• 제목/요약/키워드: Multilayered specimens.

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Effect of different coloring liquids on the flexural strength of multilayered zirconia

  • Yu, Na-Kyoung;Park, Mi-Gyoung
    • The Journal of Advanced Prosthodontics
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    • 제11권4호
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    • pp.209-214
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    • 2019
  • PURPOSE. The purpose of this study was to evaluate the effect of two coloring liquids (aqueous and acid-based coloring liquids) and the position of multilayered zirconia on the flexural strength of multilayered zirconia. MATERIALS AND METHODS. The multilayered zirconia specimens were divided into upper and lower positions. The specimens were divided into three subgroups (n=10): non-shaded, acid-based coloring liquid, and aqueous coloring liquid. The specimens were cut using a milling machine and were immersed in either a acid-based coloring liquid or aqueous coloring liquid 2 times for 5 seconds. The specimens were sintered in a sintering furnace according to the manufacturer's introduction. The flexural strength of the specimen was measured using a universal testing machine and the surface of the specimen was observed using a field emission scanning electron microscope. RESULTS. The flexural strength of multilayered zirconia was 400 - 500 MPa. There was no statistically significant difference among all groups (P>.05).The flexural strength of the multilayered zirconia was not influenced by the kind of coloring liquid used (P>.05). The flexural strength of the multilayered zirconia colored with the coloring liquids was not influenced by its position (P>.05). CONCLUSION. The different coloring liquid application did not affect the flexural strength of multilayered zirconia of all positions.

초음파 현미경을 이용한 다층구조물의 해석 (The Analysis of Multilayered Media Using Ultrasonic Microscopy)

  • 고대식;전계석
    • 한국음향학회지
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    • 제9권2호
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    • pp.5-13
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    • 1990
  • 본 연구에서는 수 파장 이상의 깊이에 존재하는 결함을 탐상하기 위하여 50MHz의 중심주파수에서 동작하는 small aperture형 초음파현미경을 구성하였고 다층구조 샘플에 대한 영상을 연구분석하였다. 다층구조물에서의 출력특성을 음향감쇠, 수차, 렌즈형태, 샘플의 특성에 영향을 받으며 이것은 다층구조 I.C.와 bonding층 탐상에 이용할 수 있다. 실험결과, small aperture형 초음파현미경은 large aperture형 시스템에 비하여 두꺼운 샘플의 탐상에 유리하며 타 도구에서 관찰이 어려운 다층구조의 층별 탐상과 내부구조의 변형상태등을 2차원 영상으로 탐상할 수 있는 유용한 도구임을 확인하였다.

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Yb-Ba-Cu-Ag 리본의 열처리 온도에 따라 형성된 초전도 산화물의 종류와 미세구조의 변화 (Variation in the Kind of Formed Superconducting Oxide and Microstructure with Heat-Treatment Temperature in Yb-Ba-Cu-Ag Ribbons)

  • 송명엽
    • 한국세라믹학회지
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    • 제35권1호
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    • pp.79-87
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    • 1998
  • Melt spun YbBa2Cu3Agx(x=0, 5, 12, 16 and 53) precursor alloy ribbons were oxidized at 263-330$^{\circ}C$ and treated at 820$^{\circ}C$, 855$^{\circ}C$ and 885$^{\circ}C$ under 1.0 atm oxygen pressure. In the ribbons treated at 820$^{\circ}C$, 855$^{\circ}C$and 885$^{\circ}C$ 1-2-4 phase (YbBa2Cu4O8) and 1-2-3 phase (YbBa2Cu3O{{{{ OMICRON _7-$\delta$ }})were formed respectively. The shape of 1-2-4 phase was distorted or ellipsoid. The 2-4-7 and 1-2-3 phases tooked the shape of bar. All the ribbons showed zero critical current density Jc at 77K in zero magnetic field. By considering the shape and the highest critical temperature (among the three phases) of the 1-2-3 phase we tried to increase the critical current density of the ribbons treated at 885$^{\circ}C$ by press deformation. About tenribbons were stacked and coupled by press deformation and then treated at 885$^{\circ}C$ These 1-2-3 phase did not show any texture in any of the ribbons. However they exhibited weak texture in the multilayered specimens. Among the multilayered specimens YbBa2Cu3Ag16 exhibited a Jc of 180 A/cm2 Among the above ribbons YbBa2Cu3Ag16 ribbon has the optimum composition to produce textured superconducting oxide with improved Jc by press deformation. Onset critical temperatures Ton of the multilayered YbBa2Cu3Agx(x=5, 12, 16 and 53) were measured as 88-90 K.

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Al 7075/CFRP 다적층 하이브리드 복합재료의 피로수명에 대한 연구 (A study on fatigue life of Al 7075/CFRP multilayered hybrid composite materials)

  • 윤한기;김연겸;박준수;이경봉
    • 한국해양공학회지
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    • 제10권4호
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    • pp.92-102
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    • 1996
  • In this research, to develope the A1 7075/CFRP multilayered hybrid composites, CRALL(Carbon Reinforced aluminum lamiate) specimens were processed by autoclavecuring system that curing temperature, time, surface pretreatment condition of aluminum were constant. Andthe fatigye life and failure mechanism on CFRP volume fraction and fiber orientation of CRALLspecimens were investigated. A fatigue life was greatly influenced by effect of CFRP fiber volume fraction but it was less effected than those of fiber orientation. The fatigue failure arised from interface delamination of CFRP and aluminum sheet after shear fracture of aluminum layer. The failure mechanism is assumed that the aluminum laminates which divide the CFRP into many thim layers tend to arrest the failure propagation.

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반도체용 박막재료의 열응력-변형 특성에 미치는 passivation 층의 영향 분석 (Effects of passivation layer on the thermal deformation behavior of metal film used in semiconductor devices)

  • 최호성;이광렬;권동일
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1998년도 추계학술대회 논문집 학회본부 C
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    • pp.732-734
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    • 1998
  • Metal thin films such as aluminum have been used as interconnects in semiconductor device. Recently, these materials are applied to structural materials in microsensors and microactuators. In this study, we evaluate deformation and strength behavior of aluminum alloy film. Three layer model for thermal deformation of multilayered thin film material is introduced and applied to Si/Al(1%Si)/$SiO_2$ system. Based on beam bending theory and concept of bending strain. elastic and elastic/plastic thermal deformation behaviors of multilayered materials can be estimated. In the case of plastic deformation of ductile layer, strain rate equations based on deformation mechanism map are employed for describe the stress relaxation effect. To experimentally examine deformation of multilayered thin film materials, in-situ laser scanning method is used to measure curvature of specimens during heating and cooling. The thickness of $SiO_2$ layer is varied to estimate third-layer effect of thermal deformation of metal films, and its effect on deformation behavior are discussed.

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융체방사법으로 제작한 $YBa_2Cu_3Ag_{15}$$YbBa_2Cu_3Ag_x$ (x=5, 16 and 53)미세복합재의 초전도 특성 (Superconducting Characteristics of Melt Spun $YBa_2Cu_3Ag_{15}$ and $YbBa_2Cu_3Ag_x$ (x=5, 16 and 53) Microcomposites)

  • 송명엽
    • 한국재료학회지
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    • 제5권7호
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    • pp.880-887
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    • 1995
  • 융체방사법으로 제작한 YB $a_2$C $u_3$A $g_{15}$과 YbB $a_2$C $u_3$A $g_{x}$(x=5, 16 and 53) 예비 합금 리본(precursor alloy ribbon)을 263~322$^{\circ}C$에서 산화시키고, 산소 1기압 온도 872~89$0^{\circ}C$에서 열처리하였다. 또한 약 10개의 리본을 층으로 쌓아 프레스로 압축.접착시켜 다층 시편(multilayered specimen)을 제작하였다. 이 다충 시편도 위의 리본과 같은 조건에서 열처리하였다. YB $a_2$C $u_3$ $O_{7-{\delta}}$ 혹은 YbB $a_2$C $u_3$ $O_{7-{\delta}}$상이 모든 리본과 모든 다층 시편에서 형성되었다. 이 1-2-3상들은 모든 리본에서 집합조직(texture)을 나타내지 않았으나, 다층 시편들에서는 약간의 집합조직을 나타내었다. 모든 리본은 0 자장 77K에서 임계 전류 밀도 $J_{c}$가 0을 나타내었다. 다층 시편 중에서 YB $a_2$C $u_3$A $g_{15}$과 YbB $a_2$C $u_3$A $g_{16}$시편이 각각 260, 180A/$\textrm{cm}^2$의 임계 전류 밀도를 나타내었다. 여러 리본들 중에서 YB $a_2$C $u_3$A $g_{15}$ 과 YbB $a_2$C $u_3$A $g_{16}$ 리본이, 프레스 변형으로 집합조직을 가지게 함으로써 향상된 $J_{c}$를 가진 초전도 산화물을 만들 수 있는 적절한 조성을 가지고 있다. 다층 YB $a_2$C $u_3$A $g_{15}$ 시편의 개시 임계 온도 ( $T_{on}$ )는 92K 이었으며, 다층 YbB $a_2$C $u_3$A $g_{x}$(x=5, 16 and 53)의 $T_{on}$ 은 88~90K이었다.

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음극아크증착법으로 합성한 다층박막의 국부부식 기구에 관한 연구 (A Study of Localized Corrosion Mechanisms in the Multilayered Coatings by Cathodic Arc Deposition)

  • 김호건;안승호;이정호;김정구;한전건
    • 한국표면공학회지
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    • 제36권4호
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    • pp.301-306
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    • 2003
  • Multilayered WC-Ti/suv $1-x/Al_{x}$ N coatings were deposited on AISI D2 steel using cathodic arc deposition (CAD) method. These coatings contain structural defects such as pores or droplets. Thus, the substrate is not completely isolated from the corrosive environment. The growth defects (pores, pinholes) in the coatings are detrimental to corrosion resistance of the coatings used in severe corrosion environments. The localized corrosion behavior of the coatings was studied in deaerated 3.5 wt.% NaCl solution using electrochemical techniques (potentiodynamic polarization test) and surface analyses (GDOES, SEM, AES, TEM). The porosity was calculated from the result of potentiodynamic polarization test of the uncoated and coated specimens. The calculated porosity is higher in the $WC-Ti_{0.6}$ $Al_{0.4}$ N than others, which is closely related to the packing factor. The positive effects of greater packing factor act on inhibiting the passage of the corrosive electrolyte to the substrate and lowering the localized corrosion kinetics. From the electrochemical tests and surface analyses, the major corrosion mechanisms can be classified into two basic categories: localized corrosion and galvanic corrosion.

Ba 치환된 PMN-PT-PZ계 세라믹스의 압전 및 변위특성 (A Study on Piezoelectric and Strain Properties Using PMN-PT-PZ Ceramics with Ba Substitution)

  • 지승한;이능헌;박광현;박종국;이덕출
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1993년도 하계학술대회 논문집 B
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    • pp.1113-1115
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    • 1993
  • Piezoelectric Actuator samples were fabricated using PMN-PT-PZ ceramics with Barium substitution, and the strain properties of them were investigated. The tartest Piezoelectric coefficient and electromechanical coupling coefficient were observed at the sintering temperature $1250^{\circ}C$, Barium 5mol%. In the case of Multilayered specimens, they showed considerable strain and small hysteresis than single round type.

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용접 공정 디자인에 따른 클래드강의 기계적 성질 변화 (Change of Mechanical Properties of Clad Steel According to the Welding Process Design)

  • 이정현;박재원
    • 한국생산제조학회지
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    • 제22권3호
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    • pp.372-379
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    • 2013
  • In this study, we investigated the traits of the clad metals used in hot-rolled clad steel plates. We examined the sensitization and mechanical properties of STS 316 steel plate and carbon steel (A516) under the specific circumstances of post heat treatment and whether a weld was multilayered and thick or repeated because of repairs. The test conditions were as follows. The clad steel plates were butt-welded using FCAW/SAW, and the heat treatment was conducted at $625^{\circ}C$, for 80, 160, 320, 640, or 1280 min. The change in the corrosion resistance was evaluated in these specimens. In the case of the carbon steel (A516), as the heat treatment time increased, the annealing effect caused the tensile strength to decrease. The micro- hardness gradually increased and then decreased after 640 min. The elongation and contraction of the area increased gradually. An oxalic acid etch test and EPR test on STS316, a clad metal, showed a STEP structure and no sensitization. From the test results for the multi-layered and repair welds, it could be concluded that there is no effect on the corrosion resistance of clad metals. In summary, the purpose of this study was to suggest some considerations when developing on-site techniques and evaluate the sensitization of stainless steels.

피라미드 트러스형 금속 샌드위치 판재의 적외선 브레이징을 이용한 효율적 적층식 제작 및 특성에 관한 연구 (Efficient Layered Manufacturing Method of Metallic Sandwich Panel with Pyramidal Truss Structures using Infrared Brazing and its Mechanical Characteristics)

  • 이세희;성대용;양동열
    • 한국정밀공학회지
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    • 제27권8호
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    • pp.76-83
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    • 2010
  • Metallic sandwich panels with pyramidal truss structures are high-stiffness and high-strength materials with low weight. In particular, bulk structures have enough space for additional multi-functionalities. In this work, in order to fabricate 3-D structures efficiently, Layered Manufacturing Method (LMM) which was composed of three steps, including crimping process, stacking process and bonding process using rapid infrared brazing, was proposed. The joining time was drastically reduced by employing infrared brazing of which heating rate and cooling rate were faster than those of conventional furnace brazing. By controlling the initial cooling rate slowly, the bonding strength was improved up to the level of strength by conventional vacuum brazing. The observation of infrared brazed specimens by optical microscope and SEM showed no defect on the joining sections. The experiments of 1-layered pyramidal structures and 2-layered pyramidal structures subject to 3-point bending were conducted to determine structural advantages of multilayered structures. From the results, the multi-layered structure has superior mechanical properties to the single-layered structure.