• Title/Summary/Keyword: NaC_60$

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Effect of Ethanol Concentration on Index Components and Physicochemical Characteristics of Cinnamon Extracts (에탄올의 농도가 계피추출액의 지표성분 및 품질특성에 미치는 영향)

  • Kim, Na-Mi;Yang, Jae-Won;Kim, Woo-Jung
    • Korean Journal of Food Science and Technology
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    • v.25 no.3
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    • pp.282-287
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    • 1993
  • The effect of ethanol concentration for extraction of cinnamon on chemical and physical properties of the extracts was investigated. The cinnamon was extracted at $80^{\circ}C$ for 5 hours. High contents of cinnamic acid, aldehyde, eugenol and antioxidant activity were found in the extracts of $60{\sim}90%$ ethanol. Free sugar, tannin, degree of browning and total solids were measured relatively high in 70% ethanol extract while total amino acids and minerals were increased as the ethanol concentration decreased. The overall data suggested 70% ethanol as the most effective solvent for cinnamon extraction.

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A Study on the Leaching of Vanadium and Nickel from Heavy Oil Fly Ash (중유회로부터 바나듐과 니켈 침출에 관한 연구)

  • 박경호
    • Resources Recycling
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    • v.1 no.1
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    • pp.29-36
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    • 1992
  • The extration of vanadium and nickel from heavy oil fly ash was carried out by using water ans sulfuric acid as leaching agent. In the leaching with water, vanadium and nickel were extracted 86% and 88% respectively under pulp density of 25g/l, room temperature and leaching time of 60 minutes, but extraction of vanadium decreased with increasing leaching time. Addition of oxidant decreased the extractions of vanadium and nickel, and roasting of fly ash at temperature higher than $300^{\circ}C$ before water leaching decreased the vanadium extraction to about zero. In the leaching with 1N sulfuric acid, the extractions of vanadium and nickel both increased to 96% and the addition of oxidant did not affect the extraction of these metals.

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Studies on the Processing of Rapid- and low Salt-Fermented Liquefaction of Anchovy(Engrulis japonica)(III) - Changes in ATP-related compounds, TMAO, TMA, Creatine, and Creatinine during Fermentation - (저식염 속성 멸치 발효액화물 가공에 관한 연구(III) - 숙성 중 ATP관련화합물, TMAO, TMA, creatine 및 creatinine 함량변화 -)

  • Park, Choon-Kyu
    • Journal of the Korean Society of Food Culture
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    • v.17 no.4
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    • pp.482-495
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    • 2002
  • Changes in ATP and related compounds, TMAO, TMA, creatine and creatinine were analyzed to establish the processing conditions for rapid- and low salt-fermented liquefaction of anchovy(Engrulis japonica) extracts during fermentation. Experimental sample A: chopped whole anchovy, adding 20% water, heating at $50^{\circ}C$ for 9 hrs and then adding 10% NaCl. Sample B: chopped whole anchovy, adding 20% water, heating at $50^{\circ}C$ for 9 hrs and then adding 13% NaCl. Sample C: chopped whole anchovy adding 13% NaCl. Sample D: whole anchovy adding 17% NaCl. ATP, ADP, AMP and IMP were broken down during fermentation period, while inosine and hypoxanthine or hypoxanthine were detected in each fermented liquefaction of anchovy. However the amounts of them were varied from collection to collection according to the pretreatment methods. Possibly ATP and their related compounds will not make a great contribution to the umami taste in fermented liquefaction of anchovy. The contents of TMAO were decreased during fermentation period, ranging from 3 to 15 mg/100g in the fermented liquefaction of anchovy after 180 days. The TMA contents were increased slowly during fermentation period, ranging from 60 to 114 mg/100g in the 180 days specimens, however their contents were varied from sample to sample. The contents of creatine and creatinine were increased during early fermentation period, and then they were decreased in the last period. As for distribution of nitrogen in the anchovy extracts, the contribution of creatine and creatinine to the extractive nitrogen was occupying 6.8, 5.7, 4.6 and 5.7% in the experimental sample A, B, C and D, respectively. The contribution of ATP and related compounds to the extractive nitrogen was occupying 2.1, 2.4, 2.2 and 2.7% in the experimental sample A, B, C and D, respectively. The contribution of TMAO and TMA to the extractive nitrogen was very low as they are occupying $0.7{\sim}1.2%$ in the four experimental samples.

Effect of Quenching and Tempering Temperatures on Mechanical Properties of A487 Cast with Different C Contents (C 함량이 다른 A487 주강품의 열처리 조건에 따른 기계적 및 부식 특성)

  • Jung, Woo-Jin;Jeong, Dae-Ho;Lee, Young-Cheol;Lee, Jae-Hyun;Kim, Sang-Shik
    • Journal of Korea Foundry Society
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    • v.35 no.4
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    • pp.88-98
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    • 2015
  • The effects of quenching and tempering temperatures on the tensile, impact and corrosion properties of A487 alloy cast with different C contents of 0.16, 0.19 to 0.23 wt.% were examined. The impact tests were conducted at $25^{\circ}C$ and $-60^{\circ}C$ and the immersion test was performed using 3.5% NaCl solution for 14 days. The quenching temperature affected the mechanical properties of A487 alloy cast, while the magnitude of change varied depending on the C content. The increase in tempering temperature showed the typical trend of decreasing tensile strength and increasing impact properties. The change in quenching and tempering temperature in this study did not affect the corrosion properties of A487 alloy significantly. The change in mechanical and corrosion properties of A487 with different C contents was discussed based on the microstructural and fractographic observation.

Heat-Induced Denaturation of Salt Soluble Protein Extracted from Spent Layer Meat (산란 노계육에서 추출한 염용성 단백질의 열변성에 관한 연구)

  • 이성기;장호선;김희주
    • Food Science of Animal Resources
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    • v.18 no.3
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    • pp.209-215
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    • 1998
  • Effects of protein concentration, ionic strength, pH, and temperature range on the heat-induced denaturation of salt soluble protein extracted from spent layer meat were investigated. Viscosity of salt soluble protein heated at 65$^{\circ}C$ for 30 min began to increase sharply above 7 mg/ml of breast protein concentration, and above 21 mg/ml of leg protein concentration, respectively. Both turbidity and viscosity showed the highest value in cooked protein solution with pH 6.0 and 1% NaCl. The turbidity of salt soluble protein started to increase continuously from 40$^{\circ}C$ to 80$^{\circ}C$. The viscosity increased rapidly from 45$^{\circ}C$ to 60$^{\circ}C$ in breast protein, and increased from 50$^{\circ}C$ to 55$^{\circ}C$ in leg protein, respectively, and then kept relatively constant. Breast protein had higher viscosity than leg protein during heat-induced gelation. Therefore, salt soluble protein from spent layer meat was associated with denatured protein (turbidity change) prior to gelation (viscosity change) during heating. Breast protein showed lower thermal transition temperature, and better gel formation than leg protein during heating.

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Assessment and Analysis of Coal Seam Gas Water Management Study for Water Resource Production 2. Prediction of Treatment Technology and Design of Co-treatment System (물 자원 생산을 위한 Coal Seam Gas Water Management Study의 평가 및 분석 2. 처리기술 예측 및 병합 시스템 설계)

  • Shin, Choon-Hwan
    • Journal of Environmental Science International
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    • v.24 no.12
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    • pp.1629-1637
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    • 2015
  • To develop various usable water from coal seam gas (CSG) water that needs to be pumped out from coal seams for methane gas production, a feasibility study was carried out, evaluating and analysing a recent report (Coal Seam Gas Water Management Policy 2012) from Queensland State Government in Australia to suggest potential CSG water treatment options for fit-for-purpose usable water production. As CSG water contains intrinsically high salinity-driven total dissolved solid (TDS), bicarbonate, aliphatic carbon, $Ca^{+2}$, $Mg^{+2}$ and so on, it was found that appropriate treatment technologies are required to reduce the hardness below 60 mg/L as $CaCO_3$ by setting the reduction rates of $Ca^{+2}$, $Mg^{+2}$ and Na+ concentrations, as well as TDS reduction. Also, Along with fiber filtration and membrane separation, an oxidation degradation process was found to be required. Along with salinity reduction, as CSG water contains organic compounds (TOC: 248 mg/L, $C_6-C_9$: <20 mg/L and $C_{10}-C_{36}$: <60 mg/L), compounds with relatively high molecular weights ($C_{10}-C_{36}$) need to be treated first. Therefore, this study suggests a combined system design with filtration (Reverse osmosis) and oxidation reduction (electrolysis) technologies, offering proper operating conditions to produce fit-for-purpose usable water from CSG water.

Comparison on the Growth of Costaria costata and Undaria pinnatifida Sporophytes in Culture and Their Field Populations (쇠미역사촌과 미역 포자체의 배양 및 야외 개체군의 생장 비교)

  • Park, Seo-Kyoung;Heo, Jin-Suk;Kim, Bo-Yeon;Song, Ji-Na;Lim, Geo-Yeong;Kim, Ha-Ni;Choi, Han-Gil
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.44 no.1
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    • pp.71-77
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    • 2011
  • The effects of temperature, light, and salinity on the growth of Costaria costata and Undaria pinnatifida juveniles were examined in laboratory cultures. In a cultivation farm, the monthly yield and density were also investigated between December and April for C. costata and between December and March in 2007 and 2008 for U. pinnatifida. The relative growth rates (RGRs) were greater at $20{\sim}60\;{\mu}mol$ photons $m^{-2}s^{-1}$ than at low ($0{\sim}10\;{\mu}mol$ photons $m^{-2}s^{-1}$) and high ($100{\sim}180\;{\mu}mol$ photons $m^{-2}s^{-1}$) irradiance levels. The optimal growth conditions for the two species were $17^{\circ}C$, 35 psu, $60\;{\mu}mol$ photons $m^{-2}s^{-1}$, and a daylength of 12 h, indicating that C. costata and U. pinnatifida have very similar growth responses to temperature, light, and salinity. However, the growth responses of the two species to various environmental factors were different; C. costata grew faster than U. pinnatifida but the latter species grew well at low salinity. The monthly yield of C. costata and U. pinnatifida increased steadily over the study period, and it was maximal in March for both species, but the yield of U. pinnatifida was greater than that of C. costata.

The Effect of CTSA Treatment on the Corrosion Resistance of AA5052 Alloy (AA5052 합금의 내식성에 영향을 미치는 CTSA처리의 영향)

  • Gu, Ga-Yeong;Bae, Seong-Hwa;Son, In-Jun;Jeong, So-Yeong;Baek, Ji-Yeon;Im, Lee-Geun
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2018.06a
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    • pp.91-91
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    • 2018
  • 스마트폰 및 카메라 케이스 등에 널리 적용되고 있는 알루미늄은 내식성, 내마모성과 같은 물리적, 화학적 성질이 우수하지 못하여 이를 향상시키기 위해 양극산화법이 산업적으로 널리 이용되고 있다. 알루미늄에 양극산화법을 적용하면 강도, 내마모성 및 내식성이 향상될 뿐만 아니라 알루미늄 표면에 규칙적으로 배열된 30nm~100nm 크기의 pore에 염료를 흡착시켜 다양한 색상의 외관을 가지는 양극산화피막을 형성시킬 수 있다. Pore간의 간격은 수십 nm~수백 nm 정도이며, pore의 크기와 간격 및 깊이는 양극산화조건(양극산화 전압, 전해액의 종류와 농도 및 온도)에 의해 크게 변화한다. 본 연구에서는 CTSA를 통한 AA5052합금의 양극산화 착색처리와 내식성의 개선 여부를 조사하였다. 알루미늄은 Al5052에는 Mg 외에, 소량의 Si을 포함하고 있다. 이 Si는 알루미늄 표면에 석출물 형태로 존재한다. 이 Si 석출물은 양극산화 시 기지상의 알루미늄 표면의 pore 형성을 방해하는 원인이다. 이러한 Si 석출물의 존재가 균일한 pore 형성을 방해하게 되고, 불균일한 포어를 가지는 표면은 착색처리 시 색상의 편차를 크게하는 원인이 되어 불량률을 높인다. 이러한 요인을 개선하기 위해 CTSA의 처리조건을 최적화 하였다. Al5052 합금을 이용하여 에칭, 디스머트, CTSA처리를 실시하였다. $55^{\circ}C$ 100g/L NaOH 용액에서 에칭을, $25^{\circ}C$ 10 vol.% $HNO_3$ 용액에서 디스머트를 실시한 다음, CTSA의 조건을 다르게 하고 SEM을 통해 Si 석출물의 감소율을 비교하였다. CTSA조건으로는 시간(60s, 180s, 300s), 농도(10%, 20%, 30%, 40%) 및 온도($25^{\circ}C$, $40^{\circ}C$, $50^{\circ}C$, $60^{\circ}C$)를 변화시켰으며, CTSA 처리 전과 후의 시편의 위치를 동일하게 하여 비교하였다. 결과 적정 시간, 농도, 온도 조건하에 pore를 불균일하게 하는 Si 석출물들이 제거되는 것을 확인할 수 있었다. CTSA 처리는 온도가 높을수록, 시간이 길수록, 농도가 적당히 진할수록 석출물이 잘 제거되는 것을 확인하였다. 또한 CTSA처리가 알루미늄의 내식성에 미치는 영향을 확인하기 위해서 침적시험에 의한 무게감소율 및 전기화학측정을 실시하였다.

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Characterization and Genomic Analysis of Novel Bacteriophage ΦCS01 Targeting Cronobacter sakazakii

  • Kim, Gyeong-Hwuii;Kim, Jaegon;Kim, Ki-Hwan;Lee, Jin-Sun;Lee, Na-Gyeong;Lim, Tae-Hyun;Yoon, Sung-Sik
    • Journal of Microbiology and Biotechnology
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    • v.29 no.5
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    • pp.696-703
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    • 2019
  • Cronobacter sakazakii is an opportunistic pathogen causing serious infections in neonates. In this study, a bacteriophage ${\Phi}CS01$, which infects C. sakazakii, was isolated from swine feces and its morphology, growth parameters, and genomic analysis were investigated. Transmission electron microscopy revealed that ${\Phi}CS01$ has a spherical head and is 65.74 nm in diameter with a 98.75 nm contracted tail, suggesting that it belongs to the family Myoviridae. The major viral proteins are approximately 71 kDa and 64 kDa in size. The latent period of ${\Phi}CS01$ was shown to be 60 min, and the burst size was 90.7 pfu (plaque-forming units)/infected cell. Bacteriophage ${\Phi}CS01$ was stable at $4-60^{\circ}C$ for 1 h and lost infectivity after 1 h of heating at $70^{\circ}C$. Infectivity remained unaffected at pH 4-9 for 2 h, while the bacteriophage was inactivated at pH <3 or >10. The double-stranded ${\Phi}CS01$ DNA genome consists of 48,195 base pairs, with 75 predicted open reading frames. Phylogenetic analysis is closely related to that of the previously reported C. sakazakii phage ESP2949-1. The newly isolated ${\Phi}CS01$ shows infectivity in the host bacterium C. sakazakii, indicating that it may be a promising alternative to antibacterial agents for the removal of C. sakazakii from powdered infant formulas.

Synthesis and Electrochemical Properties of Carbon Coated Mo6S8 using PVC (PVC를 원료로 탄소코팅한 Mo6S8의 합성 및 전기화학적 특성)

  • Si-Cheol Hyun;Byung-Won Cho;Byung-Ki Na
    • Korean Chemical Engineering Research
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    • v.61 no.3
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    • pp.348-355
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    • 2023
  • Magnesium secondary batteries are attracting much attention due to their potential to replace conventionally used lithium ion batteries. Magnesium secondary battery cathode material Mo6S8 were synthesized by molten salt synthesis method and PVC as a carbon materials were added to improve electrochemical properties. Crystal structure, size and surface of the synthesized anode materials were measured through XRD and SEM. Charge-discharge profiles and rate capabilities were measured by battery test system. 2.81 wt% PVC coated sample showed the best rate capabilities of 85.8 mAh/g at 0.125 C-rate, 69.2 mAh/g at 0.5 C-rate, and 60.5 mAh/g at 1 C-rate.