• 제목/요약/키워드: Nanopowder

검색결과 229건 처리시간 0.024초

Enhanced Visible Light Activity and Stability of TiO2 Nanopowder by co-doped with Mo and N

  • Hu, Shaozheng;Li, Fayun;Fan, Zhiping
    • Bulletin of the Korean Chemical Society
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    • 제33권4호
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    • pp.1269-1274
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    • 2012
  • A visible light responsive N, Mo co-doped $TiO_2$ were prepared by sol-gel method. X-ray diffraction, TEM, $N_2$ adsorption, UV-vis spectroscopy, photoluminescence, and X-ray photoelectron spectroscopy were used to characterize the prepared $TiO_2$ samples. Doping restrained the phase transformation from anatase to rutile and reduced the particle sizes. The band gap was much narrowed after N, Mo co-doping. The photocatalytic activities were tested in the degradation of an aqueous solution of a reactive dyestuff, methylene blue, under visible light. The photocatalytic activities of doped $TiO_2$ were much higher than that of neat $TiO_2$. The photocatalytic stability of N, Mo co-doped $TiO_2$ was much better than that of N doped $TiO_2$.

나노분말이 분산된 기능성 코팅액 제조를 위한 대용량 교반기의 유동해석 (Computational Flow Analysis of a Large Scale Mixer for Nanopowder Dispersion in Coating Liquid)

  • 김동주;김경진
    • 반도체디스플레이기술학회지
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    • 제12권3호
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    • pp.1-6
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    • 2013
  • In many technical fields including electronics and display manufacturing processes, properties of coating liquids could be greatly enhanced by adding nanopowders and it requires efficient mixing techniques to achieve uniform dispersion of nanoparticles in liquids. This paper presents the three-dimensional CFD simulations on the flowfields of a highly viscous liquid in the large scale industrial mixer of impeller type. The effects of several important design and operation parameters such as impeller geometry, rotational speed, and degree of liquid viscosity are investigated to appreciate the mixing performance by examining the computational results for flow pattern of rotationally stirred liquid of high viscosity in the mixer.

Solid State Sintering of Micrometric and Nanometric WC-Co Powders

  • Escobar, J.A.;Campo, F.A.;Serrano, C.H.
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.350-351
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    • 2006
  • A solid stage sinterizacion model of the WC-Co is applied on this work. These results are compaired with the experimental data obtained for nanometric and micrometric sinter powder in an electric furnace and micrometric in a plasma reactor (using Abnormal Glow Discharge AGD). The correlations obtained allow the prediction of the sintering behavior in AGD for nanometric powder. The activation of the solid state sintering is shown with the decraease of the WC size and the use of AGD

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Preparation and Sintering Behavior of Fe Nanopowders Produced by Plasma Arc Discharge Process

  • Choi, Chul-Jin;Yu, Ji-Hun
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.284-285
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    • 2006
  • The nano-sized Fe powders were prepared by plasma arc discharge process using pure Fe rod. The microstructure and the sintering behavior of the prepared nanopowders were evaluated. The prepared Fe nanopowders had nearly spherical shapes and consisted of metallic core and oxide shell structures. The higher volume shrinkage at low sintering temperature was observed due to the reduction of surface oxide. The nanopowders showed 6 times higher densification rate and more significant isotropic shrinkage behavior than those of micron sized Fe powders.

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Effect of Electrical Parameters and Surrounding Gas on the Electroexplosive Tungsten Nanopowders Characteristics

  • Kwon, Young-Soon;Kim, Jin-Chun;Ilyin, Alexander P.;Nazarenko, Olga B.;Tikhonov, Dmitry V.
    • 한국분말재료학회지
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    • 제19권1호
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    • pp.49-54
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    • 2012
  • Tungsten nanopowders were produced by the method of wires electrical explosion in the different gases. The study of phase and dispersed composition of the powders was carried out. The influence of electrical parameters such as the value of energy input in wire and the arc stage of the explosion was discussed. The factors that make for decreasing the particles size are the lower pressure of surrounding gas and the use of addition of chemically reactive gas.

Electroexplosive Technology of Nanopowders Production: Current Status and Future Prospects

  • Kwon, Young-Soon;Kim, Jin-Chun;Ilyin, Alexander P.;Nazarenko, Olga B.;Tikhonov, Dmitry V.
    • 한국분말재료학회지
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    • 제19권1호
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    • pp.40-48
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    • 2012
  • The current situation of the nanopowders production technology based on the process of electrical explosion of wires is described. The advantages and disadvantages of the electroexplosive technology are indicated. The results of studies characterizing the effect of the electrical explosion conditions on the nanopowders properties are presented, including latest results: conditions of nanopowders passivation, conditions of nanopowders production having narrow size distribution, the methods of nanopowders diagnostic and standartization. In addition, the application and area of future research on this technology are proposed.

다양한 변화가 가능한 그래핀 복합체 제작 및 응용 (Fabrication and Application of Graphene Composite with Various Modifications)

  • 박종성;김동수;김지관
    • 센서학회지
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    • 제29권3호
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    • pp.201-204
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    • 2020
  • In this study, we fabricated and evaluated graphene composite based 3D scaffolds and planar films. The hybrid composite was prepared by mixing a calculated amount of graphene nanopowder and polydimethylsiloxane in tetrahydrofuran solution. The hybrid composite is easy to manufacture into various forms using direct printing technology or a pressing method. A 3D scaffold structure was prepared at ambient temperature with a flow rate of 240 mm/min. The nozzle pressure was maintained at 350 kPa by adjusting the viscosity of the composite material. The planar film was prepared at different thicknesses using a roll-to-roll equipment. The prepared hybrid nanocomposites were evaluated to investigate their electrical properties according to temperature and mechanical deformation. The obtained results were consistent with each other. Therefore, it can be used effectively as sensors through shape definition.

액상환원법에 의한 저온 열처리용 Ag 나노분말의 합성 (Synthesis of Ag Nanopowder for Low Temperature Heat Treatment Prepared by Liquid Phase Reduction Method)

  • 이종국;최남규;송대성;양권승;서동석
    • 열처리공학회지
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    • 제18권4호
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    • pp.242-246
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    • 2005
  • Silver nanoparticles were synthesized by liquid phase reduction method from aqueous silver nitrate solution and borohybride as a reduction agent. The morphology, particle size and shape were influenced by the reaction conditions such as the concentration of $AgNO_3$, a reduction agent and addition of surfactant. The particle size decreased with decreasing the concentration of silver nitrate and using a borohydride. The obtained Ag particles showed the spherical shape with the range of 10-20 nm.

Synthesis and Dispersion Stabilization of Indium Tin Oxide Nanopowders by Coprecipitation and Sol-Gel Method for Transparent and Conductive Films

  • Cho, Young-Sang;Hong, Jeong-Jin;Kim, Young Kuk;Chung, Kook Chae;Choi, Chul Jin
    • 대한금속재료학회지
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    • 제48권9호
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    • pp.831-841
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    • 2010
  • Indium tin oxide (ITO) nanopowders were synthesized by coprecipitation and the sol-gel method to prepare a stable dispersion of ITO nano-colloid for antistatic coating of a display panel. The colloidal dispersions were prepared by attrition process with a vibratory milling apparatus using a suitable dispersant in organic solvent. The ITO coating solution was spin-coated on a glass panel followed by the deposition of partially hydrolyzed alkyl silicate as an over-coat layer. The double-layered coating films were characterized by measuring the sheet resistance and reflectance spectrum for antistatic and antireflective properties.

Features of Nickel Nanoparticles Structure Synthesized by the Spark Discharge Method

  • Rhee, C.K.;Maksimov, A.D.;Beketov, I.V.;Medvedev, A.I.;Murzakaev, A.M.
    • 한국분말재료학회지
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    • 제27권6호
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    • pp.464-467
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    • 2020
  • Nickel nanopowders are obtained by the spark discharge method, which is based on the evaporation of the electrode surface under the action of the discharge current, followed by vapor condensation and the formation of nanoparticles. Nickel electrodes with a purity of 99.99% are used to synthesize the nickel nanoparticles in the setup. Nitrogen is used as the carrier gas with a purity of 99.998%. XRD, TEM, and EDX analyses of the nanopowders are performed. Moreover, HRTEM images with measured interplanar spacings are obtained. In the nickel nanopowder samples, a phase of approximately 90 wt% with an expanded crystal lattice of 6.5% on average is found. The results indicate an unusual process of nickel nanoparticle formation when the spark discharge method is employed.