• Journal of the Korean Magnetics Society
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• v.12 no.3
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• pp.88-93
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• 2002

Rapidly solidified NdFeB powders were mixed with fine powders of pure metal elements before CA-press employed to obtain a fully dense isotropic precursor. Subsequently, the precursor was deformed by CA-deformation to obtain an anisotropic magnet. The CA-deformed anisotropic NdFeB magnets with 0.3 wt.% Zn or Sn exhibited the coercivities about 80% higher (11.4. and 11.2 kOe, respectively) than that (6.4 kOe) of the additive-free magnet.

• Proceedings of the KIEE Conference
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• 1991.07a
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• pp.43-46
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• 1991

Nd-Fe-B Permanent Magnet, which is recently more used, has some advantages in comparison with other permanent magnet. However, for the Nd-Fe-B has higher RTC(reversible temperature coefficient), property of the Nd-Fe-B magnet is changed by temperature rise. In this paper temperature rise of a disc type motor is calculated using a heat source network method.

• Proceedings of the KIEE Conference
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• 2001.04a
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• pp.404-406
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• 2001

This paper is about designing the magnetizing system which is used for magnetizing the NdFeB magnet in a squirrel cage rotor. It propose the shape of the magnetizing yoke, the number of coil turn and the capacitor discharging circuit parameter. In case of magnetizing the NdFeB magnet assembled with a squirrel cage rotor, the eddy current which is produced during magnetizing becomes a disturbance in magnetizing NdFeB magnet. Hence in this paper, we try to design optimized magnetizing system with eddy current considered by FEM(Finite Element Method).

• Resources Recycling
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• v.22 no.4
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• pp.55-61
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• 2013

In this study, eco efficiency analysis is performed to analyze Neodymium (Nd) containing permanent magnet recycling process. Life cycle assessment (LCA) and life cycle costing (LCC) are used to apply eco efficiency analysis. In the environmental aspects, global warming potential (GWP) of 1kg permanent magnet is 1.25E + 00 kg $CO_2$ eq. and abiotic resource depletion potential (ADP) is 1.10E - 02 Sb eq. This recycling process costs about 2130 KWR. Environmental efficiency of GWP is at 6.43 and ADP is at 5.32 when compared with vigin metal. Economic efficiency is at 6.74. This study confirms that Nd containing permanent magnet recycling process is sustainable system because of environmental and economical improvement.

• Resources Recycling
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• v.27 no.1
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• pp.38-44
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• 2018

A large amount of Nd-Fe-B magnet scraps are generated during magnet manufacture process. In this study, selective chlorination of the rare earth elements by hydrogen chloride gas which obtained from the pyrolysis of polyvinyl chloride (PVC) was investigated. In thermogravimetric analysis, drastic weight loss was occurred at about 500 K and 710 K. At the isothermal experiments, the weight loss reaches about 30% above 673 K. XRD patterns characterized that after each experiments, ${\alpha}$-Fe, Nd oxychloride, Nd chloride, and Fe chlorides were formed, and the leaching residues remain only ${\alpha}$-Fe. The yields of Nd, Dy, and Fe for the isothermal experiment were increased with temperature and peaked at 873 K. As PVC ratio increased, the yields of Nd, Dy and Fe were also increased.

• Journal of Magnetics
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• v.4 no.3
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• pp.73-75
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• 1999

By appliying an slternate pulsed magnetic field -generated by using a sequential ignition circuit and a magnet exciting circuit- with peak value of about 10 T to the rod type Nd based magnet Nd2Fe12.7Cr1.3B with length of 5 mm and diameter of 3.6 mm, the basic magnetic properties such as saturation magnetization, residual magnetization, coercivity, maximum energy products, magnetic anisotropy and anisotropic field are investigated with obtaining the major and minor J-H loops of the magnet. The increase in coercivity due to eddy currents in ac measurement of coercivity is calculated considering eddy current loss by analyzing a wave of generating magnetic field. The average coercivity calculated for the magnet is about 12.2 kOe, anisotropy magnetic field and anisotropic constant are measured as 60 kOe 2.43 Mj/$m^3$, respectively.

• Journal of the Korean Magnetics Society
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• v.22 no.2
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• pp.58-65
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• 2012

Since Nd-Fe-B magnet was first synthesized in 1983, many new applications have emerged in the past two decades. With regard to motor market, it will expand because of strong energy saving requirements from the automobile and electric application markets. Especially, permanent magnet motors for hybrid and electric vehicles are drawing great attention and the usage of Nd-Fe-B magnets will increase all the more hereafter. There is, however, a serious problem as motors in such eco-friendly cars are said to operate in high temperatures of about $200^{\circ}C$. Nd-Fe-B magnet has a drawback of dramatically decreasing coercive force with the rise of temperature. In order to improve this aspect. the best way is to add dysprosium (Dy) into the magnet. So, Dy has become an essential element for Nd-Fe-B high-performance magnet as it helps to maintain coercive force even at high temperatures. On the other hand, the rare earth resources in the earth crust are eccentrically-located and its majority is produced in China. There is a need to reduce its usage as, especially compared to light rare earth elements as neodymium (Nd) and samarium (Sm), heavy rare earth elements including Dy are unevenly distributed to a dramatic degree, their output low, and their prices are about 10 times that of Nd. The present article includes a summary of the trend in research and development of motors and permanent magnets to solve rare-earth resources problem.

• Journal of Magnetics
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• v.9 no.4
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• pp.109-112
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• 2004

The HDDR (Hydrogenation-Disproportionation-Desorption-Recombination) process is a special method to produce anisotropic NdFeB powders for bonded magnet. The effect of the modified HDDR process on magnetic properties of $Nd_2Fe_{14}B$-based magnet with several composition $Nd_{11.2}Fe_{66.5-x}Co_{15.4}B_{6,8}Zr{0.1}Ga_x(x=0{\sim}1.0)$ and that of microelement Ga, disproportional temperature and annealing temperature on $_jH_c$, grain size were investigated in order to produce anisotropic powder with high magnetic properties. It was found that modified HDDR process is very effective to enhance magnetic properties and to fine grain size. The addition of Ga could change disproportionation character remarkably of the alloy and could improve magnetic properties of magnet powder. Increasing annealing temperature induces significant grain growth. And grain size produced by modified HDDR process is significantly smaller than those produced by conventional HDDR process.

• Journal of Powder Materials
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• v.20 no.3
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• pp.169-173
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• 2013

High-coercive (Nd,Dy)-Fe-B magnets were fabricated via dysprosium coating on Nd-Fe-B powder. The sputtering coating process of Nd-Fe-B powder yielded samples with densities greater than 98%. $(Nd,Dy)_2Fe_{14}B$ phases may have effectively penetrated into the boundaries between neighboring $Nd_2Fe_{14}B$ grains during the sputtering coating process, thereby forming a $(Nd,Dy)_2Fe_{14}B$ phase at the grain boundary. The maximum thickness of the Dy shell was approximately 70 nm. The maximum coercivity of the Dy sputter coated samples(sintered samples) increased from 1162.42 to 2020.70 kA/m. The microstructures of the $(Nd,Dy)_2Fe_{14}B$ phases were effectively controlled, resulting in improved magnetic properties. The increase in coercivity of the Nd-Fe-B sintered magnet is discussed from a microstructural point of view.

• Journal of Magnetics
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• v.20 no.1
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• pp.21-25
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• 2015

Fine Nd-Fe-B-type particles were prepared by ball milling of different types of Nd-Fe-B precursor materials, such as die-upset magnet, HDDR-treated material, and sintered magnets. Coercivity dependence on the grain and particle size of the powder was investigated. Coercivity of the milled particles was reduced as the particle size decreased, and the extent of coercivity loss was dependent upon the precursor material. Coercivity loss in the finely milled particles was attributed to the surface oxidation. The extent of coercivity loss in the fine particles was closely linked to grain size of the precursor materials. Coercivity loss was more profound for the fine particles with larger grain size. Contrary to the fine particles from the sintered magnets with larger grain size the fine particles (~10 um) from the die-upset magnet and HDDR-treated material with much finer grain size still retained high coercivity (> 10 kOe for die-upset magnet, > 4 kOe for HDDR-treated material).