• Title/Summary/Keyword: Non-destructive techniques

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Calibration Methods for the Gas Chromatographic Analysis of ppt-level Hydrogen Sulfide (H2) in Air (환경 대기 중 ppt 수준의 황화수소 분석을 위한 GC 방식의 검량 기법에 대한 연구)

  • 김기현;오상인;최여진;최규훈;주도원
    • Journal of Korean Society for Atmospheric Environment
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    • v.19 no.6
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    • pp.679-687
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    • 2003
  • In this study, we investigated the analytical techniques to quantify the ambient concentration of hydrogen sulfide (H$_2$S) in air at ppt concentration level. For this purpose, an on-line GC analytical system equipped with both pulsed-flame photometric detector (PFPD) and thermal desorption unit (TDU) was investigated by collecting ambient air samples. The results of our study generally indicated that calibration conditions of GC system is highly sensitive to affect the accuracy of the analytical technique. Most importantly. we found that the use of different matrices in the the preparation stage of working standards was sensitive to control the overall performance of this technique. The calibration of our analytical system was tested by the two types of working standard (prepared by mixing either with high purity $N_2$ or with the ambient air). According to this test, the latter represented more efficiently the detecting conditions of actual air samples. The peak occurrence patterns of both air samples and standards (prepared by mixing with ambient air) were altered in a similar manner as the function of the loaded volume; however, it was not the case for the $N_2$-mixed standards. Results of our study suggest that detection of H$_2$S is highly different from other sulfides and that its quantification requires minimiaing interfering effects of non -pure substance (like water vapor) and (either sorptive or destructive) loss effects.

Damage Detection in Time Domain on Structural Damage Size (구조물의 손상크기에 따른 시간영역에서의 손상검출)

  • Kwon Tae-Kyu;Yoo Gye-Hyoung;Lee Seong-Cheol
    • Journal of the Korean Society for Precision Engineering
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    • v.23 no.6 s.183
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    • pp.119-127
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    • 2006
  • A non-destructive time domain approach to examine structural damage using parameterized partial differential equations and Galerkin approximation techniques is presented. The time domain analysis for damage detection is independent of modal parameters and analytical models unlike frequency domain methods which generally rely on analytical models. The time history of the vibration response of the structure was used to identify the presence of damage. Damage in a structure causes changes in the physical coefficients of mass density, elastic modulus and damping coefficients. This is a part of our ongoing effort on the general problem of modeling and parameter estimation for internal damping mechanisms in a composite beam. Namely, in detecting damage through time-domain or frequency-domain data from smart sensors, the common damages are changed in modal properties such as natural frequencies, mode shapes, and mode shape curvature. This paper examines the use of beam-like structures with piezoceramic sensors and actuators to perform identification of those physical parameters, and detect the damage. Experimental results are presented from tests on cantilevered composite beams damaged at different locations and different dimensions. It is demonstrated that the method can sense the presence of damage and obtain the position of a damage.

Comparison of FEA with Condition Monitoring for Real-Time Damage Detection of Bearing Using Infrared Thermography Techniques (적외선열화상을 이용한 베어링 실시간 손상검출 상태감시의 전산수치해석 비교)

  • Kim, Hojong;Kim, Wontae
    • Journal of the Korean Society for Nondestructive Testing
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    • v.35 no.3
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    • pp.185-192
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    • 2015
  • Since real-time monitoring systems, such as early fault detection, have been very important, an infrared thermography technique was proposed as a new diagnosis method. This study focused on damage detection and temperature characteristic analysis of ball bearings using the non-destructive, infrared thermography method. In this paper, for the reliability assessment, infrared experimental data were compared with finite element analysis (FEA) results from ANSYS. In this investigation, the temperature characteristics of ball bearing were analyzed under various loading conditions. Finally, it was confirmed that the infrared thermography technique was useful for the real-time detection of damage to bearings.

An Image Processing Algorithm for a Visual Weld Defects Detection on Weld Joint in Steel Structure (강구조물 용접이음부 외부결함의 자동검출 알고리즘)

  • Seo, Won Chan;Lee, Dong Uk
    • Journal of Korean Society of Steel Construction
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    • v.11 no.1 s.38
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    • pp.1-11
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    • 1999
  • The aim of this study is to construct a machine vision monitoring system for an automatic visual inspection of weld joint in steel structure. An image processing algorithm for a visual weld defects detection on weld bead is developed using the intensity image. An optic system for getting four intensity images was set as a fixed camera position and four different illumination directions. The input images were thresholded and segmented after a suitable preprocessing and the features of each region were defined and calculated. The features were used in the detection and the classification of the visual weld defects. It is confirmed that the developed algorithm can detect weld defects that could not be detected by previously developed techniques. The recognized results were evaluated and compared to expert inspectors' results.

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A Sequential Separation Procedure for the Determination of Uranium, Thorium and Their Isotopes in Geological Materials (지질시료 중의 U과 Th 분석 및 자연방사성동위원소 측정을 위한 화학적 분리)

  • Kim, Jung Suk;Choi, Kwang Soon
    • Analytical Science and Technology
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    • v.10 no.5
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    • pp.307-314
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    • 1997
  • Inductively coupled plasma atomic emission spectrometry(ICP/AES) was used for the determination of uranium and thorium in geological materials. Samples were predecomposed by mixed acid digestion technique. The separation of the uranium and thorium was achieved by systematic solvent extraction with TTA(thenoyltrifluoroacetone) and TOA (tri-n-octylamine) and back extraction into HCl. The results for standard rock sample, NIST SRM 278, showed a good agreement with those certified from NIST as well as found values by other non-destructive techniques. Additional purification for extracted portions was carried out by anion exchange chromatography for measurement of several natural radioisotopes of uranium and thorium by alpha spectrometry.

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Quantitative nondestructive evaluation of thin plate structures using the complete frequency information from impact testing

  • Lee, Sang-Youl;Rus, Guillermo;Park, Tae-Hyo
    • Structural Engineering and Mechanics
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    • v.28 no.5
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    • pp.525-548
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    • 2008
  • This article deals the theory for solving an inverse problem of plate structures using the frequency-domain information instead of classical time-domain delays or free vibration eigenmodes or eigenvalues. A reduced set of output parameters characterizing the defect is used as a regularization technique to drastically overcome noise problems that appear in imaging techniques. A deconvolution scheme from an undamaged specimen overrides uncertainties about the input signal and other coherent noises. This approach provides the advantage that it is not necessary to visually identify the portion of the signal that contains the information about the defect. The theoretical model for Quantitative nondestructive evaluation, the relationship between the real and ideal models, the finite element method (FEM) for the forward problem, and inverse procedure for detecting the defects are developed. The theoretical formulation is experimentally verified using dynamic responses of a steel plate under impact loading at several points. The signal synthesized by FEM, the residual, and its components are analyzed for different choices of time window. The noise effects are taken into account in the inversion strategy by designing a filter for the cost functional to be minimized. The technique is focused toward a exible and rapid inspection of large areas, by recovering the position of the defect by means of a single accelerometer, overriding experimental calibration, and using a reduced number of impact events.

Study on the Debonding Detection Techniques of Liner/Propellant Interface of Rocket Motor (추진기관의 라이너/추진제 미접착 검출 기법 연구)

  • Kim, Dong-Ryun;Ryoo, Baek-Neung
    • Journal of the Korean Society of Propulsion Engineers
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    • v.12 no.2
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    • pp.40-47
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    • 2008
  • It is known that the adhesive interface testing of the rocket motor using the ultrasonic wave is superior to the other testing methods about the ability to economical detect the defects. But, the signal analysis of the ultrasonic wave takes a lot of time and efforts because the time interval of the transmitted pulse and the received pulse is too short to separate the reflected signals due to the multi-layers of the rocket motor. The ultrasonic testing of rocket motor have only applied to the automatic system about extremely limited areas like the debond in adhesive interface between the motor case and the insulator. In this study the new technique to detect the debond between the liner and the propellant using the property of the resonance and the lamb waves instead of the existing ultrasonic testing was described.

Determination of defect depth in industrial radiography imaging using MCNP code and SuperMC software

  • Khorshidi, Abdollah;Khosrowpour, Behzad;Hosseini, S. Hamed
    • Nuclear Engineering and Technology
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    • v.52 no.7
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    • pp.1597-1601
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    • 2020
  • Background: Non-destructive evaluation of defects in metals or composites specimens is a regular method in radiographic imaging. The maintenance examination of metallic structures is a relatively difficult effort that requires robust techniques for use in industrial environments. Methods: In this research, iron plate, lead marker and tungsten defect with a 0.1 cm radius in spherical shape were separately simulated by MCNP code and SuperMC software. By 192Ir radiation source, two exposures were considered to determine the depth of the actual defined defect in the software. Also by the code, displacement shift of the defect were computed derived from changing the source location along the x- or y-axis. Results: The computed defect depth was identified 0.71 cm in comparison to the actual one with accuracy of 13%. Meanwhile, the defect position was recognized by disorder and reduction in obtained gamma flux. The flux amount along the x-axis was approximately 0.5E+11 units greater than the y-axis. Conclusion: This study provides a method for detecting the depth and position of the defect in a particular sample by combining code and software simulators.

Accuracy Enhancement of Reflection Signals in Impact Echo Test

  • Lho, Byeong-Cheol
    • Journal of the Korea Concrete Institute
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    • v.15 no.6
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    • pp.924-929
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    • 2003
  • A majority of infrastructures has been deteriorated over time. Therefore, it is very important to verify the quality of construction, and the level of structural deterioration in existing structures, to ensure their safety and functionality. Many researchers have studied non-destructive testing (NDT) methods to identify structural problems in existing structures. The impact echo technique is one of the widely used NDT techniques. The impact echo technique has several inherent problems, including the difficulties in P-wave velocity evaluation due to inhomogeneous concrete properties, deterioration of evaluation accuracy where multiple reflection boundaries exist, and the influence of the receiver location in evaluating the thickness of the tested structures. Therefore, the objective of this paper is to propose an enhanced impact echo technique that can reduce the aforementioned problems and develop a Virtual Instrument for the application via a thickness evaluation technique which has same technical background to find deterioration in concrete structures. In the proposed impact echo technique, transfer function from dual channel system analysis is used, and coherence is improved to achieve reliable data. Also an averaged signal -ensemble- is used to achieve more reliable results. From the analysis of transfer function, the thickness is effectively identified.

Measurement of Vibration Mode Shapes Using Time Average ESPI (시간 평균 ESPI를 이용한 진동 물체의 모우드 형태의 계측)

  • Kang, Young-June;Choi, Jang-Seob
    • Journal of the Korean Society for Precision Engineering
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    • v.13 no.2
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    • pp.84-93
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    • 1996
  • Non-destructive inspection techniques using laser have been broading their application areas as well as growing their measurement skills together with the rapid development of circumferential technology like fiber optics, computer and image processing. The ESPI technique is already on the stage of on-line testing with commercial products in developed country nations. Especially, this technique is expected to be applied to the nuclear industry, automobile and aerospace because it is proper for the vibration measurement and it can be applied to objects of a high temperature. This paper describes the use of the ESPI system for measuring vibration patterns on the reflecting objects. Using this system, high-quality Jo fringes for identifying mode shapes are displayed. A bias vibration is introduced into the reference beam to shift the Jo fringes so that fringe shift algorithms can be used to determine vibration amplitude. Using this method, amplitude fields for vibrating objects were obtained directly from the time-average interferograms recorded by the ESPI system.

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