• Macromolecular Research
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• v.13 no.3
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• pp.257-264
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• 2005

Polyurethanes containing z-Iysine segments in the main chain (PULL) were synthesized from 4,4'-diphe-nylmethyl diisocyanate, poly(tetramethylene glycol), and z-Iysine oligomer as a chain extender. The PULL film was treated first with a $10\%$ HBr-acetic acid solution and subsequently with a saturated sodium bicarbonate aqueous solution to produce a primary amine group on the surface (PULL-N). Lactobionic acid (LA)-immobilized PULL (PULL-L) was prepared by the coupling reaction of the PULL surface amine groups and the LA carboxylic acid groups. The surface-modified PULLs were then characterized by attenuated total reflection-Fourier transform infra-red spectroscopy, electron spectroscopy for chemical analysis, atomic force microscopy, and contact angle goniometry. In the hepatocytes adhesion experiment, the cells poorly adhered to the PULL surface, although they adhered moderately well to the PULL-N surface. On the other hand, the cells adhered well to the PULL-L surface, suggesting the good affinity of the surface $\beta$-galactose moieties for hepatocytes. When hepatocytes were cultured in the presence of epidermal growth factor for 48 h, the cells rapidly aggregated on the PULL-L surface, whereas they aggregated only slowly on the other surfaces. The PULL prepared in this study has the potential to be used as a coating material for the enhancement of hepatocyte adhesion.

• Polymer(Korea)
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• v.27 no.5
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• pp.421-428
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• 2003

The kinetics of photoinitiated polymerization of reactive oligomer methacrylates and oligomer methacrylate/SBS blends have been studied to characterize the diffusion-controlled reaction using Fourier Transform Infrared Spectroscopy-Attenuated Total Reflectance (ATR-FTIR). The polymerization rates of reactive oligomer methacrylates and oligomer methacrylate/SBS blends were autocatalytic in nature at the initial stage and then a retardation of the reaction conversion occurred gradually as the polymer matrix became vitrified, and finally the reaction became diffusion controlled. Photopolymerization behavior of methacrylate/SBS blends was well predicted using the diffusion-controlled reaction model. N-Vinyl-2-pyrrolidinone (NVP) as a reactive solvent was used to incorporate SBS into methacrylate to form semi-IPN via photopolymerization. Due to the high reactivity of NVP, polymerization rate increased with the increase of NVP content. As the content of NVP-SBS in the blends increased up to 10 phr, the reaction conversion maintained almost constant. But above 20 phr of NVP-SBS in the blends, the reaction conversion gradually decreased since the increase of viscosity affected on the photopolymerization rate. The semi-IPN films of methacrylate/SBS blends were transparent at room temperature as well as at increased temperature and were able to be applied to surface coating.

• Proceedings of the Korean Vacuum Society Conference
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• 2010.08a
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• pp.234-234
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• 2010

The PR transitions in asymmetric dot-in-double-quantum-well (DdWELL) photodetector is identified by bias-dependent spectral behaviors. Discrete n-i-n infrared photodetectors were fabricated on a 30-period asymmetric InAs-QD/[InGaAs/GaAs]/AlGaAs DdWELL wafer that was prepared by MBE technique. A 2.0-monolayer (ML) InAs QD ensemble was embedded in upper combined well of InGaAs/GaAs and each stack is separated by a 50-nm AlGaAs barrier. Each pixel has circular aperture of 300 um in diameter, and the mesa cell ($410{\times}410\;{\mu}m^2$) was defined by shallow etching. PR measurements were performed in the spectral range of $3{\sim}13\;{\mu}m$ (~ 100-400 meV) by using a Fourier-transform infrared (FTIR) spectrometer and a low-noise preamplifier. The asymmetric photodetector exhibits unique transition behaviors that near-/far-infrared (NIR/FIR) photoresponse (PR) bands are blue/red shifted by the electric field, contrasted to mid-infrared (MIR) with no dependence. In addition, the MIR-FIR dual-band spectra change into single-band feature by the polarity. A four-level energy band model is proposed for the transition scheme, and the field dependence of FIR bands numerically calculated by a simplified DdWELL structure is in good agreement with that of the PR spectra. The wavelength shift by the field strength and the spectral change by the polarity are discussed on the basis of four-level transition.

• The Journal of Korean Institute of Communications and Information Sciences
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• v.35 no.2A
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• pp.209-215
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• 2010

This paper describes a design of variable-length FFT/IFFT processor (VL_FCore) for OFDM-based multi-standard communication systems. The VL_FCore adopts in-place single-memory architecture, and uses a hybrid structure of radix-4 and radix-2 DIF algorithms to accommodate various FFT lengths in the range of $N=64{\times}2^k\;(0{\leq}k{\leq}7)$. To achieve both memory size reduction and the improved SQNR, a two-step conditional scaling technique is devised, which conditionally scales the intermediate results of each computational stage. The performance analysis results show that the average SQNR's of 64~8,192-point FFT's are over 60-dB. The VL_FCore synthesized with a $0.35-{\mu}m$ CMOS cell library has 23,000 gates and 32 Kbytes memory, and it can operate with 75-MHz@3.3-V clock. The 64-point and 8,192-point FFT's can be computed in $2.25-{\mu}s$ and $762.7-{\mu}s$, respectively, thus it satisfies the specifications of various OFDM-based systems.

• Carbon letters
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• v.15 no.1
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• pp.57-66
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• 2014

Three activated carbons (ACs) were prepared using NaOH (N) as an activating agent. Hydrofluoric acid pre-leached rice husk was used as a precursor. After leaching, the precursor was washed with distilled water, dried, crushed, and then sieved; a size fraction of 0.3-0.5 mm was selected for carbonization in the absence of air at $600^{\circ}C$. The carbonization product (LC) was mixed with NaOH at ratios of 1:2, 1:3, and 1:4 (wt of LC: wt of NaOH) and the produced ACs after activation at $800^{\circ}C$ were designated NLC21, NLC31, and NLC41, respectively. Surface and textural properties were determined using nitrogen adsorption at $-196^{\circ}C$, scanning electron microscopy images, thermogravimetric analysis, and Fourier transform infrared spectra. These ACs were used as adsorbents for lead(II) from aqueous solutions. The effects of the textural properties and the chemistry of the carbon surfaces were investigated and the impact of the operation conditions on the capacity for lead(II) sorption was also considered. Modification of NLC41 with $H_2O_2$ and $HNO_3$ gave two other adsorbents, $H_{NLC41}$ and $N_{NLC41}$ respectively. These two new samples exhibited the highest removal capacities for lead(II), i.e.117.5 and 128.2 mg/g, respectively. The adsorption data fitted the Langmuir isotherm and the kinetic adsorption followed pseudo-second order kinetics. The thermodynamic parameters have been determined and they indicated a spontaneous endothermic process.

• Journal of KIISE:Software and Applications
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• v.26 no.12
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• pp.1468-1481
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• 1999

didates.본 논문은 절차 중심 소프트웨어를 객체 지향 소프트웨어로 재/역공학하기 위한 다단계 절차중 첫 절차인 객체 추출 절차에 대하여 기술한다. 사용한 객체 추출 방법은 전처리, 기본 분할 및 결합, 정제 결합, 결정 및 통합의 다섯 단계로 이루어진다 : 1) 전처리 과정에서는 객체 추출을 위한 FTV(Function, Type, Variable) 그래프를 생성/분할 및 클러스터링하고, 2) 기본 분할 및 결합 단계에서는 다중 객체 추출을 위한 그래프를 생성하고 생성된 그래프의 정적 객체를 추출하며, 3) 정제 결합 단계에서는 동적 객체를 추출하며, 4) 결정 단계에서는 영역 모델링과 다중 객체 후보군과의 유사도를 측정하여 영역 전문가가 하나의 최적합 후보를 선택할 수 있는 측정 결과를 제시하며, 5) 통합 단계에서는 전처리 과정에서 분리된 그래프가 여러 개 존재할 경우 각각의 처리된 그래프를 통합한다. 본 논문에서는 클러스터링 순서가 고정된 결정론적 방법을 사용하였으며, 가능한 경우의 수에 따른 다중 객체 후보, 객관적이고 의미가 있는 객체 추출 방법으로의 정제와 결정, 영역 모델링을 통한 의미적 관점에 기초한 방법 등을 사용한다. 이러한 방법을 사용함으로써 전문가는 객체 추출 단계에서 좀더 다양하고 객관적인 선택을 할 수 있다.Abstract This paper presents an object extraction process, which is the first phase of a methodology to transform procedural software to object-oriented software. The process consists of five steps: the preliminary, basic clustering & inclusion, refinement, decision and integration. In the preliminary step, FTV(Function, Type, Variable) graph for object extraction is created, divided and clustered. In the clustering & inclusion step, multiple graphs for static object candidate groups are generated. In the refinement step, each graph is refined to determine dynamic object candidate groups. In the decision step, the best candidate group is determined based on the highest similarity to class group modeled from domain engineering. In the final step, the best group is integrated with the domain model. The paper presents a new clustering method based on static clustering steps, possible object candidate grouping cases based on abstraction concept, a new refinement algorithm, a similarity algorithm for multiple n object and m classes, etc. This process provides reengineering experts an comprehensive and integrated environment to select the best or optimal object candidates.

• Journal of Ginseng Research
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• v.39 no.4
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• pp.392-397
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• 2015

Background: Red ginseng (RG) is processed from Panax ginseng via several methods including heat treatment, mild acid hydrolysis, and microbial conversion to transform the major ginsenosides into minor ginsenosides, which have greater pharmaceutical activities. During the fermentation process using microbial strains in a machine for making red ginseng, a change of composition occurs after heating. Therefore, we confirmed that fermentation had occurred using only microbial strains and evaluated the changes in the ginsenosides and their chemical composition. Methods: To confirm the fermentation by microbial strains, the fermented red ginseng was made with microbial strains (w-FRG) or without microbial strains (n-FRG), and the fermentation process was performed to tertiary fermentation. The changes in the ginsenoside composition of the self-manufactured FRG using the machine were evaluated using HPLC, and the 20 ginsenosides were analyzed. Additionally, we investigated changes of the reducing sugar and polyphenol contents during fermentation process. Results: In the fermentation process, ginsenosides Re, Rg1, and Rb1 decreased but ginsenosides Rh1, F2, Rg3, and Compound Y (C.Y) increased in primary FRG more than in the raw ginseng and RG. The content of phenolic compounds was high in FRG and the highest in the tertiary w-FRG. Moreover, the reducing sugar content was approximately three times higher in the tertiary w-FRG than in the other n-FRG. Conclusion: As the results indicate, we confirmed the changes in the ginsenoside content and the role of microbial strains in the fermentation process.

• Advances in nano research
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• v.3 no.2
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• pp.97-109
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• 2015

Citrate ion is a commonly used reductant in metal colloid synthesis, undergoes strong surface interaction with silver nanocrystallites. The slow crystal growth observed as a result of the interaction between the silver surface and the citrate ion makes this reduction process unique compared to other chemical and radiolytic synthetic methods. The antimicrobial effects of silver (Ag) ion or salts are well known, but the effects of citrate coated Ag nanoparticles (CAgNPs) are scant. Herein, we have isolated biofilm causative bacteria and fungi from drinking water PVC pipe lines. Stable CAgNPs were prepared and the formation of CAgNPs was confirmed by UV-visible spectroscopic analysis and recorded the localized surface plasmon resonance of CAgNPs at 430 nm. Fourier transform infrared spectroscopic analysis revealed C=O and O-H bending vibrations due to organic capping of silver responsible for the reduction and stabilization of the CAgNPs. X-ray diffraction micrograph indicated the face centered cubic structure of the formed CAgNPs, and morphological studies including size (average size 50 nm) were carried out using transmission electron microscopy. The hydrodynamic diameter (60.7 nm) and zeta potential (-27.6 mV) were measured using the dynamic light scattering technique. The antimicrobial activity of CAgNPs was evaluated (in vitro) against the isolated fungi, Gram-negative and Gram-positive bacteria using disc diffusion method and results revealed that CAgNPs with 170ppm concentration are having significant antimicrobial effects against an array of microbes tested.

• The KIPS Transactions:PartD
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• v.9D no.4
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• pp.531-542
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• 2002

As most of metadata have been handled on restricted applications, we need a same metadata in order to represent a same video data. However, these metadata make problems that the same video data should be supported by the same metadata. Therefore, in this paper, we extend the Dublin core elements to support the metadata which can solve the problems. The proposed video data representation is managed by the extended metadata of Doblin core model, by using the information of structure, content and manipulation of video data. The thirteen temporal relationship operators are reduced to the six temporal relationship operators by using a dummy shot temporal transformation relationship. The reduced six temporal relationship operators through excluding reverse temporal relationship not only maintain a consistency of representation between a metadata and a video data, but also transform n-ary temporal relationship to binary relationship on shots. We show that the proposed metadata model can be applied to representing and retrieving on various applications as equivalent as the same structure.

• Journal of Broadcast Engineering
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• v.17 no.1
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• pp.17-25
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• 2012

In this paper, we propose a method of producing a stereoscopic image from multiple images captured from a monoscopic camera. By translating a camera in the horizontal direction, left and right images are chosen among N captured images. For this, image edges are extracted and a rotational angle is estimated from edge orientation. Also, a translational vector is also estimated from the correlation of projected image data. Then, two optimal images are chosen and subsequently compensated using the rotational angle as well as the translational vector in order to make a satisfactory stereoscopic image. The proposed method was performed on thirty-two test image set. The subjective visual fatigue test was carried out to validate the 3D quality of stereoscopic images. In terms of visual fatigue, the 3D satisfaction ratio reached approximately 84%.