• Title/Summary/Keyword: Nickel powder

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Toughening of Ni Bonded $Cr_3C_2$ by Mo Particulates (Mo 입자에 의한 Ni 결합 $Cr_3C_2$의 고인성화)

  • 한동빈;장철우;백성기;박병학
    • Journal of the Korean Ceramic Society
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    • v.30 no.6
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    • pp.429-432
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    • 1993
  • Cr3C2 material is characterized by high chemical stability and poor sinterability with low strength [50~150MPa]. In his study, low melting temperature nickel powder was used to improve sinterability as well as strength. In addition, molydenum particles were added to the Ni-bonded Cr3C2 cermet pseudomatrix to increase resistance to fracture. The specimens made by hot-pressing under vacuum and strength was measured by 4-point bending. Indentation cracking and fractographic examination were conducted to study the interaction of the indentation cracks with the reinforcing particles. Toughening mechanisms and failure will be discussed in terms of crack/particle interactions and compared with previous works.

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Ni-P Coated Sn Powders as Anode for Lithium Secondary Batteries

  • Jo, Yong-Nam;Im, Dong-Min;Kim, Jae-Jung;Oh, Seung-M.
    • Journal of the Korean Electrochemical Society
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    • v.10 no.2
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    • pp.88-93
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    • 2007
  • Nano-sized Sn particles were coated with Ni-P layer using an electroless deposition method and their anodic performance was tested for lithium secondary batteries. Uniform coating layers were obtained, of which the thickness was controlled by varying the $Ni^{2+}$ concentration in the plating bath. It was found that the Ni-P layer plays two important roles in improving the anodic performance of Sn powder electrode. First, it prevents the inter-particle aggregation between Sn particles during the charge/discharge process. Second, it provides an electrical conduction pathway to the Sn particles, which allows an electrode fabrication without an addition of conductive carbon. A pseudo-optimized sample showed a good cyclability and high capacity ($>400mAh\;g^{-1}$) even without conductive carbon loading.

Study on the Coordination Polymers of Metal (II) Ions with 2,5-Diamine 1,4-Dihydroxybenzene (2,5-Diamine 1,4-Dihydroxybenzene과 금속 (II) 이온이 만드는 Coordination Polymer에 관하여)

  • Joon Suk Oh;Kyun Ok Cho
    • Journal of the Korean Chemical Society
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    • v.13 no.4
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    • pp.309-312
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    • 1969
  • A series of metal ion-2, 5-diamine 1, 4-dihydroxybenzene polymers containing copper(II), nickel(II) or cobalt (II) have been prepared. The structure was postulated on the basis of elementary analysis of polymers. It was found that copper polymer is most likely the coordination polymers by X-ray powder pattern studies. The thermal stability of the polymers was also studied by a simple method, utilizing a thermogravimetric balance. The order of thermal stabilities is Cu(II) > Ni(II) > Co(II). The polymers start to decompose at a relatively low temperature.

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Analysis of Bonding Interfaces between Cemented Carbide and Stainless Steel made via Hot Vacuum Brazing (고온 진공 브레이징을 이용한 초경합금과 스테인리스강의 접합 계면 특성)

  • Park, D.H.;Hyun, K.H.;Kwon, H.H.
    • Transactions of Materials Processing
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    • v.29 no.6
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    • pp.307-315
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    • 2020
  • The cemented carbide and stainless steel were bonded using a hot-vacuum brazing method to analyze the bonding interface. Since it is suitable for the hot vacuum brazing, nickel metal was used as a binder among the main components of the cemented carbide, and a new cemented carbide material was developed by adjusting the alloy composition. The paste, which is one of the important factors affecting the hot vacuum brazing bonding, was able to improve brazing adhesion by mixing solder as Ni powder and a binder as an organic compound at an appropriate ratio. Division of the stainless steel yielded a dense brazing result. This study elucidated the interfacial characteristics of wear-resistant parts by bonding stainless steel and cemented carbide via hot vacuum brazing.

A study on Manufacture of EMI Composite Powder by the Electroless Ni Plating Method (무전해 니켈도금방법을 이용한 EMI 복합분말제조에 관한 연구)

  • Joung, I.;Yoon, S.R.;Han, S.N.;Na, J.H.;Kim, C.W.
    • Korean Journal of Materials Research
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    • v.8 no.5
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    • pp.444-449
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    • 1998
  • There are various shielding materials that have been considered; the use of a metallic plate or the layering of a conductive material on a plastic surface and the insertion of filler in plastics. All of these methods have shown their merits and weakness. Therefore, many studies have concentrated on developing materials that effectively cut down EMI without increase in weights of housing materials. In these respects, this study has focused on investigations of the shielding effect of materials that have electroless nickel plating on the lamella structured micro particles surface with low specific gravity. When a film of electroless nickel were plated on a micro particle surfaces and then mixed with paint, the electromagnetic shielding effects were measured as 63dB. Although these effects were less than that 90dB of the copper plate, trials in a series of 6 times increased the shielding effect by IOdB and is applicable to wide range of EMI shielding.

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The Effects of Current Density on the Grain Size of Electroplated Thick Film Nickel(Ni) by Using Ni Metal Powder Dissolved Chloride Bath (금속분말 Ni을 용해 한 Chloride Bath로 도금된 니켈후막의 입자크기에 대한 전류밀도 영향)

  • Park, Keun Yung;Uhm, Young Rang;Choi, Sun Ju;Park, Deok-Yong
    • Journal of the Korean Magnetics Society
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    • v.23 no.1
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    • pp.12-17
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    • 2013
  • Nanocrystalline nickel (Ni) tick films were synthesized by direct current electrodeposition at current density from 1 to $30mA/cm^2$ and pH = 4. The basic composition of the bath, which was prepared by dissolving Ni metal particles in HCl, was 0.2M Ni ions. The effects of the current density on the average grain size of Ni deposits were investigated by XRD and SEM techniques. The results showed that the surface roughness was decreased as the saccharin addition was increased up to 2 g/l. The experimental results showed that the increase in the current density had a considerable effect on the average grain size of the Ni deposits. The perpendicular magnetization was raised as the thickness of coating layer was increased.

A Study on the Properties of Hwangto Permeable Block Using Ferro Nickel Slag (페로니켈슬래그를 혼입한 황토투수블럭 물성에 관한 연구)

  • Kim, Soon-Ho
    • Journal of the Korea Institute of Building Construction
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    • v.22 no.6
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    • pp.607-618
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    • 2022
  • This study involves the development of a Hwangto permeable block for rainwater storage tanks. The permeable products that form continuous voids between Hwangto binders and aggregates are fine milled slag powder, which is an industrial by-product generated during the production of Hwangto and iron, and ferro nickel slag. The properties of Hwangto permeable blocks were studied using recycled resource aggregates. The target quality is based on KSF 2394. The Hwangto permeable block for a rainwater storage tank is made of water-permeable material, and the permeability of the Hwangto permeable block itself is 0.1mm/sec or higher, with a physical performance of over 5.0MPa in flexural strength and over 20.0MPa in compressive strength. The physical properties of Hwangto permeable block for rainwater storage tanks were researched and developed. In order to prevent flooding due to heavy rain in summer and the urban heat island phenomenon due to depletion of ground water, continuous pores are formed in the block to secure a permeability function to prevent rainwater from accumulating in the pavement of the floor, and to prevent slippage for comfortable and safe storage.

A study on heavy metal concentration of cosmetics on the market (국내 시판중인 일부 화장품의 중금속 농도에 관한 연구)

  • Lee, Hun;Yoo, Yoo-Jung;Park, Myoung-Hee;Kim, Jung-Ho;Lee, Yong-Hee;Moon, Chan-Seok;Hwang, Yong-Shik;Moon, Deog-Hwan
    • Journal of Preventive Medicine and Public Health
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    • v.31 no.4 s.63
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    • pp.666-679
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    • 1998
  • This study aims at providing the fundamental data on the field of cosmetics by comparing heavy metal concentration in terms of domestic/foreign products, items, companies and colors. This study has determined the concentration of chromium, lead, mangagnese, nickel, copper and vanadium in cosmetics such as moisturizer, concealer, foundation (Ivory-yellow), compact powder (Ivory-yellow), lip colo. (Red, brown), eye shadow (Red, brwon and dark green) and eye liner (Black) manufactured by five domestic cosmetic companies and five foreign cosmetic companies on the market. The samples have been collected in cosmetic stores in Pusan from Dec. lst 1996 to Jan. 3lst 1997. The results are as follows : 1. The heavy metal concentration in cosmetics was $2.420{\mu}g/g$ for chromium, $0.82{\mu}g/g$ for lead, $4.49{\mu}g/g$ for manganese, $1.69{\mu}g/g$for nickel, $0.53{\mu}g/g$ for copper, and $51{\mu}g/g$ for vanadium, respectively. 2. Lead and vanadium concentration were significantly higher in domestic cosmetics than foreign cosmetics(p<0.05). 3. The mean(GM) concentrations of heavy metal were different significantly (p<0.01) when classified with cosmetic items. The highest means shown at eye shadow in $Cr(14.96{\mu}g/g),\;Cu(1.32{\mu}g/g),\;V(1.28{\mu}g/g),\;and\;Ni(8.30{\mu}g/g)$, compact powder in $Pb(2.50{\mu}g/g)$, eye liner in $Mn(90.62{\mu}g/g)$. 4. The mean(GM) concentrations of heavy metal were different significantly (p<0.01) among colored cosmetics. The highest mean concentration of Cr, Ni, Cu and V were dark green-colored cosmetics, that of Mn was black-colored cosmetics, and that of Pb was ivory yellow- colored cosmetics.

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Fabrication of Nano-Sized Complex Oxide Powder from Waste Solution Produced during Shadow Mask Processing by Spray Pyrolysis Process (새도우마스크 제조 공정중 발생되는 폐액으로부터 분무열분해 공정에 의한 복합산화물 나노 분말 제조)

  • Yu Jae-Keun
    • Resources Recycling
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    • v.12 no.6
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    • pp.38-46
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    • 2003
  • In this study, nano-sized Ni-ferrite and $Fe_2$$O_3$+NiO powder was fabricated by spray pyrolysis process in the condition of 1kg/$\textrm{cm}^2$ air pressure using the Fe-Ni complex waste acid solution generated during the manufacturing process of shadow mask. The average particle size of the produced powder was below 100 nm. The effects of the reaction temperature, the concentration of raw material solution and the nozzle tip size on the properties of powder were studied. As the reaction temperature increased from $800 ^{\circ}C$ to $1100^{\circ}C$, the average particle size of the powder increased from 40 nm to 100 nm, the structure of the powder gradually became solid, yet the distribution of the particle size appeared more irregular. Along with the increase of the reaction temperature, the fraction of the Ni-ferrite phase were also on the rise, and the surface area of the powder was greatly reduced. As the concentration of Fe in solution increased from 20g/l to 200g/l, the average particle size of the powder gradually increased from 30 nm to 60 nm, while the distribution of the particle size appeared more irregular. Along with the increase of the concentration of solution, tie fraction of the Ni-ferrite phase was on the rise, and the surface area of the powder was greatly reduced. Along with the increase of the nozzle tip size, the distribution of the particle size appeared more irregular, yet the average particle size of the powder showed no significant change. As the nozzle tip size increased from 1 mm to 2 mm, the fraction of the Ni-ferrite phase showed no significant change, while the surface area of the powder slightly reduced. As the nozzle tip size increased to 3 mm and 5 mm, the fraction of the Ni-ferrite phase gradually reduced, and the surface area of the powder slightly increased.

On the Leakage Safety Analysis of $9\%$ Nickel Type LNG Storage Tank with Thermal Resistance Effects (열저항 효과를 고려한 $9\%$ 니켈강재식 LNG 저장탱크의 누설 안전성에 관한 연구)

  • Kim C.K.;Cho S.H.;Suh H.S.;Hong S.H.;Lee S.R.;Kim Y,G.;Kwon B.K.
    • Journal of the Korean Institute of Gas
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    • v.9 no.1 s.26
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    • pp.1-8
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    • 2005
  • In this study, the FE analysis has been presented for the leakage safety of $9\%$ nickel type LNG storage tank based on the thermal resistance effects between insulation panels, comer protection and prestressed concrete(PC) structures. The FEM calculated results show that the leakage safety of fiber glass blanket, perlite powder and cellular glass insulators does not guarantee any more due to a strength failure of the insulation structure. But the corner protection and PC structure of outer tank may delay or sustain the leaked LNG of 10 days even though the inner tank and insulation structure are simultaneously failed. This means that $9\%$ nickel steel type LNG storage tank may be safe because of a high strength of the corner protection and outer tank structures.

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