• Title/Summary/Keyword: Neutral treatment

Search Result 550, Processing Time 0.024 seconds

Chemical Characterization of Neutral Extracts Prepared by Treating Pinus radiata Bark with Sodium Bicarbonate

  • MUN, Ji Sun;KIM, Hwan Chul;MUN, Sung Phil
    • Journal of the Korean Wood Science and Technology
    • /
    • v.48 no.6
    • /
    • pp.878-887
    • /
    • 2020
  • A neutral extract (NE), that is soluble in cold water and has excellent antioxidant activity, from Pinus radiata pine bark was prepared by sodium bicarbonate treatment, and its chemical characteristics were investigated. NE was prepared by treating P. radiata bark with 0.8% NaHCO3 aqueous solution with a 5 : 1 liquor-to-bark ratio at boiling temperature for 1 h, resulting in 44% yield and final pH of 6.66. The yield of NE was 11% higher than that of the hot water extract (HWE) due to the increase in the solubility of polyphenols, the main component in the bark, by NaHCO3 treatment. NE was characterized through FT-IR, NMR, and MALDI TOF MS analyses. The results indicated that NE is mostly composed of proanthocyanidins (PAs) consisting of procyanidin (PC) units. The acetylated neutral extract (Ac-NE) had weight average molecular weight (${\bar{M}}w$) of 5,300 Da. The Ac-NE had wide molecular weight distribution and its polydispersity (${\bar{M}}w/{\bar{M}}n$) was 6 times higher than that of pure PA. The antioxidant activity of NE was determined by 2-diphenyl-1-picrylhydrazyl (DPPH) free radical scavenging assay and showed that NE had comparable antioxidant activity with pure PA.

Studies on Silk Contraction Treated with Neutral Salts (중성염에 의한 견사의 수축작용)

  • Lee, Gwang-Gil;Lee, Yong-U;Nam, Jung-Hui
    • Journal of Sericultural and Entomological Science
    • /
    • v.39 no.1
    • /
    • pp.44-55
    • /
    • 1997
  • This study was carried out to find out the relationship between qualities and contraction phenomenon of silk fibers by treatment of concentrated neutral salts. The contraction effects of silk fibers showed the critical point on the treatment conditions of concentration, temperature and time, among three kinds of neutral salts such as calcium nitrate, calcium chloride and lithium bromide. But, The silk fibers, pretreated with bromide and/or formaldehyde, did not show the contraction upon treating with calcium nitrate. This indicates that tyrosine and serine can be correlated with the contraction reaction because of coupling these amino acids with bromide and formaldehyde. In conclusion, a mechanism for the contraction of silk fiber with highly concentrated calcium nitrate solution is supposed as follows. At the initial stage of ration, the water was penetrated into the amorphous regions and fibers swollen, therefore, the contraction took place mainly in amorphous regions, which have plenty of functional groups with hydroxyl residues. Then, as the calcium nitrate is penetrated into the microfibril, the gydrogen bonds of tyrosine and serine residues and broken and crystalline regions are more and more influenced by increasing concentration of calcium nitrate solution. Microgibrils of crystalline regions become entangled, contracted to linear direction and rearranged to form new stable hydrogen bonds.

  • PDF

Comparison between PY and YP on Bleach Efficiency of White Ledger according to Deinking Method (탈묵방법에 따른 백상폐지의 표백효율에 미치는 PY와 YP간의 비교)

  • 백기현;안병준
    • Journal of Korea Technical Association of The Pulp and Paper Industry
    • /
    • v.33 no.3
    • /
    • pp.37-43
    • /
    • 2001
  • The bleach efficiency between PY and YP bleaching of pulps, which were deinked in neutral (cellulase) and alkaline (NaOH, NaOH/${Na_2}{SiO_3}$) ranges, and were treated on kneader, was compared in this study. The brightness of pulps (84.8~88.4% ISO) which were deinked in alkaline or neutral ranges increased up to 88.4%~88.8% ISO after PY or YP bleaching. There was no difference in the brightness between PY and YP bleaching. And the dirt count of bleached pulps was similar each other at the range of 17~38 ppm. The tensile index of bleached pulps was slightly higher in PY bleaching than those in YP bleaching. While with the treatment of kneading, the brightness and dirt count decreased remarkably compared to those of no-kneading. However, the sharp difference in the brightnesses or in dirt count of bleached pulps decreased after bleaching. The brightness of bleached pulps at YP stages was only numberically higher than those at PY stages without regard to the treatment of kneading. Therefore, in the case of the neutral deinkiing process, the conversion of PY bleaching stages to YP bleaching stages was profitable to water loop system, and was harmless in the aspect of the bleach efficiency.

  • PDF

Effects of pH and Plating Bath Temperature on Formation of Eco-Friendly Electroless Ni-P Plating Film on Aluminum (알루미늄 위 친환경적 무전해 Ni-P 도금막 형성에 pH와 도금조 온도가 미치는 영향)

  • Gee, Hyun-Bae;Bin, Jung-Su;Lee, Youn-Seoung;Rha, Sa-Kyun
    • Korean Journal of Materials Research
    • /
    • v.32 no.9
    • /
    • pp.361-368
    • /
    • 2022
  • The overall process, from the pre-treatment of aluminum substrates to the eco-friendly neutral electroless Ni-P plating process, was observed, compared, and analysed. To remove the surface oxide layer on the aluminum substrate and aid Ni-P plating, a zincation process was carried out. After the second zincation treatment, it was confirmed that a mostly uniform Zn layer was formed and the surface oxide of aluminum was also removed. The Ni-P electroless plating films were formed on the secondary zincated aluminum substrate using electroless plating solutions of pH 4.5 and neutral pH 7.0, respectively, while changing the plating bath temperature. When a neutral pH7.0 electroless solution was used, the Ni-P plating layer was uniformly formed even at the plating bath temperature of 50 ℃, and the plating speed was remarkably increased as the bath temperature was increased. On the other hand, when a pH 4.5 Ni-P electroless solution was used, a Ni-P plating film was not formed at a plating bath temperature of 50 ℃, and the plating speed was very slow compared to pH 7.0, although plating speed increased with increasing bath temperature. In the P contents, the P concentration of the neutral pH 7.0 Ni-P electroless plating layer was reduced by ~ 42.3 % compared to pH 4.5. Structurally, all of the Ni-P electroless plating layers formed in the pH 4.5 solution and the neutral (pH 7.0) solution had an amorphous crystal structure, as a Ni-P compound, regardless of the plating bath temperature.

Design Optimization on Wastewater Treatment Pump of Satisfaction for High Head and Low Flow Rate (고양정 및 저유량을 만족하는 폐수처리용 펌프 설계 최적화)

  • KIM, SUNG;KIM, JIN-HYUK
    • Journal of Hydrogen and New Energy
    • /
    • v.33 no.5
    • /
    • pp.583-590
    • /
    • 2022
  • In this paper, the performance characteristics of the 2 vane pump for wastewater treatment were investigated using response surface method(RSM) with commercial computation fluid dynamics(CFD) software. Design variables of wastewater treatment pump were defined with the meridional plane of the 2 vane pump impeller. The objective functions were defined as the total head and the efficiency at the design flow rate. The hydraulic performance of optimum model was verified by numerical analysis and the reliability of the model was retained by comparison of numerical analysis and comparative analysis with the reference model.

Single-dose Intramuscular Toxicity of Neutral Natured Blood Stasis Pharmacopuncture in Sprague-Dawley Rats

  • Yeo, In Ho;Lee, Eun Yong
    • Journal of Pharmacopuncture
    • /
    • v.17 no.2
    • /
    • pp.41-45
    • /
    • 2014
  • Objectives: This study was performed to analyze the single-dose toxicity of neutral natured blood stasis pharmacopuncture extracts. Methods: All experiments were conducted at Biotoxtech, an institution authorized to perform non-clinical studies, under the regulations of Good Laboratory Practice (GLP). Sprague-Dawley rats were chosen for the pilot study. Doses of neutral natured blood stasis pharmacopuncture extracts, 0.1, 0.5 and 1.0 mL, were administered to the experimental group, and the same doses of normal saline solution were administered to the control group. This study was conducted under the approval of the Institutional Animal Ethics Committee. Results: In all 4 groups, no deaths occurred, and the neutral natured blood stasis pharmacopuncture extracts administered by intramuscular (IM) injection was over 1.0 mL/animal. No significant changes in the body weights between the control group and the experimental group were observed. To check for abnormalities in organs and tissues, we used microscopy to examine representative histological sections of each specified organ; the results showed no significant differences in any organs or tissues. Conclusion: The above findings suggest that treatment with neutral natured blood stasis pharmacopuncture extracts is relatively safe. Further studies on this subject should be conducted to yield more concrete evidence.

Changes on the Components of Free Polysaccharide from Cell Wall of Persimmon Fruit by Treatments of Cell Wall Degrading Enzymes (세포벽분해효소의 처리에 따른 감과실의 세포벽 유리 다당류의 변화)

  • 신승렬;김미현
    • Food Science and Preservation
    • /
    • v.2 no.1
    • /
    • pp.173-183
    • /
    • 1995
  • This paper was carried out to investigate changes in chromatograms of polysacctatides and soluble pectins on Sephadex G-50 and non-cellulosic neutral sugars of polysaccharides isolated from cell wall of persimmon fruits treated with polygalacturonase and $\beta$-galactosidase in vitro. The chromatogram pattern of soluble pectins extracted from cell wall treated with $\beta$-galactosidase on Sephacryl S-500 column were similar to those of untreatment, but contents of soluble pectins treated with $\beta$-galactosidase were different from those of untreatment. The patterns of chromatograms In soluble pectins extracted from cell wall treated with polygalacturonase were more complex and lower molecular polymer than those of other cell wall-degrading enzyme treatments. Non-cellulosic neutral sugar of polysaccharides in fraction I of soluble material treated with polygalacturonase was rhamnose, those in fraction II were similar to those in fraction III and contents of arabinose, xylose and glucose were higher than contents of other non-cellulosic neutral sugars. Non-cellulosic neutral sugars of polysaccharides in fraction I in soluble material by $\beta$-galactosidase treatment were rhamnose, arabinose, galactose and mannose. Content of glucose of polysaccharides in fraction II was higher than that in fraction I . Non-cellulosic neutral sugars treated with mixed enzyme were rhamnose, fucose, arabinose, xylose, mannose, galactose and glucose. Compositions of non-cellulosic neutral sugars of polysaccharides in fraction I were similar to those in fraction II and III.

  • PDF

The Effects of Nitrite Treatment on the Lipid Composition, Fatty Acid Composition, and Susceptibility to Oxidation of Pork Biceps Femoris Muscle

  • Han, S.K.;Yamauchi, K.
    • Asian-Australasian Journal of Animal Sciences
    • /
    • v.13 no.12
    • /
    • pp.1764-1769
    • /
    • 2000
  • The purpose of this experiment was to investigate the antioxidant effect of nitrite on total, neutral, and polar lipids and fatty acid composition in laboratory-cooked ground pork. Muscle samples (Biceps femoris) were analyzed using Iatroscan, gas chromatography, phosphorus content, and TBARS value. The total and neutral lipid contents of muscle were higher in nitrite-untreated meat (0 ppm) than in nitrite-treated meat (100 ppm) but the reverse was observed for polar lipid contents. The results for neutral lipids showed a similar trend when compared with total lipids. Polyunsaturated fatty acids contents of total, neutral and polar lipid in 100 ppm treated meat were higher than that of 0 ppm. The phosphorus content was higher in 100 ppm meat than in 0 ppm but the reverse was observed for TBARS value. These results showed that the addition of 100 ppm nitrite to ground pork resulted in a remarkable antioxidant effect during refrigeration storage.

NUTRITIVE EVALUATION OF SAGO FIBRE

  • Yadav, D.P.;Mahyuddin, M.
    • Asian-Australasian Journal of Animal Sciences
    • /
    • v.4 no.2
    • /
    • pp.177-182
    • /
    • 1991
  • Nutrient evaluation of sago fibre showed that the fibre has potential and could be utilized as feed for ruminants. However, as a source of nutrients, it has limitations arising from low intake, digestibility, crude protein and minerals content. The present study showed that the sago fibre is low in crude protein (3.3%) and high in neutral detergent fibre (72.5%) and acid detergent lignin (25.8%) contents. Treatment of sago fibre with urea increased the crude protein content from 3.3 to 16.7%. Both urea and sodium hydroxide treatment decreased the neutral detergent fibre level from 72.5 to 59 and 56.5%, respectively. Rumen degradation of sago fibre by nylon bag showed that both urea and sodium hydroxide treatments increased dry matter and organic matter disappearance of the fibre significantly. In vivo digestibility of 2% urea treated sago fibre was 47.5% and intake of the fibre was 1.57% of body weight of the lamb.

Quantitative Analysis of Acylcarnitines and Amino Acids Using ESI-MS/MS (ESI-MS/MS를 이용한 아실카르니틴과 아미노산의 정량분석)

  • Kim, Hohyun;Han, Sang-Beom;Yoon, Hye-Ran
    • Analytical Science and Technology
    • /
    • v.14 no.5
    • /
    • pp.384-391
    • /
    • 2001
  • In this study, a new quantitative analytical method has been developed for the rapid determination of acylcarnitines and amino acids in human blood using electrospray ionization / tandem mass spectrometry (ESI-MS/MS). Acylarmitines and amino acids were analyzed by tandem mass spectrometry after conversion to their butylesters through treatment with 3N butanolic hydrogen chloride. Acylcrnitines were analyzed using precursor 85 ion scan and alanine, valine, leucine/isoleucine, methionine, phenylalanine, tyrosine, aspartic acid and glutamic acid were analyzed using neutral loss 102 scan, ornitine and citrulline were analyzed neutral loss 119 scan, glycine was analyzed using neutral loss 56 scan, arginine was analyzed using neutral loss 161 scan and argininosuccinic acid was analyzed product ion 459 scan. This method reduced sample preparation time compared to that with conventional amino acid analyzer and liquid chromatography, with high sensitivity and good reproducibility.

  • PDF