• 제목/요약/키워드: Oil detector

검색결과 91건 처리시간 0.029초

Canola oil is an excellent vehicle for eliminating pesticide residues in aqueous ginseng extract

  • Cha, Kyu-Min;Lee, Eun-Sil;Kim, Il-Woung;Cho, Hyun-Ki;Ryu, Ji-Hoon;Kim, Si-Kwan
    • Journal of Ginseng Research
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    • 제40권3호
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    • pp.292-299
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    • 2016
  • Background: We previously reported that two-phase partition chromatography between ginseng water extract and soybean oil efficiently eliminated pesticide residues. However, an undesirable odor and an unpalatable taste unique to soybean oil were two major disadvantages of the method. This study was carried out to find an alternative vegetable oil that is cost effective, labor effective, and efficient without leaving an undesirable taste and smell. Methods: We employed six vegetable oils that were available at a grocery store. A 1-mL sample of the corresponding oil containing a total of 32 pesticides, representing four categories, was mixed with 10% aqueous ginseng extract (20 mL) and equivalent vegetable oil (7 mL) in Falcon tubes. The final concentration of the pesticides in the mixture (28 mL) was adjusted to approximately 2 ppm. In addition, pesticides for spiking were clustered depending on the analytical equipment (GC/HPLC), detection mode (electron capture detector/nitrogen-phosphorus detector), or retention time used. Samples were harvested and subjected to quantitative analysis of the pesticides. Results: Soybean oil demonstrated the highest efficiency in partitioning pesticide residues in the ginseng extract to the oil phase. However, canola oil gave the best result in an organoleptic test due to the lack of undesirable odor and unpalatable taste. Furthermore, the qualitative and quantitative changes of ginsenosides evaluated by TLC and HPLC, respectively, revealed no notable change before or after canola oil treatment. Conclusion: We suggest that canola oil is an excellent vehicle with respect to its organoleptic property, cost-effectiveness and efficiency of eliminating pesticide residues in ginseng extract.

변압기의 고장검출을 위한 유중 코로나 특성 연구 (Transformer diagnosis using characteristics of corona in Oil)

  • 권태원;곽희로;김재철;김응상;박민규
    • 한국조명전기설비학회:학술대회논문집
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    • 한국조명전기설비학회 1989년도 추계학술발표회논문집
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    • pp.65-70
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    • 1989
  • This paper presents resarch results on the use of a corona detector and a pulse counter in order to diagnose for oil transformers. Using these experimental apparatus, tests were carried out on a typical transformer oil containing different carbonized paper and various moisture contents to measure the picocoulomb val-ues and pulse count. Through the result of this study it was found that the picocoulomb values and pulse count of corona were depended on the getting stained in transformer oil. The amplitude of the partial discharge amount and the number of pulse were decreased up to 70 [。c] and then was increased as the oil temperature goes up. It was concluded that the determinati-on level for diagnosis of oil transform-er was taken into account the temperatu-er of transformer oil, The use of pulse counter method, which have been taken the same property of voltage and temperature variation for the corona measurement mothod, considera-bly increase insulator avilability.

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식물성 유지 10종에 대한 주요 Phytosterol 함량 분석 (Analysis of Major Phytosterol Contents for 10 Kind of Vegetable Oils)

  • 조상훈;이명진;김기유;박건영;강석호;엄경숙;강효정;박용배;윤미혜
    • 한국식품영양학회지
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    • 제34권2호
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    • pp.217-223
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    • 2021
  • Vegetable oils are a rich source of bioactive substances. Phytosterols in those have been known for many years for their properties for reducing blood cholesterol levels, as well as their other beneficial health effects. Phytosterols are triterpenes that are important structural components of plant cell membranes just as cholesterol does in animal cell membranes. The aim of this study was to provide consumers with information about phytosterol contents in vegetable oils in Korea market. The contents of major phytosterols (campesterol, stigmasterol, β-sitosterol) in 50 vegetable oils of 10 kinds (perilla oil, peanut oil, avocado oil, olive oil, pine nut oil, sesame oil, canola oil, coconut oil, grape seed oil, and sunflower oil) were analyzed by gas chromatography with flame ionization detector. The average contents of vegetable oils containing 5 or more samples were in the order of sesame oil (334.43 mg/100 g), perilla oil (262.16 mg/100 g), grape seed oil (183.71 mg/100 g), and olive oil (68.68 mg/100 g). Phytosterol content of sesame oil and perilla oil was high among vegetable oils.

Detection of the Ultrasonic Signals due to Partial Discharges in a 154kV Transformer

  • Kweon, Dong-Jin;Chin, Sang-Bum;Kwak, Hee-Ro
    • KIEE International Transactions on Electrophysics and Applications
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    • 제2C권6호
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    • pp.297-303
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    • 2002
  • We have developed an on-line ultrasonic detector to monitor partial discharge in an operating transformer. The ultrasonic sensor has 150[KHz] resonance frequency and contains a pre-amplifier with 60[㏈] gain. The on-line ultrasonic detector has 50~300[KHz] frequency band-pass filter to remove electrical and mechanical noises from the transformer. This detector has an ultrasonic signal discrimination algorithm which discriminates ultrasonic signals due to partial discharge in a transformer. A moving average method of ultrasonic signal number was employed to effectively monitor the increasing trend of the partial discharge. This paper describes an experience of partial discharge detection in a 154[㎸] operating transformer using an ultrasonic detector. With regards to gas analysis in oil, C2H2 gas was produced with a warning level in this transformer We detected ultrasonic signals on the transformer steel wall, and estimated the position of partial discharge. With further inspection, we found carbonized marks due to partial discharge on the supporting bolt which fastens the windings.

유중 부분방전 펄스 특성을 이용한 TF 분석에 대한 고찰 (Considerations on the TF Anal,ysis using Partial Discharge Pulse Characteristics in Oil)

  • 김정태
    • 대한전기학회논문지:전기물성ㆍ응용부문C
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    • 제54권11호
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    • pp.508-514
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    • 2005
  • In this paper, it was investigated the characteristics of PD(partial discharge) pulse shapes in oil and the possibility of TF(Time-Frequency) analysis for the discrimination of air corona in on-site PD measurement of oil transformers. For the purpose, single and multiple discharges combined with oil discharges and air corona were generated and measured by use of artificial models through the HFPD pulse detector and the oscilloscope. PD pulse shapes were different according to the type of defects, especially including air corona- pulses. Also, through the TF analysis, data clusters could be classified each other in the TF Map, even in the case of multiple discharges. Therefore, it is known that TF analysis could be aprlied for the improvement of on-site PD measurement in oil transformers.

사철쑥 정유의 저장 중 향기성분 변화 (Changes in the Volatile Compounds of Artemisia capillaris Essential Oil during Storage)

  • 정미숙
    • 한국식품조리과학회지
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    • 제23권4호통권100호
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    • pp.413-422
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    • 2007
  • In this study, changes in the volatile compounds of Artemisia capillaris essential oil were investigated under six different storage conditions for 6 months. The essential oil was collected by steam distillation and analyzed by a gas chromatography-mass selective detector (GC-MSD). Seventy-five volatile compounds were identified from the fresh essential oil of Artemisia capillaris. During storage, the total levels of aldehydes, alcohols, and ketones slightly decreased and the level of hydrocarbons greatly decreased; the total level of esters also decreased in the essential oil. Notably, the levels of carvacrol, eugenol, myrcene, 1,8-cineole, caryophyllene, coumarin, ${\alpha}-thujone$, ${\beta}-thujone$, borneol, and ${\gamma}-terpinene$, known as antioxidants and antimicrobial agents, decreased during storage. Finally, aerobic storage conditions caused greater reductions in some compounds even at low temperatures.

참기름의 특이성분함량(特異成分含量)과 순도결정(純度決定)에 관(關)한 연구(硏究) (제(第) 1 보(報)) -Sesamin 및 관련(關聯)Sterol를 중심(中心)으로- (Studies on the Contents of Special Components and Estimation of Purity in Sesame oil -I : Contents of Sesamin and Sterols-)

  • 노일협;이문선
    • Journal of Nutrition and Health
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    • 제16권2호
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    • pp.107-114
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    • 1983
  • There has been no specific test available for identifying the sesame oil among common edible oils. As the contents of sesamin and the ratio of sterols allowed the estimation for the genuine sesame oil, the author investigated to establish some instrumental methods for verification of genuine sesame oil and its distribution in the market. The sesame oil was saponified and the sesamin and sterols were isolated from the unsaponiable fraction by Florisil column chromatography. The individual components were determined by gas- chromatography and sesamin standard (purified sesamin) was obtained by silicagel column chromatography. The gas- chromatographic condition using Flame Ionization Detector supported on 10% OV-101 with di-(2-ethylhexyl) sebacate as an internal standard was suitable, and quantitation of sesamin and sterols, including campesterol, stigmasterol and ${\beta}-sitosterol$ was carried out. The results of this study showed that contents of sesamin in genuine sesame oil were 0.3-0.5% and the ratio of stigmasterol to compesterol was 0.3-0.6 and ${\beta}-sitosterol$ to campesterol 3.0-3.8. The 50 samples from the markets in Seoul were composed of 70% genuine sesame oil, and others were mixed with palm oil, rape seed oil and soybean oil.

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변압기 절연유중 수소 가스의 검지 시스템 설계 (Developement of Gas Detector Dissolved In Transfomer Oil)

  • 황규현;서호준;이동희
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2004년도 하계학술대회 논문집 Vol.5 No.1
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    • pp.207-210
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    • 2004
  • In oil-filled equipment such as transformers, partial discharge or local overheating will make insulating material(oil, kraft paper, proclain and wood) be stressed and generate many sort of gases($CO,\;CO_2,\;H_2,\;C_2H_4$) which are dissolved in transformer oil. The ratio of this gas can make diagnostic tecchniques of the lifetime of transfomer so, it is important to monitoring $H_2$ gas continuously. This paper developes a system of detecting about $H_2$ gas by using $H_2$ gas sensor, and we describe operation and performance of this system

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초피 정유의 저장 중 향기성분 변화 (Compositional Changes in Essential Oil of Zanthoxylum piperitum A.P. DC. During Storage)

  • 정미숙
    • 한국식생활문화학회지
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    • 제21권4호
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    • pp.433-438
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    • 2006
  • Compositional changes In essential oil of Zanthoxylum piperitum A.P. DC. were investigated under six different storage conditions for 3 months. Essential oil from Zanthoxylum piperitum was collected by steam distillation method and analyzed by gas chromatography-mass selective detector (GC-MSD). Forty-one volatile compounds, consisting of 12 hydrocarbons, 11 alcohols, 8 aldehydes, 3 oxides, 3 esters, 3 ketones and 1 acid were identified from the fresh essential oil of Zanthoxylum piperitum. In essential oils, compositional changes occurred in particularly monoterpene hydrocarbons. Total levels of ketones, esters, oxides and alcohols increased during storage. Moreover, aerobic condition caused decrease in a few constituents duringstorage even at low temperature.

변압기 절연유중 수소 가스의 검지 시스템 설계 (Developement of Gas Detector Dissolved In Transfomer Oil)

  • 황규현;서호준;이동희
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2004년도 하계학술대회 논문집 C
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    • pp.1842-1844
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    • 2004
  • In oil-filled equipment such as transformers, partial discharge or local overheating will make insulating material(oil, kraft paper, proclain and wood) be stressed and generate many sort of gases(CO, $CO_2,\;H_2,\;C_2H_4$) which are dissolved in transformer oil. The ratio of this gas can make diagnostic tecchniques of the lifetime of transfomer so, it is important to monitoring $H_2$ gas continuously. This paper developes a system of detecting about $H_2$ gas by using $H_2$ gas sensor, and we describe operation and performance of this system.

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