• 제목/요약/키워드: Nitrogen atmosphere

검색결과 540건 처리시간 0.028초

Effects of Transverse Magnetic Field on Laser-produced Carbon Plasma Plume in Nitrogen Atmosphere

  • Nam, Sang-Hwan;Ko, Min-Jung;Lee, Mi-Ae;Park, Hye-Sun;Song, Jae-Kyu;Park, Seung-Min
    • Bulletin of the Korean Chemical Society
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    • 제28권5호
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    • pp.767-771
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    • 2007
  • By adopting a time-resolved optical emission spectrometry, we have investigated the effects of transverse magnetic field on C2 and CN molecules produced by laser ablation of a graphite target in nitrogen atmosphere. We found that the spectroscopic temperatures of both species, obtained via simulation of the optical emission spectra, as well as their emission intensities from the electronically excited states increased significantly in the presence of a magnetic field. The cyclotron radii and frequencies for electrons and ions were estimated to explain the increase in the number of collisions in the laser-produced carbon plasma plume under a magnetic field.

DC 스트레스 시간에 따른 ZnO 세라믹 바리스터의 열화기구 (Degradation Mechanism of ZnO Ceramic Varistors with the Time on the DC Stress Test)

  • 소순진;김영진;소병문;박춘배
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2000년도 하계학술대회 논문집
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    • pp.857-860
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    • 2000
  • The objective of this paper is to demonstrate degradation phenomena through DC degradation tests and predicts degradation phenomena as a function of time from the tests. The ZnO varistor used in this investigation were fabricated by standard ceramic techniques. Especial, these were sintered in nitrogen atmosphere, at 2 h, for $1300^{\circ}C$. The conditions of DC degradation test were 115$\pm$$2^{\circ}C$for 0, 2, 4, and 8 h, respectively. To demonstrate the degradation phenomena of ZnO varistors, Voltagecurrent analyses were performed before and after the degradation test, and frequency analyses were used with the time of the degradation tests. It was found that the degradation occurred in not grain but grain boundary and the degradation behavior of varistors was unsymmetrically degraded with the direction of tests.

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금형온도와 탈지조건이 사출성형에 의한 알루미나 부품 제조에 미치는 영향 (EFfect of Molding Temperature and Debinding Conditions on Fabrication of Alumina Component by Injection Molding)

  • 임형택;임대순
    • 한국세라믹학회지
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    • 제32권5호
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    • pp.559-566
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    • 1995
  • Alumina powder was coated with stearic acid and then mixed with isotactic polypropylene, atactic polypropylene as binders at 15$0^{\circ}C$ for 2 hours. The mixture was then injection molded at various mold temperatures using injection molding machine to investigate the effect of the molding temperature and debinding parameters on the formation of the defects. The molded specimens were debinded in both air and nitrogen atmospheres. Wicking and solvent methods were also used to enhance debinding efficiency. The specimens were prefired at 120$0^{\circ}C$ and then sintered at 150$0^{\circ}C$ for 3 hours. Various defects were formed at mold temoperature of 3$0^{\circ}C$, 6$0^{\circ}C$ and 10$0^{\circ}C$ and any noticeable defect was not formed at 85$^{\circ}C$. The density of green body increased with mold temperature. Debinding in air atmosphere was more effective than in nitrogen atmosphere. Results also proved that wicking and solvent treatments helped minimize the number of defects.

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A Spectroscopic Study on A Plume Produced By Laser Ablation of Graphite in a Nitrogen Atmosphere

  • Wee, Sang-Wook
    • Journal of Photoscience
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    • 제6권3호
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    • pp.141-144
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    • 1999
  • A Spectroscopic study on a pulme produced by a reactive laser pulse irradiates the graphite target in a nitrogen atmosphere, two emission bands of C2(d3IIg longrightarrowa3 IIu, Swan band) and CN(B2$\Sigma$+ longrightarrowX$^2$$\Sigma$+, Violet band ) were observed. By simulation of the optical emissionspectra, spectroscopic temperature of $C_2$ and CN molecules were obtained. The depended of vibrational and rotational temperatures on the laser fluence and distance from the target as well as the pressure dependence of the emission intensities of $C_2$ and CN was examined to elucidate the expansion dynamics of the plume and formation mechanisms of $C_2$and CN molecules.

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Al-20Si-5.5Fe-1.2Mg-0.5Mn 합금분말의 치밀화에 미치는 소결온도와 분위기의 영향 (Effects of Sintering Temperature and Atmosphere on Densification of Hypereutectic Al-Si Alloy Powders)

  • 이재욱;박상빈;양상선;김용진
    • 한국분말재료학회지
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    • 제15권3호
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    • pp.196-203
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    • 2008
  • The densification behavior of Al-20Si-5.5Fe-1.2Mg-0.5Mn powders was investigated through micro-structure analysis of sintered specimens. The specimens sintered in vacuum or in high purity (99.999%) nitrogen showed porous near-surface microstructures. The densification of near-surface part was enhanced by means of ultra-high purity (99.9999%) nitrogen atmosphere. The relationship between slow densification and oxide surfaces of Al alloy powders was discussed. And the effects of Mg addition, nitrogen gas, and humidity on densification were discussed. In addition, the rapid growth of primary Si crystals above the critical temperature was reported.

Thick Film Copper Conductor 의 소결과 소성 분위기 (On Atmospheres for Firing the Thick Film Coper Conductors)

  • 이준
    • 공업화학
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    • 제2권3호
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    • pp.193-198
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    • 1991
  • 후막 구리도체는 귀금속계 도체에 비하여 가격이 저렴하고 전기전도도, 납땜성, 땜납 침식저항, 와이어 본딩성등의 양호한 성질 때문에 매우 중요성을 갖는다. 그러나 우수한 후막 구리도체를 형성하는 것은 구리가 높은 온도에서 쉽게 산화하는 성질로 인해 상당히 복잡하다. 양호한 구리후막을 얻기 위하여 하이브리드 마이크로회로업계는 질소분위기, 반응성분위기 또는 공기분위기를 사용한다. 이 글에서는 후막 구리도체의 소성공정과 세종류의 소성분위기에 대하여 종합적으로 고찰하였다.

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분위기 변화에 따른 반도성 $BaTiO_3$ 전기적 특성 연구 (Studies on the Electrical Properties of Semiconducting $BaTiO_3$ by Changing Sintering Atmosphere)

  • 최기영;한응학;박순자
    • 한국세라믹학회지
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    • 제28권3호
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    • pp.179-188
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    • 1991
  • The semiconducting BaTiO3 ceramics used in this study were sintered in the reducing atomosphere(hydrogen gas) and neutral atmosphere(nitrogen gas), then were heat-treated in air to vary defect concentrations. In this experiment, the correlations between the composition analysis and electrical characteristics of these samples were investigated. When the BaTiO3 ceramics were sintered in N2 atmosphere, it was observed that the Ba contents near the interface were lower than that of the grain center, and these samples showed superior PTCR effects. From analysis of the resistivities of grains and grain boundaries by CIRM(Complex Impedance Resonance Method), it was confirmed that the PTCR effects were caused by the resistivity of grain boundaries. And from measurement of the capacitance at each temperature, the samples sintered in N2 atmosphere show the increase of room temperature resistance and the decrease of capacitance as a result of the increase of the charge depletion layers. This phenomenon agrees well with the cation deficiencies in the analytical results.

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극저온 전력케이블을 액체질소에 대한 방전특성에 관한 연구 (A study on the discharge characteristics of liquid nitrogen using at cryogenic cable)

  • 이현동;주재현;박원주;이광식;이동인
    • 한국조명전기설비학회:학술대회논문집
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    • 한국조명전기설비학회 1996년도 추계학술발표회논문집
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    • pp.125-129
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    • 1996
  • This study describes that electrical breakdown of liquid nitrogen which is influenced with bubble has been investigated as liquid nitrogen is used coolant of high temperature(T/sub c/) superconductivity. In order to investigate breakdown of liquid nitrogen, we formed electrode system of parallel and vertical configuration toward gravitutional direction. In case of changing with electrode configuration of equal electrode and gap spacing in uniform and nonuniform electric field bubble behavior is changed. In result of that, breakdown voltage is changed. Therefore, this study proved that electrode configuration must be formed the smallest existing probability of bubble between two electrodes in order to increase breakdown strength of liquid nitrogen at atmosphere pressure.

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스테인레스강중의 Ti첨가에 따른 질소용해도 측정 (Measurement of Nitrogen Solubility with Ti addition in Stainless Steel)

  • 이영욱
    • 한국산학기술학회논문지
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    • 제10권11호
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    • pp.3043-3047
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    • 2009
  • 액상의 304스테인레스강중의 질소용해도와 질화물 형성관계를 시료채취법을 이용하여 측정하였으며, 이를 열역학적 함수로 규명하였다. 용융 304스테인레스강의 온도가 높을수록 질소용해도는 증가하였으며, 스테인레스강은 1기압의 질소 분위기하에서 0.3wt.% 이상의 Ti 첨가시 Ti계 질화물이 형성되었다. 또한 스테인레스강중에 Ti 첨가로 형성된 질화물은 TiN으로 판명되었다.

송전선용 고질소강선의 비틀림 특성에 미치는 열처리의 영향 (Effect of Heat Treatment on Torsion Characteristics of High Nitrogen Steel Wire for Overhead Conductors)

  • 김정훈;김봉서;박수동;김병걸;이희웅
    • 한국전기전자재료학회논문지
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    • 제17권2호
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    • pp.190-195
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    • 2004
  • The effect of heat treatment on torsion characteristics of high nitrogen steel wire has been studied by torsion test, tensile test, specific resistivity, X-ray diffraction and scanning electron microscopy. After heat treatment at 600∼$700^{\circ}C$, torsion cycle was increased with increasing temperature. Especially, in case of high nitrogen steel wire heat teated at $650^{\circ}C$, torsion cycle was sharply increased. It is estimated that cold worked high nitrogen steel wire started to recrystallize and phase transform at 64$0^{\circ}C$ in air atmosphere.