• Title/Summary/Keyword: Novel metal

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A Novel Method to Fabricate Tough Cylindrical Ti2AlC/Graphite Layered Composite with Improved Deformation Capacity

  • Li, Aijun;Chen, Lin;Zhou, Yanchun
    • Journal of the Korean Ceramic Society
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    • v.49 no.4
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    • pp.369-374
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    • 2012
  • Based on the structure feature of a tree, a cylindrical $Ti_2AlC$/graphite layered composite has been fabricated through heat treating a graphite column and six close-matched thin wall $Ti_2AlC$ cylinders bonded with the $Ti_2AlC$ powders at $1300^{\circ}C$ and low oxygen partial pressure. SEM examination reveals that the bond interlayers between cylinders or that between cylinder and column are not fully dense without any crack formation. During the compressive test, the strain of the $Ti_2AlC$/graphite layered composite is about twice higher than that of the monolithic $Ti_2AlC$ ceramic, and the compressive strength of the layered composite is 348 MPa. The layered composite show the noncatastrophic fracture behaviors due to the debonding and shelling off of the layers, which are different from the monolithic $Ti_2AlC$ ceramic. The mechanism of the improved deformation capacity and noncatastrophic failure modes are attributed to the presence of the central soft graphite column and cracks deflection by the bond interlayers.

Development of Nitric Acid Free Desmut Solution for the Aluminum Alloy in Alkaline Etching and Acid Desmut Processes (Aluminum 합금소재의 알칼리에칭 공정으로 발생한 Smut 제거를 위한 무질산 혼합산용액 개발)

  • Choo, Soo-Tae;Choi, Sang Kyo
    • Clean Technology
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    • v.9 no.2
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    • pp.57-61
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    • 2003
  • A novel nitric acid-free desmut solution has been developed to remove smut, which is produced from a NaOH etching, on the surface of aluminum alloy metal in metal surface treatment processes. Comparing with the performance of 5% $HNO_3$ desmut solution, the mixed acid solution containing 2% $H_2O_2$, 0.5% HF, and 10% $H_2SO_4$ shows the same effect of smut removal for aluminum alloy samples of A16061 and A15052. To examine the surface alterations of the aluminum samples, in addition, the surface analysis is carried out with scanning electron microscopy (SEM) and electron probe microanalysis (EPMA).

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A High Frequency Complex Modulation Method of the Electronic Ballast for Metal Halide Lamps (메탈 할라이드 램프용 전자식 안정기의 고주파 복합 변조법)

  • 오덕진;김희준;조규민
    • Journal of the Institute of Electronics Engineers of Korea SC
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    • v.40 no.3
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    • pp.215-224
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    • 2003
  • This paper presents an electronic ballast using a novel complex modulation method for the metal halide lamp. The proposed modulation method, which has a modulating signal of swept complex frequency, can eliminate the acoustic resonance more effectively than the conventional modulation method, which has a modulating signal of constant frequency. For the purpose of future application specific integrated circuits (ASIC). the controller of the proposed ballast has been designed only with erasable programmable logic devices (EPLDs), but without a microprocessor. In this paper, detailed proposed modulation schemes are described and experimental results on the proto type 150W metal halide lamp ballast with the proposed modulation method ate discussed.

Fabrication and Characterization of Carbon Nanotube/Cu Nanocomposites by Molecular Level Mixing Process (분자수준 혼합공정을 이용한 탄소나노튜브/Cu 나노복합재료의 제조 및 특성평가)

  • Kim, Kyung-Tae;Cha, Seung-Il;Hong, Soon-Hyung
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2005.04a
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    • pp.261-264
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    • 2005
  • Since the first discovery of carbon nanotube (CNT) in 1991, a window to new technological areas has been opened. One of the emerging applications of CNTs is the reinforcement of composite materials to overcome the performance limits of conventional materials. However, because of the difficulties in distributing CNTs homogeneously in metal or ceramic matrix by means of traditional composite processes, it has been doubted whether CNTs can really reinforce metals or ceramics. In this study, CNT reinforced Cu matrix nanocomposite is fabricated by a novel fabrication process named molecular level mixing process. This process produces CNT/Cu composite powders whereby the CNTs are homogeneously implanted within Cu powders. The CNT/Cu nanocomposite, consolidated by spark plasma sintering of CNT/Cu composite powders, shows to be 3 times higher strength and 2 times higher Young’s modulus than Cu matrix. This extra-ordinary strengthening effect of carbon nanotubes in metal is higher than that of any other reinforcement ever used for metal matrix composites.

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Preparation of Pt/C catalyst for PEM fuel cells using polyol process (Polyol Process를 통한 PEM Fuel Cell용 Pt/C촉매 제조)

  • Oh, Hyoung-Seok;Kim, Han-Sung
    • 한국신재생에너지학회:학술대회논문집
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    • 2006.11a
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    • pp.443-446
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    • 2006
  • Carbon-supported Platinum (Pt) is the potential electro-catalyst material for anodic and cathodic reactions in fuel cell. Catalytic activity of the metal strongly depends on the particle shape, size and distribution of the metal in the porous supportive network. Conventional preparation techniques based on wet impregnation and chemical reduction of the metal precursors often do not provide adequate control of particle size and shape. We have proposed a novel route for preparing nano sized Pt colloidal particles in solution by oxidation of ethylene glycol. These Pt nano particles were deposited on large surface area carbon support. The process of nano Pt colloid formation involves the oxidation of solvent ethylene glycol to mainly glycolic acid and the presence of its anion glycolate depends on the solution pH. In the process of colloidal Pt formation glycolate actsas stabilizer for the Pt colloidal particle and prevents the agglomeration of colloidal Pt particles. These mono disperse Pt particles in carbon support are found uniformly distributed in nearly spherical shape and the size distribution was narrow for both supported and unsupported metals. The average diameter of the Pt nano particle was controlled in the range off to 3 nm by optimizing reaction parameters. Transmission electron microscopy, CV and RRDE experiments were used to compliment the results.

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A Development of Longitudinal and Transverse Springback Prediction Model Using Artificial Neural Network in Multipoint Dieless Forming of Advanced High Strength Steel (초고강도 판재 다점성형공정에서의 인공신경망을 이용한 2중 곡률 스프링백 예측모델 개발)

  • Kwak, M.J.;Park, J.W.;Park, K.T.;Kang, B.S.
    • Transactions of Materials Processing
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    • v.29 no.2
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    • pp.76-88
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    • 2020
  • The need for advanced high strength steel (AHSS) forming technology is increasing as interest in light weight and safe automobiles increases. Multipoint dieless forming (MDF) is a novel sheet metal forming technology that can create any desired longitudinal and transverse curvature in sheet metal. However, since the springback phenomenon becomes larger with high strength metal such as AHSS, predicting the required MDF to produce the exact desired curvature in two directions is more difficult. In this study, a prediction model using artificial neural network (ANN) was developed to predict the springback that occurs during AHSS forming through MDF. In order to verify the validity of model, a fit test was performed and the results were compared with the conventional regression model. The data required for training was obtained through simulation, then further random sample data was created to verify the prediction performance. The predicted results were compared with the simulation results. As a result of this comparison, it was found that the prediction of our ANN based model was more accurate than regression analysis. If a sufficient amount of data is used in training, the ANN model can play a major role in reducing the forming cost of high-strength steels.

A novel approach to predict surface roughness in machining operations using fuzzy set theory

  • Tseng, Tzu-Liang (Bill);Konada, Udayvarun;Kwon, Yongjin (James)
    • Journal of Computational Design and Engineering
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    • v.3 no.1
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    • pp.1-13
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    • 2016
  • The increase of consumer needs for quality metal cutting related products with more precise tolerances and better product surface roughness has driven the metal cutting industry to continuously improve quality control of metal cutting processes. In this paper, two different approaches are discussed. First, design of experiments (DOE) is used to determine the significant factors and then fuzzy logic approach is presented for the prediction of surface roughness. The data used for the training and checking the fuzzy logic performance is derived from the experiments conducted on a CNC milling machine. In order to obtain better surface roughness, the proper sets of cutting parameters are determined before the process takes place. The factors considered for DOE in the experiment were the depth of cut, feed rate per tooth, cutting speed, tool nose radius, the use of cutting fluid and the three components of the cutting force. Finally the significant factors were used as input factors for fuzzy logic mechanism and surface roughness is predicted with empirical formula developed. Test results show good agreement between the actual process output and the predicted surface roughness.

Precision measuring of burrs on sheet metal using the laser (레이저를 이용한 박판 버의 정밀측정)

  • 신홍규;홍남표;김헌영;김병희
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2003.06a
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    • pp.1824-1827
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    • 2003
  • The sheet metal shearing process is normally used in the precision elements such as semi-conductor components. In precision elements, burrs usually reduce the quality of machined parts and cause interference, jamming and misalignment during assembly procedures and because of their sharpness, they can be safety hazard to personnel. Furthermore, not only burrs are hard to predict and avoid, but also deburring, the process of removing burrs, is time-consuming and costly. In order to get the burr-free parts, therefore, we developed the precise burr measuring system using the laser. The laser burr measuring system consists of the laser probe, the photo detector, the achromatic doublet lens, and the rotary & the X-Y table. In previous reports, we used simple vertical measuring method. But, as we used relatively bigger laser spot diameter and had the limited reflection angle, it was difficult to obtain the precise measuring results. So called, the spot size effect makes the profile of burr measured distorted and the burr height measured smaller. By introducing the novel laser measuring method which employing the achromatic lens system and the tilting mechanism, we could make the spot size smaller and get the appropriate beam direction angle. Through the experiments, the accuracy of the developed system is proved. The burr height measured during the punching process can be used for automatic deburring and in-situ aligning.

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AFM-based nanofabrication with Femtosecond pulse laser radiation (원자간력 현미경(AFM)과 펨토초 펄스 레이저를 이용한 나노 형상 가공)

  • Kim Seung-Chul;Kim Seung-Woo
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2006.05a
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    • pp.149-150
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    • 2006
  • We describe a novel method of scanning probe nanofabrication using a AFM(atomic force microscopy) tip with assistance of Femtosecond laser pulses to enhance fabrication capability. Illumination of the AFM tip with ultra-short light pulses induces a strong electric field between the tip and the metal surface, which allows removing metal atoms from the surface by means of field evaporation. Quantum simulation reveals that the field evaporation is triggered even en air when the induced electric field reaches the level of a few volts per angstrom, which is low enough to avoid unwanted thermal damages on most metal surfaces. For experimental validation, a Ti: sapphire Femtosecond pulse laser with 10 fs pulse duration at 800 nm center wavelength was used with a tip coated with gold to fabricate nanostructures on a thin film gold surface. Experimental results demonstrate that fine structures with critical dimensions less than ${\sim}10nm$ can be successfully made with precise control of the repetition rate of Femtosecond laser pulses.

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Graphene Oxide Thin Films for Nonvolatile Memory Applications

  • Kim, Jong-Yun;Jeong, Hu-Young;Choi, Hong-Kyw;Yoon, Tae-Hyun;Choi, Sung-Yool
    • Proceedings of the Korean Vacuum Society Conference
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    • 2011.02a
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    • pp.9-9
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    • 2011
  • There has been strong demand for novel nonvolatile memory technology for low-cost, large-area, and low-power flexible electronics applications. Resistive memories based on metal oxide thin films have been extensively studied for application as next-generation nonvolatile memory devices. However, although the metal oxide-based resistive memories have several advantages, such as good scalability, low-power consumption, and fast switching speed, their application to large-area flexible substrates has been limited due to their material characteristics and necessity of a high-temperature fabrication process. As a promising nonvolatile memory technology for large-area flexible applications, we present a graphene oxide-based memory that can be easily fabricated using a room temperature spin-casting method on flexible substrates and has reliable memory performance in terms of retention and endurance. The microscopic origin of the bipolar resistive switching behaviour was elucidated and is attributed to rupture and formation of conducting filaments at the top amorphous interface layer formed between the graphene oxide film and the top Al metal electrode, via high-resolution transmission electron microscopy and in situ x-ray photoemission spectroscopy. This work provides an important step for developing understanding of the fundamental physics of bipolar resistive switching in graphene oxide films, for the application to future flexible electronics.

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