• Title/Summary/Keyword: Nanocrystalline Fe

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Magnetic Properties of Nanocrystalline Fe-Co-Cu-Nb-Si-B Alloys (Fe-Co-Cu-Nb-Si-B 초미세결정합금의 자기적 특성연구)

  • 김약연;백종성;서영수;임우영;유성초;이수형
    • Journal of the Korean Magnetics Society
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    • v.3 no.2
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    • pp.130-134
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    • 1993
  • The magnetic properties of the amorphous $Fe_{73.5-X}Co_{X}Cu_{1}Nb_{3}Si_{13.5}B_{9}(x=2,\;4)$ alloys, fabricated by a single roll rapid quenching technique and annealed at $400~650^{\circ}C$, have been investigated. The optimum annealing temperature is $550^{\circ}C$ for the amorphous $Fe_{71.5}Co_{2}Cu_{1}Nb_{3}Si_{13.5}B_{9}$ alloy. The properties of the nanocrystalline $Fe_{71.5}Co_{2}Cu_{1}Nb_{3}Si_{13.5}B_{9}$ alloy show the relative permeability of $1.1{\times}10^{4}$ and the coercive force of 0.22 Oe at 1 kHz. When annealed at $600^{\circ}C$, the nanocrystalline $Fe_{69.5}Co_{4}Cu_{1}Nb_{3}Si_{13.5)B_{9}$ alloy shows the relative permeability of $1.0{\times}10^{4}$ and the coercive force of 0.19 Oe at 1 kHz. From the X-ray measurement, it is found that the remarkably improved soft magnetic properties are the effect of the formation of $\alpha$-Fe(Si) grain. By the results of FMR exper-imeIlt, the optimum annealing condition is just below temperature which the peak-to-peak line width of FMR spectrum increase rapidly.

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The Magnetic Properties of Ultrathin Fe-Al-Nb-B-Cu Nanocrystalline Alloys (극박형 Fe-Al-Nb-B-Cu계 초미세결정합금의 자기적 특성)

  • 박진영;서수정;김광윤;노태환
    • Journal of the Korean Magnetics Society
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    • v.6 no.4
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    • pp.211-217
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    • 1996
  • The effects of Al addition to Fe-B-Nb-Cu alloy for improving the high-frequency magnetic properties and the magnetic properties of ultrathin $Fe_{78}Al_{4}Nb_{5}B_{12}Cu_{1}$ nanocrystalline alloy ribbons with the thickness less than $10\;\mu\textrm{m}$ were investigated. It was found that the effective permeability at frequencies over- 100 kHz was very high and the core loss was very low for the composition $Fe_{78}Al_{4}Nb_{5}B_{12}Cu_{1}$ alloy. Moreover, the reduction of the ribbon thickness below $10\;\mu\textrm{m}$ was very effective in improving their permeability and the core loss characteristics up to the MHz frequency range. The values of effective permeability at 1 MHz and core loss at 0.2 T, 1 MHz were 5,000 and 1.4 kW/kg, respectively. It was considered that these results were due to far refined $\alpha-Fe$ phase structure with grain size less than 10 nm and domain structure modification.

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RELATION BETWEEN MICROSTRUCTURE AND SOFT MAGNETIC PROPERTIES OF Fe-TM-C-N (TM:Hf, Zr AND Nb) NANOCRYSTALLINE FILMS

  • Ryu, H.J.;Choi, J.O.;Han, S.H.;Kim, H.J.;Lee, J.J.;Kang, I.K.
    • Journal of the Korean Magnetics Society
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    • v.5 no.5
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    • pp.519-523
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    • 1995
  • The Fe-TM-C-N nanocrystalline films (TM : Hf, Zr and Nb) are investigated to examine the relation between microstructure and soft magnetic properties. In these films, as the atomic radius of TM element increases, $P_{N2}$ which was added to get good soft magnetic properties was decreased and the maximum value of the permeability shifted to the high Fe range in the composition diagram. The best soft magnetic properties achieved in these films are : Hc of 0.15 Oe, $\mu_{eff}$ of 7800 (1MHz) and $4{\pi}M_{s}$ of 17.5 kG in Fe-Hf-C-N film ; Hc of 0.06 Oe, $\mu_{eff}$ of 2750 (1MHz) and $4{\pi}M_{s}$ of 16.8 kG in Fe-Zr-C-N film and Hc of 0.31 Oe; $\mu_{eff}$ of 2100 (1MHz) and $4{\pi}M_{s}$ of 15.5 kG in Fe-Nb-C-N film. It was considered that the stronger the bonding force between TM and C(N), the finer TM(C,N) phase is precipitated and therefore, the finer $\alpha$-Fe grains are formed. The effective permeability of the Fe-Zr-C-N films and Fe-Nb-C-N films remains nearly constant up to 10 MHz.

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Ultra-Soft Magnetic Properties in Nanocrystalline $Fe_81B_11Nb_7Cu_1$Alloy

  • Lee, Heebok;Lee, Kyeong-Jae;Kim, Yong-Kook;Yoon, Sung-Ho;Kim, Taik-Kee;Yu, Seong-Cho
    • Journal of Magnetics
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    • v.5 no.3
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    • pp.102-105
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    • 2000
  • The extremely soft magnetic behaviors in the nanocrystalline $Fe_81B_11Nb_7Cu_1$ alloy annealed at 450 $\circ C$ and 550 $\circ C$ for 1 hour in a vacuum were investigated by means of the magnetoimpedance (MI) effect and the incremental permeability. Because the MI effect can be obtained only in ultra-soft magnetic materials, the improvement of magnetic softness by proper thermal treatment was carefully monitored by the MI effect for all annealed samples. The changes of the incremental permeability as a function of an external field were also measured to verify the magnetic softness along with the MI measurement.

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Inter-grain Exchange Interactions for Nanocrystalline Nd2.33Fe14B1.06Si0.21 Magnets

  • Jin, Han-Min;Yan, Yu;Wang, Xuefeng;Su, Feng
    • Journal of Magnetics
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    • v.8 no.4
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    • pp.157-159
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    • 2003
  • The strengths of the inter-grain exchange interaction were evaluated for nanocrystalline $Nd_{2.33}Fe_{14}B_{1.06}Si_{0.21}$ magnets of different grain size by comparing the $_{i}H_{c}$ calculated by micromagnetics with the experiments. With increase of the grain boundary thickness to that of the magnet of grain diameter 12.4, 24.8, 37.2 and 49.6 nm, the strengh of the interaction in reference to that without the grain boundary phase decreases to 83%, 69%, 54% and 42%.

Magnetoimpedance Effect in Nanocrystalline Fe91.5-xZr7BxCu1Al0.5 (x=2, 4, 6, 8) Alloys

  • Lee, Heebok;Kim, Yong-Kook;Kim, Taik-Kee;Kim, Chong-Oh;Yu, Seong-Cho
    • Journal of Magnetics
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    • v.7 no.1
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    • pp.21-23
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    • 2002
  • The magnetoimpedance of $Fe_{91.5-x}Zr_7B_xCu_1Al_{0.5}$alloys has been measured to investigate the influence of structural changes in the nanocrystallization process after thermal treatment. Annealing was performed at temperatures of $350^\circ{C}$, $450^\circ{C}$, and $550^\circ{C}$ for 1 hour in a vacuum. Ultra soft magnetic behavior was observed in the samples annealed at $550^\circ{C}$. The magnetoimpedance ratio and the longitudinal permeability ratio coincided with the softness of the magnetic properties of the thermally treated samples.

Ultra-Soft Magnetic Properties in Nanocrystalline $Fe_{81}B_{11}Nb_7Cu_1$ Alloy

  • Lee, Heebok;Lee, Kyeong-Jae;Kim, Yong-Kook;Yoon, Sung-Ho;Kim, Taik-Kee;Yu, Seong-Cho
    • Proceedings of the Korean Magnestics Society Conference
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    • 2000.09a
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    • pp.466-472
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    • 2000
  • The extremely soft magnetic behaviors in the nanocrystalline Fe$_{81}$B$_{11}$Nb$_{7}$Cu$_{1}$ alloy annealed at 450 $^{\circ}C$ and 550 $^{\circ}C$ for 1 hour respectively in a vacuum were obtained, and examined by means of the magnetoimpedance(MI) effect and the incremental permeability. Because the MI effect can be obtained only in ultra-soft magnetic materials, the improvement of magnetic softness by proper thermal treatment was carefully monitored by the MI effect for all annealed samples. The changes of the incremental permeability as a function of an external field were also measured to verify the magnetic softness along with the MI measurement.ent.

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