• Title/Summary/Keyword: Nitrogen pressure

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Studies on Stability of Soymilk Suspension (두유(豆乳)의 현탁안정성에 관한 연구)

  • Kim, Eun-Soo;Jo, Jae-Sun
    • Korean Journal of Food Science and Technology
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    • v.22 no.3
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    • pp.312-318
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    • 1990
  • The effects of blanching, homogenization and heat sterilization on the stability of soymilk suspension were investigated by determination of nitrogen solubility index(NSI) of suspension and measuring the volume of precipitates and cream separated. The results obtained were that the NSI was decreased as the blanching temperature increased from $50^{\circ}C\;to\;80^{\circ}C$. The soybean particles having $8{\mu}$ by grinding showed more stable soymilk than that of $53{\mu}$. The stability was increased as the homogenizing pressure increased to $200kg/cm^2$ and repeated homogenizing process gave more stability than single one. The sterilization resulted a significant decrease in stability as it was heated at $120^{\circ}C-125^{\circ}C$ for more than 30 minutes.

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Fabricatiion and Characterization of ${Bi_2}{Sr_2}{CaCu_2}{O_8}$ Superconductor Thick Films on Cu Substrates using Cu-free Precursors (Cu-free 전구체를 이용하여 구리 기판 위에 ${Bi_2}{Sr_2}{CaCu_2}{O_8}$ 초전도 후막의 제조 및 특성)

  • 한상철;김상준;한영희;성태현;한병성
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.13 no.4
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    • pp.349-358
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    • 2000
  • Fabrication and Characterization of Bi$_{2}$/Sr$_{2}$/CaCu$_{2}$/O$_{8}$(Bi2212) superconductor thick films were fabricated successfully on C tapes by liquid reaction between Cu-free precursors of Bi$_{x}$/SrCaO/$_{y}$(x=1.2-2) and Cu tapes. Cu-free Bi-Sr-Ca-O powder mixtures were screen-printed on Cu tapes and heat-treated at 850-87$0^{\circ}C$ for several minutes in air oxygen nitrogen and low oxygen pressure. In order to obtain the optimum heat-treatment condition we studied the effect of the precursor composition the printing thickness and the heat-treatment atmosphere on the superconducting properties of Bi2212 films and the reaction mechanism. Microstructures and phases of thick films were analyzed by films and the reaction mechanism. Microstructures and phases of thick films were analyzed by optical microscope and XRD. The electric properties of superonducting films were examined by the four probe method. At heat-treatment temperature the thick films were in a partially molten state by liquid reaction between CuO of the oxidized copper tape and the precursors which were printed on Cu tapes. During the heat-treatment procedure Bi2212 superconducting particle nucleate and grow in preferred orientations.ons.s.

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Magnetic Properties of Fe-Zr-N Soft Magnetic Thin Films (Fe-Zr-N 연자성 박막의 자기적 성질)

  • 김택수;김종오;이중환;윤선진;김좌연
    • Journal of the Korean Magnetics Society
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    • v.6 no.5
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    • pp.317-322
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    • 1996
  • Thin films of Fe-Zr-N were fabricated by rf magnetron reactive sputtering method. The saturation magnetization and coercivity as functions of annealing temperature and partial pressure of nitrogen gas, effective permeability at high frequencies, and thermal stability were investigated. Magnetic softness was exhibited in the composition range of $Fe_{72-78}Zr_{7-10}N_{15-18}$ which was boundary between polycrystalline and amorphous structure. These films exhibited magnetic softness with saturation magentic flux density of 1.55 T and effective permeability of about 3000 at 1 MHz. These films also exhibited thermal stability by sustaining effective permeability of 2500 or above as the temperature was raised to $550^{\circ}C$. It is asswned that good magnetic softness is obtained because grain growth of $\alpha-Fe$ is prohibited due to the precipitation of ZrN nanocrystals. The grain sizes of $\alpha-Fe$ films were $40~50\AA$ and the grain sizes of ZrN nanocrystals were $10~15\AA$.

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COMMISSIONING RESULT OF THE KSTAR HELIUM REFRIGERATION SYSTEM

  • Park, Dong-Seong;Chang, Hyun-Sik;Joo, Jae-Joon;Moon, Kyung-Mo;Cho, Kwang-Woon;Kim, Yang-Soo;Bak, Joo-Shik;Cho, Myeon-Chul;Kwon, Il-Keun;Andrieu, Frederic;Beauvisage, Jerome;Desambrois, Stephane;Fauve, Eric
    • Nuclear Engineering and Technology
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    • v.40 no.6
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    • pp.467-476
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    • 2008
  • To keep the superconducting (SC) magnet coils of KSTAR at proper operating conditions, not only the coils but also other cold components, such as thermal shields (TS), magnet structures, SC bus-lines (BL), and current leads (CL) must be maintained at their respective cryogenic temperatures. A helium refrigeration system (RRS) with an exergetic equivalent cooling power of 9 kW at 4.5 K without liquid nitrogen ($LN_2$) pre-cooling has been manufactured and installed. The main components of the KST AR helium refrigeration system (HRS) can be classified into the warm compression system (WCS) and the cryogenic devices according to the operating temperature levels. The process helium is compressed from 1 bar to 22 bar passing through the WCS and is supplied to cryogenic devices. The main components of cryogenic devices are consist of cold box (C/B) and distribution box (D/B). The C/B cool-down and make the various cryogenic helium for the KSTAR Tokamak and the various cryogenic helium is distributed by the D/B as per the KSTAR requirement. In this proceeding, we will present the commissioning results of the KSTAR HRS. Circuits which can simulate the thermal loads and pressure drops corresponding to the cooling channels of each cold component of KSTAR have been integrated into the helium distribution system of the HRS. Using those circuits, the performance and the capability of the HRS, to fulfill the mission of establishing the appropriate operating condition for the KSTAR SC magnet coils, have been successfully demonstrated.

Enhancement of Pool Boiling Heat Transfer in Water Using Sintered Copper Microporous Coatings

  • Jun, Seongchul;Kim, Jinsub;Son, Donggun;Kim, Hwan Yeol;You, Seung M.
    • Nuclear Engineering and Technology
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    • v.48 no.4
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    • pp.932-940
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    • 2016
  • Pool boiling heat transfer of water saturated at atmospheric pressure was investigated experimentally on Cu surfaces with high-temperature, thermally-conductive, microporous coatings (HTCMC). The coatings were created by sintering Cu powders on Cu surfaces in a nitrogen gas environment. A parametric study of the effects of particle size and coating thickness was conducted using three average particle sizes (APSs) of $10{\mu}m$, $25{\mu}m$, and $67{\mu}m$ and various coating thicknesses. It was found that nucleate boiling heat transfer (NBHT) and critical heat flux (CHF) were enhanced significantly for sintered microporous coatings. This is believed to have resulted from the random porous structures that appear to include reentrant type cavities. The maximum NBHT coefficient was measured to be approximately $400kW/m^2k$ with APS $67{\mu}m$ and $296{\mu}m$ coating thicknesses. This value is approximately eight times higher than that of a plain Cu surface. The maximum CHF observed was $2.1MW/m^2$ at APS $67{\mu}m$ and $428{\mu}m$ coating thicknesses, which is approximately double the CHF of a plain Cu surface. The enhancement of NBHT and CHF appeared to increase as the particle size increased in the tested range. However, two larger particle sizes ($25{\mu}m$ and $67{\mu}m$) showed a similar level of enhancement.

LS-MOCVD OF BARIUM STRONTIUM TITANATE THIN FILMS USING NOVEL PRECURSORS

  • Kwon, Hyun-Goo;Oh, Young-Woo;Park, Jung-Woo;Lee, Young-Kuk;Kim, Chang-Gyoun;Kim, Do-Jin;Kim, Yunsoo
    • Proceedings of the Korea Crystallographic Association Conference
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    • 2002.11a
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    • pp.19-19
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    • 2002
  • Perovskite-type titanate dielectrics have attracted much attention in memory devices such as DRAMs or FeRAMs due to their high dielectric constants. However, low volatility of the Ba, Sr, Pb or Zr precursors with only thd ligands has limitations in obtaining high quality thin films by liquid source metal organic chemical vapor deposition (LS-MOCVD) processes. To improve the volatility of these precursors, many attempts have been made such as adding polyether ligands to satisfy the coordinative saturation. We report the synthesis of new precursors Ba(thd)₂(tmeea) and Sr(thd)₂(tmeea), where tmeea = tris[2-(2-methoxyethoxy)ethyl]amino, and LS-MOCVD of barium strontium titanate (BSTO) thin films using these precursors. Due to increased basicity of amines compared with ethers, it is expected that the nitrogen-donor ligand will make a strong bond to a metal than an analogous oxygen-donor ligand, consequently improving the volatility and thermal behavior of these precursors. Thin films of BSTO were grown on Pt(111)/SiO₂/Si(100) substrates by LS-MOCVD using a cocktail source consisting of the conventional Ti precursor Ti(thd)₂(O/sup i/Pr), and these new Ba and Sr precursors. As-grown films were characterized by XPS, SEM, XRD, XRF, and C-V and I-V measurements. BSTO films grown at 420℃ were stoichiometric barium strontium titanate with very smooth surface morphology and their dielectric constants were found to be as targe as 450. Dependence of the composition, microstructure and the electrical properties of the BSTO films on the growth temperature, annealing temperature, working pressure, and the composition of the cocktail source will be discussed.

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Color Developing Capacity of Plasma-treated Water as a Source of Nitrite for Meat Curing

  • Jung, Samooel;Kim, Hyun Joo;Park, Sanghoo;Yong, Hae In;Choe, Jun Ho;Jeon, Hee-Joon;Choe, Wonho;Jo, Cheorun
    • Food Science of Animal Resources
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    • v.35 no.5
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    • pp.703-706
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    • 2015
  • The interaction of plasma with liquid generates nitrogen species including nitrite (NO2). Therefore, the color developing capacity of plasma-treated water (PTW) as a nitrite source for meat curing was investigated in this study. PTW, which is generated by surface dielectric barrier discharge in air, and the increase of plasma treatment time resulted in increase of nitrite concentration in PTW. The PTW used in this study contains 46 ppm nitrite after plasma treatment for 30 min. To evaluate the effect of PTW on the cured meat color, meat batters were prepared under three different conditions (control, non-cured meat batter; PTW, meat batter cured with PTW; Sodium nitrite, meat batter cured with sodium nitrite). The meat batters were vacuum-packaged and cooked in a water-bath at 80℃ for 30 min. The typical color of cured meat developed in cooked meat batter treated with sodium nitrite or PTW. The lightness (L*) and yellowness (b*) values were similar in all conditions, whereas, the redness (a*) values of cooked meat batter with PTW and sodium nitrite (p<0.05) were significantly higher than the control. These data indicate that PTW can be used as a nitrite source in the curing process of meat without addition of other nitrite sources.

Effect of Curvature Dependency of Surface Tension on the Result of Pore-Volume Distribution Analysis (동공부피 분포의 계산결과에 미치는 표면장력의 곡률 의존도 효과)

  • Cho Chang-Hyun;Ahn Woon-Sun;Chang Seihun
    • Journal of the Korean Chemical Society
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    • v.16 no.6
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    • pp.341-348
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    • 1972
  • The significance of the curvature dependency correction of surface tension is studied in calculating the pore volume distribution of porous adsorbent from nitrogen adsorption isotherm. That is, Kelvin radii are calculated with curvature dependent surface tension values calculated by Chang et al, and then with these Kelvin radii, pore volume distributions of three porous adsorbents, silica alumina (steam deactivated), silica gel (Davidson 59), and silica gel (Mallinc-krodt Standard Luminescent), are calculated. The results are compared with those obtained by the previous method in which surface tension is taken as constant and also with the others. obtained by the modelless method proposed by Brunauer et al. The maximum point of the distribution curve shift to the larger pore radius, when the curvature dependency is considered. Furthermore, the relative pressure at which capillary condensation commences is by far the lower than that accepted previously. This effect becomes significant as the pore radius approaches to the micropore range.

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Structures and components of pulsed DC-plasma-nitrided layers of an austenitic stainless steel (오스테나이트 스테인리스 강의 펄스 직류 플라즈마 질화처리층 조직 및 성분)

  • 박정렬;국정한
    • Journal of the Korean Vacuum Society
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    • v.5 no.4
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    • pp.377-386
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    • 1996
  • Austenitic stainless steel type 304L has been nitrided under the low pressure of high nitrogen environment for 5 hours by the square-wave-pulse-d.c. plasma as a function of temperature 400~$600^{\circ}C$ and of pulsation. At the temperature range lower than $500^{\circ}C$ and at the relatively high ratio of pulse duration to pulse period, nonstoichiometric stainless steel nitride has been developed in the form of a thin layer which has many cracks. At the temperature range higher than $500^{\circ}C$, with the increasing temperature or with the increasing ratio of the pulse duration to pulse period up to 50s/100s, the nitrided layer was composed mainly of CrN and Fe4N phases and became thick, uniform, columnar and nearly crack-free. The nitrided layer at $500^{\circ}C$ was mixed with the low-temperature layer and the high temperature layer and was very brittle.

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Analysis of the Influence of CO2 Capture on the Performance of IGCC Plants (가스화 복합화력발전 플랜트에서 CO2제거가 성능에 미치는 영향 해석)

  • Cha, Kyu-Sang;Kim, Young-Sik;Lee, Jong-Jun;Kim, Tong-Seop;Sohn, Jeong-L.;Joo, Yong-Jin
    • The KSFM Journal of Fluid Machinery
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    • v.13 no.1
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    • pp.9-16
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    • 2010
  • In the power generation industry, various efforts are needed to cope with tightening regulation on carbon dioxide emission. Integrated gasification combined cycle (IGCC) is a relatively environmentally friendly power generation method using coal. Moreover, pre-combustion $CO_2$ capture is possible in the IGCC system. Therefore, much effort is being made to develop advanced IGCC systems. However, removal of $CO_2$ prior to the gas turbine may affect the system performance and operation because the fuel flow, which is supplied to the gas turbine, is reduced in comparison with normal IGCC plants. This study predicts, through a parametric analysis, system performances of both an IGCC plant using normal syngas and a plant with $CO_2$ capture. Performance characteristics are compared and influence of $CO_2$ capture is discussed. By removing $CO_2$ from the syngas, the heating value of the fuel increases, and thus the required fuel flow to the gas turbine is reduced. The resulting reduction in turbine flow lowers the compressor pressure ratio, which alleviates the compressor surge problem. The performance of the bottoming cycle is not influenced much.