• Title/Summary/Keyword: Nano-crystalline

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Preparation of Nano Flexible Vesicles Encapsulating Adenosine and Composition Optimization by Taguchi Method (아데노신을 포집한 나노 플렉시블 베시클 제조 및 다구찌 방법에 의한 조성의 최적화)

  • Lee, Seo Young;Jin, Byung Suk
    • Applied Chemistry for Engineering
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    • v.30 no.4
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    • pp.487-492
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    • 2019
  • Nano flexible vesicles encapsulating an adenosine, an active ingredient for anti-wrinkle, were prepared for the transdermal delivery. The nano flexible vesicle is usually composed of phospholipid, ethanol, and lysolecithin, which is a type of liquid crystalline one made by dispersing the liquid crystalline phase formed through a hydration process into a water phase. In this study, the Taguchi method, one of the experimental design methods, was applied to investigate the factors affecting the vesicle droplet size. Signal to noise (S/N) ratios for the smaller the better characteristics of vesicle droplet size were calculated using the Taguchi orthogonal array. The composition of ethanol and lysolecithin in the vesicle constituents and the amount of aqueous solution added in the hydration process were main factors that had a great effect on the vesicle droplet size and ANOVA test showed that these factors were significant at 95% confidence level.

A Study on the Ultrasonic Nano Crystal Surface Modification(UNSM) Technology and It's Application (초음파 나노표면개질기술의 특성과 활용방안 연구)

  • Pyoun, Young-Sik;Park, Jeong-Hyeon;Cho, In-Ho;Kim, Chang-Sik;Suh, Chang-Min
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.33 no.3
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    • pp.190-195
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    • 2009
  • All the failure in fatigue of torsion, bending and rolling contact, and in sliding wear begins mostly from surface. So much efforts have been invested to the surface technology which deal these problems during past decades, but the industrial demand keeps growing and more significant requirements are added to researchers and engineers. Nano crystal surface modification technology which makes the surface layers into nano crystalline, induces big and deep compressive residual stress, increases surface hardness, improves surface hardness, and make micro dimples structure on surface is an emerging technology which can break limits of current surface technology and relieve the burden of researchers and engineers. In this study, a nano crystal surface modification technology which is calling UNSM(Ultrasonic nano crystal surface modification) technology, is introduced and how it has been applied to industry to solve these failure problems is explained.

Methane hydrate formation Using Carbon Nano Tubes (탄소나노튜브를 이용한 메탄 하이드레이트 형성)

  • Park, Sung-Seek;Seo, Hyang-Min;Kim, Nam-Jin
    • 한국신재생에너지학회:학술대회논문집
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    • 2009.11a
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    • pp.549-552
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    • 2009
  • Methane hydrate is crystalline ice-like compounds which formed methane gas enters within water molecules composed cavity at specially temperature and pressure condition, and water molecule and each other from physically-bond. $1m^3$ hydrate of pure methane can be decomposed to the maximum of $172m^3$ at standard condition. If these characteristics of hydrate are reversely utilized, natural gas is fixed into water in the form of hydrate solid. Therefore the hydrate is considered to be a great way to transport and store natural gas in large quantity. Especially the transportation cost is known to be 18~24% less than the liquefied transportation. However, when methane hydrate is formed artificially, the amount of consumed gas is relatively low due to a slow reaction rate between water and methane gas. In this study, for the better hydrate reaction rate, there is make nano fluid using ultrasonic dispersion of carbon nano tube. and then, Experiment with hydrate formation by nano fluid and methane gas reaction. The results show that when the carbon nano tubes of 0.004 wt% was added to pure water, the amount of consumed gas was about 300% higher than that in pure water and the hydrate formation time decreased.

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Optimization of Wet Reduction Processing for Nanosized Cobalt Powder (나노코발트 분말합성을 위한 액상환원공정의 최적화)

  • Hong, Hyun-Seon;Jung, Hang-Chul;Kim, Geon-Hong;Kang, Lee-Seung;Suk, Han-Gil
    • Journal of Powder Materials
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    • v.20 no.3
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    • pp.191-196
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    • 2013
  • Nano-sized cobalt powder was fabricated by wet chemical reduction method at room temperature. The effects of various experimental variables on the overall properties of fabricated nano-sized cobalt powders have been investigated in detail, and amount of NaOH and reducing agent and dropping speed of reducing agent have been properly selected as experimental variables in the present research. Minitab program which could find optimized conditions was adopted as a statistic analysis. 3D Scatter-Plot and DOE (Design of Experiments) conditions for synthesis of nano-sized cobalt powder were well developed using Box-Behnken DOE method. Based on the results of the DOE process, reproducibility test were performed for nano-sized cobalt powder. Spherical nano-sized cobalt powders with an average size of 70-100 nm were successfully developed and crystalline peaks for the HCP and FCC structure were observed without second phase such as $Co(OH)_2$.

Fabrication of Perforated Strings for Transparent Silicon Shingled Photovoltaic Modules (투광형 실리콘 슁글드 태양광 모듈을 위한 타공형 스트링 제작)

  • Kim, Han Jun;Park, Min-Joon;Song, Jinho;Jeong, Taewung;Moon, Daehan;Jeong, Chaehwan
    • Current Photovoltaic Research
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    • v.8 no.4
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    • pp.120-123
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    • 2020
  • Transparent photovoltaics (PV) are used in various applications such as building-integrated photovoltaics (BIPV). However, crystalline silicon (c-Si) is not used for developing transparent PV due to its opaque nature. Here. we fabficate the three holes in 6-inch c-Si solar cells using laser scribing process with an opening area ratio of about 6.8% for transparent c-Si solar modules. Moreover, we make the shingled strings using the perforated cells. Our 7 interconnected shingled string PV cells with 21 holes show a solar to power conversion of 5.721 W. In next work, we will fabricate a transparent c-Si PV module with perforated strings.

Preparation of Porous Cobalt Thin Films by Using an Electrochemical Method (전기화학적 방법을 통한 다공성 코발트 박막 합성)

  • Ha, Seong-Hyeok;Shin, Heon-Cheol
    • Journal of the Korean institute of surface engineering
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    • v.53 no.6
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    • pp.312-321
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    • 2020
  • Morphology of porous cobalt electro-deposits was systematically investigated as functions of cobalt precursors in the plating bath and applied cathodic current density with a special focus on cobalt nano-rod formation. It was proved that the concentration of cobalt precursor plays little effect on the morphology of cobalt electro-deposits at relatively low plating current density while it significantly affects the morphology with increasing plating current density. Such a dependence was discussed in terms of the kinetics of two competitive reactions of cobalt reduction and hydrogen evolution. Cobalt nano-rod structure was created at specific ranges of cobalt precursor content and applied cathodic current density, and its diameter and length varied with plating time without notable formation of side branches which is usually found during dendrite formation. Specifically, the nano-rod length was preferentially increased in relative short plating time (<15 s), resulting in higher aspect ratio of nano-rod with plating time. Whereas, both the nano-rod length and diameter were increased nearly at the same level in a prolonged plating time, making the aspect ratio unchanged. From the analysis of crystal structure, it was confirmed that the cobalt nano-rod preferentially grew in the form of single crystal on a dense poly-crystalline cobalt thin film initially formed on the substrate.