and CE2n was the most accurate in axial clearance. Conclusion: 1. Exterior observations of the casting body indicated casting defects and fins. 2. Internal clearance observations show that the occlusal clearance of the castings is larger after casting, and the axial clearance of the castings is smaller after casting. 3. It is judged that the RP2 specimen is more likely to be applied for casting than the RP1 specimen.

• 대한치과보철학회지
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• 제28권2호
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• pp.183-197
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• 1990

The purpose of this study was to analyse the magnitude and distribution of stresses using a Photoelastic model from and distal - extension removable partial dentures With four designed indirect retainers. The designs of the indirect retainers were as follows : Design No. 1 : Aker's clasp on 1st bicuspid with no indirect retainer. Design No. 2 : Aker's clasp on 1st bicuspid with indirect retainer on canine. Design No. 3 : Extension of the reciprocal arm of Aker's clasp toward incisal rest on canine. Design No. 4 : Connection with the indirect retainer as in No. 2 and extension of reciprocal arm of Aker' s clasp. A photoelastic model was made of the epoxy resin(PL - 1) and hardner(PLH - 1) and coated with plastic cement -1(PC -1) at the lingual surface of the epoxy model and set with chrome - cobalt partial dentures. A unilateral vertical load of 10kg to the right 1st molar and a vertical load of 10kg to the middle portion of the metal bar crossing both the 1st molars of the right and left, were applied. With the use of specially designed jig, fixture; loading device and the reflective circular polariscope, we obtained the following results : 1. When the unilateral vertical load and the vertical load of the middle portion of the metal bar were applied, design No. 2, 3 and 4 exhibited the higher stress concentration at the root apices and their surrounding tissues of the primary and secondary abutment teeth. 2. When the unilateral vertical load applied to design No. 2,3 and 4 the root apices of the primary and secondary abutment teeth and their surrounding tissues and the nonloaded side of edentulous area exhibited and even stress distribution. 3. When the vertical load was applied, the stress concentration fringe in the primary and secondary abutment teeth was in the order of No. 1,4,2 and 3. 4. No.1 and 4 exhibited the higher distrorted stress concentration at the primary teeth and the edentulous area in the nonloaded side. 5. No.2 design reduced the stresses at the apices of the alveoli of the primary abutment teeth bilaterally as well as on the crest of the residual ridge on the nonloaded side. 6. No. 2 design exhibited the most favorable stress distribution.

• 대한치과기공학회지
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• 제22권1호
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• pp.89-112
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• 2000

Although dental laboratory technicians are prone to be exposed to various work-related health hazardous materials such as dusts, chemicals, etc., the prevalence and nature of work-related health problems of them have not been a matter of great concern in the field of occupational health service in Korea. The purpose of the present investigation was to describe a collected profile of subjective health symptoms and their attributable factors in Korean dental laboratory technicians. A questionnaire listing five groups of health symptoms and five health symptom-related factors was mailed to randomly selected 1,900 dental laboratory technicians. Among them, 1,344 dental laboratory technicians filled out the questionnaires and returnde them. Five groups of health symptoms included musculoskeletal symptom, dermal symptoms, respiratory symptoms, eys symptoms, and ear symptoms. Five health symptom-related factors were occupational environment-related health risk factors, work history, health related habits and status, use of personal protective equipment and general characteristics. Detailed parameters of health risk factors were work posture, vibration, and chemical or physical hazards such as dust, fume, vapor, solvent, light, and noise for occupational environment-related factors; work place, area, number of employees, work hours, career, work part, and work load for work history; Broca's index, hours of sleep, eating, smoking, alcohol, exercise, health examination, and self assessed health status for health habits and status; face masks, goggles, and so on for use of personal protective equipment, and; age, sex, marital status, and education for general characteristics. Before the start of main survey, a pilot survey was carried out for validity and reliability tests of the questionnaire. All the data obtained were coded and analyzed with PC/SAS 6.12 program. The prevalence of health symptoms was the highest in musculoskelton (87.3%), and followde by eyes (78.9%), respiratory organs (64.3%), ears (57.8%), and skin (52.2%) in descending order. Statistically significant risk factors by multiple logistic regression analyses were sex, health examination, self assessed health status, and hand/finger posture in musculoskeletal symptoms; sex, self assessed health status, career, acid gas, and hand contact with resin mixture in deraml symptoms; Broka's smoking, exercise, self assessed health status, and face mask in respiratory symptoms; sex, hours of sleep, self assessed health status, work hours, work load, plaster dust, inadequate lighting, and goggle in eys symptoms, and eating, smoking, self assessed health status, and work load in ear symptoms. With the above considerations in mind, prevalence of subjective symptoms among Korean dental laboratory technicians was relatively high, and they were attributable to most of the occupational environment-related factors, work history, use of personal protective equipment, health habits and status, and general characteristics. Particularly, it is suggested that health promotion programs for promoting self- assessed health status and smoking cessation, preventive measures for protection of the female technicians’health, and reducing work load be necessary, since those factors were associated with more than one subjective symptom.

• 한국약용작물학회지
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• 제11권2호
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• pp.115-121
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• 2003

전통적인 향기치료제로 쓰여 온 회향, 유향 그리고 노간주를 사용하여 최근 신기술로 평가되고 있는 초임계 유체추출법을 통해 생체 조절기능을 지닌 기능성 정유 성분을 추출하였다. 기존의 SDE 추출법과 비교하여 추출수율 측면에서 비교적 높은 결과를 얻어내어 정유 추출시 장차 SDE 추출법을 대체할 신기술로 평가되었다. 추출용매를 사용해야 하는 SDE 추출법과는 달리 무색, 무취인 $CO_2$를 이용하여 정유 성분을 분리하는 초임계 추출법은 인체에 무해한 정유 성분을 얻을 수 있다는 것이 가장 큰 장점이라 사료되며, 분리된 정유 물질에 대해 성분 분석 결과 대부분이 휘발성 알코올 계열에 물질임을 확인할 수 있었다. 정유 성분들에 대한 생리활성 실험결과 항암, 항 돌연변이 그리고 신경활성이 아주 높은 것으로 나타나 aroma-theraphy로서의 가능성을 제시하였다고 사료된다. 나아가 이 정유성분에 대한 in vivo 실험을 통해 기초 의약품으로서 연구가 수행되어진다면 전통적인 치료제로서 사용된 천연물에 대한 현대적 가치부여가 가능하다고 생각된다.