• Title/Summary/Keyword: Nano-wire

Search Result 187, Processing Time 0.023 seconds

Synthesis of Pt/alloy Nanoparticles by Electrical Wire Explosion in Liquid Media and its Characteristics (액중 전기선 폭발 공정을 이용한 Pt/alloy 하이브리드 나노입자의 제조 및 그 특성)

  • Koo, Hye Young;Yun, Jung-Yeul;Yang, Sangsun;Lee, Hye-Moon
    • Particle and aerosol research
    • /
    • v.8 no.2
    • /
    • pp.83-88
    • /
    • 2012
  • The electrical wire explosion process in liquid media is promising for nano-sized metal and/or alloy particles. The hybrid Pt/Fe-Cr-Al and Pt/Ni-Cr-Fe nanoparticles for exhaust emission control system are synthesized by electrical wire explosion process in liquid media. The alloy powders have spherical shape and nanometer size. According to the wire component, while Pt/Fe-Cr-Al nanoparticles are shown the well dispersed Pt on the Fe-Cr-Al core particle, Pt/Ni-Cr-Fe nanoparticles are shown the partially separated Pt on the Ni-Cr-Fe core particle. Morphologies and component of two kinds of hybrid nano catalyst particles were characterized by transmission electron microscope and energy dispersive X-ray spectroscopy analysis.

Characteristic of Power Consumption in Agitated Vessel Using Wire Gauge Impeller (금망임펠러를 이용한 교반조에서의 교반소요동력 특성)

  • Kim, Moon-Gab;Lee, Young-Sei
    • Journal of the Korean Society of Industry Convergence
    • /
    • v.14 no.2
    • /
    • pp.73-78
    • /
    • 2011
  • Power consumption for wire gauge impeller in cylindrical agitated vessel was measured over a wide range of Reynolds number from laminar to turbulent flow regions. The power correlation were obtained agitation power input of WM4 at gassing condition in turbulent region, at gassing condition in transient region and at gassing condition in laminar region. Also the compared with effect of impeller diameter and blade width on agitation power input at gassing condition in turbulent region, at gassing condition in transient region and at gassing condition in laminar region.

Metal Nano Powders as a New Getter Material (새로운 게터소재로서의 금속 나노 분말)

  • Kim, Won-Baek;Park, Je-Shin;Suh, Chang-Youl;Chang, Han-Kwon;Lee, Jae-Chun;Park, Mi-Young
    • Journal of Powder Materials
    • /
    • v.14 no.1 s.60
    • /
    • pp.56-62
    • /
    • 2007
  • Getter property of nano-sized metallic powders was evaluated as a possible candidate for the future getter material. For the purpose, Ti powders of about 50 nm were prepared by electrical wire explosion. Commercial Ti powders of about 22 micrometer were tested as well for comparison. The room-temperature hydrogen-sorption speed of nano-sized Ti powders was $1.34\;L/sec{\cdot}cm^{2}$ which was more than 4 times higher than that of micron-sized ones. The value is comparable to or even higher than those of commercial products. Its sorption speed increases with activation temperature up to $500^{\circ}C$ above which it deteriorates due to low-temperature sintering effect of nano-sized particles.

Fabrication of Ni-free Fe-based Alloy Nano Powder by Pulsed Wire Evaporation in Liquid: Part 2. Effect of Solvent and Comparison of Fabricated Powder owing to Fabrication Method (액중 전기선 폭발법에 의한 Ni-free Fe계 나노 합금분말의 제조: 2. 용매의 영향 및 제조 방법에 따른 분말입자의 비교)

  • Ryu, Ho-Jin;Lee, Yong-Heui;Son, Kwang-Ug;Kong, Young-Min;Kim, Jin-Chun;Kim, Byoung-Kee;Yun, Jung-Yeul
    • Journal of Powder Materials
    • /
    • v.18 no.2
    • /
    • pp.112-121
    • /
    • 2011
  • This study investigated the effect of solvent on the fabrication of Ni-free Fe-based alloy nano powders by employing the PWE (pulsed wire evaporation) in liquid and compared the alloy particles fabricated by three different methods (PWE in liquid, PWE in Ar, plasma arc discharge), for high temperature oxidation-resistant metallic porous body for high temperature soot filter system. Three different solvents (ethanol, acetone, distilled water) of liquid were adapted in PWE in liquid process, while X-ray diffraction (XRD), field emission scanning microscope (FE-SEM), and transmission electron microscope (TEM) were used to investigate the characteristics of the Fe-Cr-Al nano powders. The alloy powder synthesized by PWE in ethanol has good particle size and no surface oxidation compared to that of distilled water. Since the Fe-based alloy powders, which were fabricated by PWE in Ar and PAD process, showed surface oxidation by TEM analysis, the PWE in ethanol is the best way to fabricate Fe-based alloy nano powder.

Correlation Between Lateral Photovoltaic Effect and Conductivity in p-type Silicon Substrates

  • Lee, Seung-Hoon;Shin, Muncheol;Hwang, Seongpil;Park, Sung Heum;Jang, Jae-Won
    • Bulletin of the Korean Chemical Society
    • /
    • v.34 no.6
    • /
    • pp.1845-1847
    • /
    • 2013
  • The lateral photovoltaic effect (LPE) can be observed in semiconductors by irradiating a light spot position between electrodes on sample's surface. Because lateral photovoltaic voltage (LPV) is sensitively changed by light spot position, a LPE device has been tried as a position-sensitive detector. This study discusses the correlation between LPV and conductivity in p-type silicon and nano-structured Au deposited p-type silicon (nano-Au silicon), respectively. Conductivity measurement of the sample was carried out using the four-wire method to eliminate contact resistance, and conductivity dependence on LPV was simultaneously measured by changing the light irradiation position. The result showed a strong correlation between conductivity and LPV in the p-type silicon sample. The correlation coefficient was 0.87. The correlation coefficient between LPV and conductivity for the nano-Au silicon sample was 0.41.

Synthesis and Compaction of Al-based Nanopowders by Pulsed Discharge Method

  • Rhee, Chang-Kyu;Lee, Geun-Hee;Kim, Whung-Whoe
    • Journal of Powder Materials
    • /
    • v.9 no.6
    • /
    • pp.433-440
    • /
    • 2002
  • Synthesis and compaction of Al-base nano powders by pulsed discharge method were investigated. The aluminum based powders with 50 to 200 nm of diameter were produced by pulsed wire evaporation method. The powders were covered with very thin oxide layer. The perspective process for the compaction and sintering of nanostructured metal-based materials stable in a wide temperature range can be seen in the densification of nano-sized metal powders with uniformly distributed hard ceramic particles. The promising approach lies in utilization of natural uniform mixtures of metal and ceramic phases, e.g. partially oxidized metal powders as fabricated in our synthesis method. Their particles consist of metal grains coated with oxide films. To construct a metal-matrix material from such powder, it is necessary to destroy the hard oxide coatings of particles during the compaction process. This goal was realized in our experiments with intensive magnetic pulsed compaction of aluminum nanopowders passivated in air.

A Correlation Study on Surface Contamination of Semiconductor Packaging Au Wire by Components of Rinse (반도체 패키지용 Au Wire의 표면처리용 린스 성분에 따른 표면오염 비교 연구)

  • Ha-Yeong Kim;Yeon-Ryong Chu;Jisu Lim;Gyu-Sik Park;Jiwon Kim;Dahee Kang;Yoon-Ho Ra;Suk Jekal;Chang-Min Yoon
    • Journal of Adhesion and Interface
    • /
    • v.25 no.2
    • /
    • pp.63-68
    • /
    • 2024
  • In this study, the contamination of gold(Au) wire according to the types of rinse applied for surface treatment in the wire bonding process is investigated and confirmed. For the surface treatment, rinses containing silicon(Si) or those based on organic materials are mainly employed. To identify their effects, surface treatment is conducted on Au wire using two types of rinse at a 1.0 wt% concentration, referred to as Si-including and Oil-based rinse-coated Au wire. Subsequently, a simulation experiment is performed to verify the reactivity of dust containing Si components that could occur in the semiconductor process. Through optical microscopy (OM) and scanning electron microscopy(SEM) analysis, it is observed that a larger amount of dust is adsorbed on the surface of Si-including rinse-coated Au wire compared with the Oil-based rinse-coated Au wire. This is attributed that the rinse containing Si components is relatively polar, causing polar interactions with dust, which also has polarity. Therefore, it is expected that using a rinse without Si components can reduce contamination caused by dust, thereby decreasing the defect rate in the practical wire bonding process.

Effect of Ambient Temperature on Insulation Lifetime of Inverter Surge Resistant Enameled Wire Prepared with Organic/Inorganic Hybrid Nanocomposite

  • Park, Jae-Jun
    • Transactions on Electrical and Electronic Materials
    • /
    • v.17 no.3
    • /
    • pp.163-167
    • /
    • 2016
  • Inverter surge resistant enameled wire was prepared with an organic/inorganic hybrid nanocomposite, and the effect of ambient temperature on the insulation lifetime of the enameled wire in the form of twisted pair was studied by a withstanding voltage tester. The organic polymer was Polyesterimide-polyamideimide (EI/AI) and the inorganic material was a Nano-sized silica (average particle size : 15 nm). The enamel thickness was 50 μm and the ambient temperature was 100, 150, 200, and 250, respectively. Transmission electron microscopy (TEM) observation showed that Nano-sized Silica were evenly dispersed in EI/AI. There were many air gaps in a twisted pair, therefore, when voltage was applied to the twisted pair, enamel erosion took place in the air gap area because of partial discharge accordi, ng to Paschen’s law. As ambient temperature increased, insulation lifetime decreased according to Arrhenius relationship, which was explained by the increasing mobility of polymer chains in EI or AI. And insulation breakdown voltage value at 10 kHz was 1,864.5 sec (31.1 min), which is 1.9 times higher than at 20 kHz, 981.6 sec (16.4 min).

Nanotexturing and Post-Etching for Diamond Wire Sawn Multicrystalline Silicon Solar Cell (다이아몬드 와이어에 의해 절단된 다결정 실리콘 태양전지의 나노텍스쳐링 및 후속 식각 연구)

  • Kim, Myeong-Hyun;Song, Jae-Won;Nam, Yoon-Ho;Kim, Dong-Hyung;Yu, Si-Young;Moon, Hwan-Gyun;Yoo, Bong-Young;Lee, Jung-Ho
    • Journal of Surface Science and Engineering
    • /
    • v.49 no.3
    • /
    • pp.301-306
    • /
    • 2016
  • The effects of nanotexturing and post-etching on the reflection and quantum efficiency properties of diamond wire sawn (DWS) multicrystalline silicon (mc-Si) solar cell have been investigated. The chemical solutions, which are acidic etching solution (HF-$HNO_3$), metal assisted chemical etching (MAC etch) solutions ($AgNO_3$-HF-DI, HF-$H_2O_2$-DI) and post-etching solution (diluted KOH at $80^{\circ}C$), were used for micro- and nano-texturing at the surface of diamond wire sawn (DWS) mc-Si wafer. Experiments were performed with various post-etching time conditions in order to determine the optimized etching condition for solar cell. The reflectance of mc-Si wafer texturing with acidic etching solution showed a very high reflectance value of about 30% (w/o anti-reflection coating), which indicates the insufficient light absorption for solar cell. The formation of nano-texture on the surface of mc-Si contributed to the enhancement of light absorption. Also, post-etching time condition of 240 s was found adequate to the nano-texturing of mc-Si due to its high external quantum efficiency of about 30% at short wavelengths and high short circuit current density ($J_{sc}$) of $35.4mA/cm^2$.