• 대한금속재료학회지
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• 제49권8호
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• pp.589-595
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• 2011

Laminated glass fiber-reinforced plastic (GFRP) composites were applied to an insulating structure of a magnet system for a nuclear fusion device. Decreased inter-laminar strength by a strong repulsive force between coils which is induced a problem of structural integrity in laminated GFRPs. Therefore, it is important to investigate the inter-laminar characteristics of laminated GFRP composites in order to assure more reliable design and better structural integrity. Three types of the laminated GFRP composites using a high voltage insulating materials were fabricated according to each molding process. To evaluate the grade of the fabricated composites, mechanical tests, such as hardness, tensile and compressive tests,were carried out. The autoclave molding composites satisfied almost of the mechanical properties reguested at the G10 class standard, but the vacuum impregnation (VPI) and Prepreg composites did not.

• 한국생산제조학회지
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• 제20권2호
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• pp.202-206
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• 2011

Works on the strength and stiffness in the structural members are carried out widely with various material and cross-sections with ever increasing safety concerns, they are presently applied in various fields including railroad trains, air crafts and automobiles. In addition to this, problem of lighting structural members became important subject by control of exhaust gas emission, fuel economy and energy efficiency. So, Light weight of member structures is necessary for the high performance and various functions. In this study, the CFRP flat and circular member was manufactured by CFRP prepreg sheet in autoclave. Carbon FRP is an anisotropy material whose mechanical properties change with its fiber orientation angle, so this study apply to the effects of the fiber orientation angle on the bending characteristics of the member. Each CFRP flat and circle are compared by strength and stiffness.

• 한국자동차공학회논문집
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• 제17권3호
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• pp.15-21
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• 2009

The anisotropic mechanical properties were measured for the three orthogonal orientations of plain weave glass fabric reinforced epoxy resin laminate. In tensile and flexural tests, axial and edge type specimens failed by pull-out of warp and fill yarns, respectively. In contrast, the thickness type specimens failed by adhesive failure process. Longitudinal cracking occurred in several of the edge type specimens during tensile test. That cracking caused pop-in in the stress-strain curve. Defects induced by improper coupon machining caused that cracking.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2004년도 춘계학술대회
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• pp.192-197
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• 2004

The anisotropy in coefficient of thermal expansion (CTE) between the in-plane and out-of-plane of 3-dimensional thick composite structures induces residual stresses and the large void content due to insufficient compaction of fabric composites, which results in low interlaminar strengths. In order to reduce the through thickness CTE and the void content, in this work, carbon fabric phenolic laminates were compacted by pressure generated by autoclave and a compressive jig, from which the through-thickness CTEs and the void contents were measured. From the measurement, it was found that the through-thickness CTE and the void content had different characteristics from ordinary composites due to gas produced during the cure reaction of phenolic resin.

• 농업과학연구
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• 제31권1호
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• pp.9-14
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• 2004

This study was carried out for deresinning the larch boards dried in a conventional kiln. Prior to heat treatment they were steamed in an autoclave for 5 hours or frozen for 24 hours at a temperature of $-35^{\circ}C$. The velocities of ultrasound transmitted through the specimens were measured to examine the correlation with their resin contents. It was found that the specimens heated at $100^{\circ}C$ for 5 hours contained less resin that those heated at $200^{\circ}C$ for an hour. Both treatments of steaming and freezing were effective for deresinning and the former was better than the latter. The ultrasonic velocities measured before the heat treatment showed a negative correlation to the resin contents of the specimens, but those measured after the heat treatment a positive correlation. This difference may be attributed to the viscosity of resin.

• 약학회지
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• 제49권1호
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• pp.56-59
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• 2005

We synthesized new N-substituted 3-amino-6-chloropyridazine derivatives which were expected to retain biological activity. All synthetic process from pyridazine to 3-aminopyridazines could be carried out conveniently in high yield. N-Substituted 3-amino-6-chloropyridazine derivatives were prepared through amination and acylation from 3,6-dichloropyridazine. 3-Amino-6-chloropyridazine was prepared from the reaction of 3,6-dichloropyridazine with liquid ammonia under autoclave for 6 hrs. The refluxing of 3-amino-6-chloropyridazine and the corresponding acid anhydride for $1{\sim}2$ hrs afforded the N-substituted 3-amino-6-chloropyridazines. Alkyl chain of N-substituent was prolonged to six carbon (hexanoic acid).

• 소음진동
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• 제8권6호
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• pp.1078-1085
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• 1998

This study is carried out to investigate the characteristics of sound insulation performances for masonry walls. PC walls and ALC walls. For these purposes. 17 types of masonry walls were selected and tested in accordance with KS F 2808 at reverberation room The sound insulation performance of 8" cement block walls are graded with D-45 ∼ D-55 which are to be evaluated very favorable grade. 4" cement block walls are D-30 ∼ D-40. 1 B cement brick walls are D-40∼D-50 favorable grade. 0.5 B brick walls are D-30∼D-45. 150 mm PC wall is D-50. and ALC walls(150 mm, 200 mm) are D-30∼D-45.

• 한국안전학회지
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• 제12권4호
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• pp.57-62
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• 1997

The combined structure of hybrid composite made through the bonding process of materials of different properties greatly defines its mechanical characteristics, as the results of the experiments on materials of different properties show much dissimilarity. When carbon/epoxy materials are applied to hybrid composite, the carbon materials helps to improve the mechanical properties of the hybrid composite, and the epoxy reduces its fracture strain and impact resistance. Carbon fiber which is now in general commercialization is classified as high modulus or high strength system, and its manufacturing methods are various. The study of the materials having combined structure is focused on the numerical analysis of the layers of bonding surface in materials with difference modulus. The hybrid composite made through the multilayered bonding of reinforced aluminium sheets with aramid fiber now faces the marketing phase, and especially its excellent fatigue resistance and mechanical properties promote active researches on the similar products of hybrid composite. This study aims to investigate the effects of CFRP volume ratio and fiber's orientation over the properties of mechanical strength and fatigue life of the hybrid composite, AI7075/CFRP. To carry out this study, static tensile and fatigue tests were given to some of the panels which, made through the co-cure processing in an autoclave, have different CFRP volume ratio and carbon fiber orientations.

• Journal of the Korean Wood Science and Technology
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• 제19권4호
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• pp.80-84
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• 1991

Lignocellulosic biomass including acetosolv ricestraw and spruce lignin were liquefied and converted into liquid hydrocarbons by catalytic hydroliquefaction reaction. These experimental works were carried out in 1-liter-capacity autoclave using 50% tetralin and m-cresol solution respectively as soluble solvent and Ni. Pd. Fe and red mud as catalyst. $H_2$ gas was supplied into the reactor for escaltion of deoxhydroenolysis reaction. Catalyst concentrations were 1 % of raw material based on weight. The ratio between raw materials and soluble solvent are 1g and 10cc. The reaction conditions are 400-$700^{\circ}C$ of reaction temperature, 10-50 atms of reaction pressure. The highest yield of hydrocarbon, so called "product oil" showed 32% and 5.5% of lowest char formation when red mud was used as catalyst. The product oil yields from those of other catalysts were in the range of 20-29%. The influence of different initial hydrogen pressures was examined in the range d 30-50 atms. A minimum pressure of 35 atms was necessary to obtain a complete recovery of souble solvent for recycling.

• 펄프종이기술
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• 제46권2호
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• pp.8-15
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• 2014

A novel antibacterial paper coated with chitosan-based silver (Ag) nanocomposite prepared by green synthesis has been investigated for a wide range of application in food, agricultural and medical packaging. Green synthesis of Ag nanoparticles (AgNPs) was carried out by a chemical reaction involving a mixture of chitosan-silver nitrate (AgNO3) in an autoclave at 15 psi, $121^{\circ}C$, for 15-120 sec. AgNPs and their formation in chitosan were confirmed by both UV-Vis spectroscopy and transmission electron microscope (TEM). Fourier transform infrared spectroscopy (FTIR) study showed that free amino groups in chitosan act as an effective reductant and AgNPs stabilizer. Antibacterial test of coated paper with as-prepared chitosan-AgNPs was performed qualitatively against E. coli based on the formation of halo zones around coated papers and it was shown to be effective in suppressing the growth of E. coli with increasing Ag contents in coating layer.