• Proceedings of the Korean Society of Precision Engineering Conference
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• 2005.10a
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• pp.220-223
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• 2005

The rapid prototyping (RP) technology has been advanced for various applications such as verification of design, functional test. However, many RP machines still have low accuracy and limitation of applications for various materials. In this research, a hybrid RP system was developed to improve precision of micro parts. This hybrid system consists of deposition and material removal process by mechanical micro machining to fabricate nano composites using photo-curable polymer resin with various nano particles. In this work, using hybrid RP process with Multi-Walled Carbon Nano Tube (MWCNT) and hydroxyapatite, micro parts were fabricated. The precision of parts was evaluated based on the original CAD design, and to see the effect of nano particles on mechanical properties, tensile strength was measured. From the results of experiments, it was confirmed that the part made by hybrid process had higher precision, and the addition of nano particles improved mechanical properties.

• Nano
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• v.13 no.12
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• pp.1850144.1-1850144.13
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• 2018

A nano-$MoS_2$/montmorillonite K-10 (K10) composite was prepared and characterized. The composite contains two types of 2H-$MoS_2$ nanoparticles. One is the hollow spherical $MoS_2$ with a size range of 75 nm, and the other is the spherical nano cluster of $MoS_2$ with a size range of 30 nm. The two kinds of nano-$MoS_2$ were formed via assembly of numerous $MoS_2$ nano-platelets with a size of ~10 nm. A tribological comparison was then made among nano-$MoS_2$/K10, K10, nano-$MoS_2$ and a mechanical mixture of K10 and nano-$MoS_2$. K10 reduced the wear but slightly increased the friction. Nano-$MoS_2$ remarkably reduced both friction and wear. The mechanical mixture demonstrated better wear resistance than nano-$MoS_2$, indicating a synergistic anti-wear effect of nano-$MoS_2$ and K10. The synergistic effect was reinforced using nano-$MoS_2$/K10 instead of the mechanical mixture. A part of the $MoS_2$ in the contact region always lubricated the friction pair, and the rest formed a tribofilm. K10 segregated the friction pair to alleviate the ablation wear but magnified the abrasive wear. S-$MoS_2$ protects K10 and they together function as both a lubricant and an isolating agent to reduce the ablation and abrasive wear.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2011.05a
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• pp.153-153
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• 2011

Ni $TiO_2$ nano composite coatings were fabricated by using pulse current electrodeposition technique at 100 Hz pulse frequency with a constant 50% pulse duty cycles and reference was taken with respect to the direct current electrodeposition. The properties of the composite coatings were investigated by using SEM, XRD, Wear test and Vicker's microhardness test. XRD patterns of pulse deposited composite coatings were found to be changed from preferred (100) orientation to the random mixed orientations. The results demonstrated that the Vickers microhardness of composite coatings under pulse condition was significantly improved than that of pure nickel coating as well as direct current electrodeposited Ni-$TiO_2$ composite coatings. Wear tracks have shown the less plastic deformation at pulse condition with reduced coefficient of friction. Nickel matrix grain size was also found to be lower in pulse plated composite coatings as compared to direct current electrodeposited composite coatings.

• Transactions of the Korean Society for Noise and Vibration Engineering
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• v.24 no.3
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• pp.247-252
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• 2014

This paper presents a novel impact sensor which can be fabricated with smart paint made of grapheme. This smart nano paint can be easily installed on structures using a spray-on technique and that can make the sensor low cost and practical. The graphene effectively improves the piezoresistivity of the smart paint and that is available to achieve sensitive impact sensor with high gauge factor. The nano smart-paint can detect sufficient impact to cover the damaged energy range of the composite around 1~3J. The voltage outputs from the sprayed paints show fairly linear responses after signal processing. The impact makes deformation of the structure and it brings change of piezoresistivity of the paint and those converts into voltage output consequently by means of a simple signal processing system. The nano smart paint is lightweight and easily applied to the structural surface, and there is no stress concentration. The nano smart paint is expected to be a cost effective and sensitive multi-functional sensor for composites and other damage monitoring applications in the field of structural health monitoring.

• Journal of Powder Materials
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• v.21 no.2
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• pp.119-123
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• 2014

Pt has been widely used as catalyst for fuel cell and exhausted gas clean systems due to its high catalytic activity. Recently, there have been researches on fabricating composite materials of Pt as a method of reducing the amount of Pt due to its high price. One of the approaches for saving Pt used as catalyst is a core shell structure consisting of Pt layer on the core of the non-noble metal. In this study, the synthesis of Pt shell was conducted on the surface of $TiO_2$ particle, a non-noble material, by applying ultraviolet (UV) irradiation. Anatase $TiO_2$ particles with the average size of 20~30 nm were immersed in the ethanol dissolved with Pt precursor of $H_2PtCl_6{\cdot}6H_2O$ and exposed to UV irradiation with the wavelength of 365 nm. It was confirmed that Pt nano-particles were formed on the surface of $TiO_2$ particles by photochemical reduction of Pt ion from the solution. The morphology of the synthesized Pt@$TiO_2$ nano-composite was examined by TEM (Transmission Electron Microscopy).

• Transactions of the Korean Society of Mechanical Engineers A
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• v.41 no.3
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• pp.187-192
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• 2017

This paper presents an ongoing study to develop a novel pressure sensor by means of a Nano Carbon Piezoresistive Composite (NCPC). The sensor was fabricated using the 3D printing process. We designed a miniaturized cantilever-type sensor electrode to improve the pressure sensing performance and utilized a 3D printer to build a small-sized body. The sensor electrode was made of 2 wt％ MWCNT/epoxy piezoresistive nano-composite, and the sensor body was encapsulated with a pipe plug cap for easy installation to any pressure system. The piezoresistivity responses of the sensor were converted into stable voltage outputs by using a signal processing system, which is similar to a conventional foil strain gauge. We evaluated the pressure-sensing performances using a pressure calibrator in the lab environment. The 3D-printed cantilever electrode pressure sensor showed linear voltage outputs of up to 16,500 KPa, which is a 200％ improvement in the pressure sensing range when compared with the bulk-type electrode used in our previous work.

• Journal of the Korean Magnetics Society
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• v.22 no.1
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• pp.11-14
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• 2012

The composites of expanded graphite oxide and magnetic nanoparticle (Ni and Co) were synthesized by using simple chemical method. From the raw material natural graphite, the expanded graphite was fabricated using sulfuric acid and $1^{st}$ heat treatment at $600^{\circ}C$ for 1 hour. The expanded graphite was changed to expanded graphite oxide by 2nd heat treatment at $1050^{\circ}C$ for 15 sec and chemical oxidation. The expanded graphite oxide/1-methyl-2-pyrrolidone solution reacts with the magnetic nanoparticle to form a magnetic graphite oxide composite. These graphite-based materials were characterized by x-ray diffractometer, Raman spectroscopy, transmission electron microscope, and vibration sample magnetometer. We expect that these results of this paper were become basis research of graphite oxide composite.

• Korean Journal of Materials Research
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• v.23 no.2
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• pp.89-97
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• 2013

The study of grinding behavior characteristics on aluminum powders and carbon nano tubes (CNTs) has recently gained scientific interest due to their useful effect in enhancing advanced nano materials and components, which significantly improves the property of new mechatronics integrated materials and components. We performed a series of dry grinding experiments using a planetary ball mill to systematically investigate the grinding behavior during Al/CNTs nano composite fabrication. This study focused on a comparative study of the various experimental conditions at several variations of rotation speeds, grinding time and with and without CNTs. The results were monitored for the particle size distribution, median diameter, crystal structure from XRD pattern and particle morphology at a given grinding time. It was observed that pure aluminum powders agglomerated with low rotation speed and completely enhanced powder agglomeration. However, Al/CNTs composites were achieved at maximum experiment conditions (350 rpm, 60 min.) of this study by a mechanical alloy process for Al/CNTs mixed powders because the grinding behavior of Al/CNTs composite powder was affected by addition of CNTs. Indeed, the powder morphology and crystal size of the composite powders changed more by an increase of grinding time and rotation speed.

• Journal of the Korean institute of surface engineering
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• v.39 no.4
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• pp.160-165
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• 2006

Ni-SiC composite coating layers were prepared by electroplating method and their deposition rate, codeposition of SiC, morphology, surface roughness, hardness, wear and friction properties were investigated. It was found that the deposition rate and the codeposition of SiC in the composite coating layer increased with increasing concentration of SiC in the solution only at the early stage. Both of them reached certain maxima and then decreased with increasing concentration of SiC. Rough surface was obtained with increasing codeposition of SiC, which is probably due to the agglomeration of the SiC particle in the vicinity of surface. Vickers hardness increased with increasing codeposition of SiC and heat treatment at $300^{\circ}C$ in air for 1 hour. Wear volume decreased with increasing codeposition of SiC and friction coefficient increased with increasing codeposition of SiC at the early stage, and it became almost constant. Such wear and friction behaviors are desirable for the practical application.

• Bulletin of the Korean Chemical Society
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• v.35 no.6
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• pp.1659-1664
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• 2014

A porous metal-organic framework (MOF), MIL-101, was synthesized in the presence of sulfated zirconia (SZ) to produce acidic SZ/MIL-101 composites for the first time. The composites were characterized with XRD, nitrogen adsorption, FT-IR, scanning electron microscope, chemical analysis and so on. The composites (SZ/MIL-101s) were successfully applied in a liquid-phase esterification for a high yield of ester. This catalytic result of SZ/MIL-101, compared with that of pure SZ or MIL-101 (showing a negligible yield of ester), suggests that the SZ in the composite is highly active in the acid catalysis probably because of the well-dispersed active species of SZ. Moreover, the esterification is catalyzed in heterogeneous mode as confirmed by negligible esterification after filtration of the catalyst. Finally, microwaves can be efficiently applied both in the synthesis of the composites and the esterification reaction to accelerate the two processes of synthesis and esterification by about 5 times.