• Title/Summary/Keyword: Multilayered specimens.

Search Result 14, Processing Time 0.035 seconds

Effect of different coloring liquids on the flexural strength of multilayered zirconia

  • Yu, Na-Kyoung;Park, Mi-Gyoung
    • The Journal of Advanced Prosthodontics
    • /
    • v.11 no.4
    • /
    • pp.209-214
    • /
    • 2019
  • PURPOSE. The purpose of this study was to evaluate the effect of two coloring liquids (aqueous and acid-based coloring liquids) and the position of multilayered zirconia on the flexural strength of multilayered zirconia. MATERIALS AND METHODS. The multilayered zirconia specimens were divided into upper and lower positions. The specimens were divided into three subgroups (n=10): non-shaded, acid-based coloring liquid, and aqueous coloring liquid. The specimens were cut using a milling machine and were immersed in either a acid-based coloring liquid or aqueous coloring liquid 2 times for 5 seconds. The specimens were sintered in a sintering furnace according to the manufacturer's introduction. The flexural strength of the specimen was measured using a universal testing machine and the surface of the specimen was observed using a field emission scanning electron microscope. RESULTS. The flexural strength of multilayered zirconia was 400 - 500 MPa. There was no statistically significant difference among all groups (P>.05).The flexural strength of the multilayered zirconia was not influenced by the kind of coloring liquid used (P>.05). The flexural strength of the multilayered zirconia colored with the coloring liquids was not influenced by its position (P>.05). CONCLUSION. The different coloring liquid application did not affect the flexural strength of multilayered zirconia of all positions.

The Analysis of Multilayered Media Using Ultrasonic Microscopy (초음파 현미경을 이용한 다층구조물의 해석)

  • Ko, Dae-Sik;Jun, Kye-Suk
    • The Journal of the Acoustical Society of Korea
    • /
    • v.9 no.2
    • /
    • pp.5-13
    • /
    • 1990
  • In this paper, 50MHz reflection ultrasonic microscope system with small aperture acoustic lens has been constructed in order to study the defects which lay deep in thick specimens, and acoustic images of multilayered media have been analyzed. Output characteristics of this system for multilayered media have been influenced by acoustic attenuation, aberration in specimen, type of lens and the properties of a defect, and it has been used for image processing of the multilayered I.C. and the bonding layer. In experimental results, it has been shown that small aperture ultrasonic microscope system was powerful tool for inspection of thick specimens such as electronic device, bonding layer, quality of ceramic materials.

  • PDF

Variation in the Kind of Formed Superconducting Oxide and Microstructure with Heat-Treatment Temperature in Yb-Ba-Cu-Ag Ribbons (Yb-Ba-Cu-Ag 리본의 열처리 온도에 따라 형성된 초전도 산화물의 종류와 미세구조의 변화)

  • 송명엽
    • Journal of the Korean Ceramic Society
    • /
    • v.35 no.1
    • /
    • pp.79-87
    • /
    • 1998
  • Melt spun YbBa2Cu3Agx(x=0, 5, 12, 16 and 53) precursor alloy ribbons were oxidized at 263-330$^{\circ}C$ and treated at 820$^{\circ}C$, 855$^{\circ}C$ and 885$^{\circ}C$ under 1.0 atm oxygen pressure. In the ribbons treated at 820$^{\circ}C$, 855$^{\circ}C$and 885$^{\circ}C$ 1-2-4 phase (YbBa2Cu4O8) and 1-2-3 phase (YbBa2Cu3O{{{{ OMICRON _7-$\delta$ }})were formed respectively. The shape of 1-2-4 phase was distorted or ellipsoid. The 2-4-7 and 1-2-3 phases tooked the shape of bar. All the ribbons showed zero critical current density Jc at 77K in zero magnetic field. By considering the shape and the highest critical temperature (among the three phases) of the 1-2-3 phase we tried to increase the critical current density of the ribbons treated at 885$^{\circ}C$ by press deformation. About tenribbons were stacked and coupled by press deformation and then treated at 885$^{\circ}C$ These 1-2-3 phase did not show any texture in any of the ribbons. However they exhibited weak texture in the multilayered specimens. Among the multilayered specimens YbBa2Cu3Ag16 exhibited a Jc of 180 A/cm2 Among the above ribbons YbBa2Cu3Ag16 ribbon has the optimum composition to produce textured superconducting oxide with improved Jc by press deformation. Onset critical temperatures Ton of the multilayered YbBa2Cu3Agx(x=5, 12, 16 and 53) were measured as 88-90 K.

  • PDF

A study on fatigue life of Al 7075/CFRP multilayered hybrid composite materials (Al 7075/CFRP 다적층 하이브리드 복합재료의 피로수명에 대한 연구)

  • 윤한기;김연겸;박준수;이경봉
    • Journal of Ocean Engineering and Technology
    • /
    • v.10 no.4
    • /
    • pp.92-102
    • /
    • 1996
  • In this research, to develope the A1 7075/CFRP multilayered hybrid composites, CRALL(Carbon Reinforced aluminum lamiate) specimens were processed by autoclavecuring system that curing temperature, time, surface pretreatment condition of aluminum were constant. Andthe fatigye life and failure mechanism on CFRP volume fraction and fiber orientation of CRALLspecimens were investigated. A fatigue life was greatly influenced by effect of CFRP fiber volume fraction but it was less effected than those of fiber orientation. The fatigue failure arised from interface delamination of CFRP and aluminum sheet after shear fracture of aluminum layer. The failure mechanism is assumed that the aluminum laminates which divide the CFRP into many thim layers tend to arrest the failure propagation.

  • PDF

Effects of passivation layer on the thermal deformation behavior of metal film used in semiconductor devices (반도체용 박막재료의 열응력-변형 특성에 미치는 passivation 층의 영향 분석)

  • Choi, Ho-Seong;Lee, Kwang-Ryol;Kwon, Dong-Il
    • Proceedings of the KIEE Conference
    • /
    • 1998.11c
    • /
    • pp.732-734
    • /
    • 1998
  • Metal thin films such as aluminum have been used as interconnects in semiconductor device. Recently, these materials are applied to structural materials in microsensors and microactuators. In this study, we evaluate deformation and strength behavior of aluminum alloy film. Three layer model for thermal deformation of multilayered thin film material is introduced and applied to Si/Al(1%Si)/$SiO_2$ system. Based on beam bending theory and concept of bending strain. elastic and elastic/plastic thermal deformation behaviors of multilayered materials can be estimated. In the case of plastic deformation of ductile layer, strain rate equations based on deformation mechanism map are employed for describe the stress relaxation effect. To experimentally examine deformation of multilayered thin film materials, in-situ laser scanning method is used to measure curvature of specimens during heating and cooling. The thickness of $SiO_2$ layer is varied to estimate third-layer effect of thermal deformation of metal films, and its effect on deformation behavior are discussed.

  • PDF

Superconducting Characteristics of Melt Spun $YBa_2Cu_3Ag_{15}$ and $YbBa_2Cu_3Ag_x$ (x=5, 16 and 53) Microcomposites (융체방사법으로 제작한 $YBa_2Cu_3Ag_{15}$$YbBa_2Cu_3Ag_x$ (x=5, 16 and 53)미세복합재의 초전도 특성)

  • Song, Myeong-Yeop
    • Korean Journal of Materials Research
    • /
    • v.5 no.7
    • /
    • pp.880-887
    • /
    • 1995
  • Melt spun YB $a_2$C $u_3$A $g_{15}$ and YbB $a_2$C $u_3$A $g_{x}$(x=5, 16 and 53) precursor alloy ribbons were oxidized at 263~322$^{\circ}C$, and heat-treated at 872~89$0^{\circ}C$ under 1.0atm oxygen pressure. In addition, about ten ribbons were stacked and coupled by pressing, and then followed the same heat treatment. YB $a_2$C $u_3$ $O_{7-{\delta}}$(1-2-3) or YbB $a_2$C $u_3$ $O_{7-{\delta}}$(1-2-3) phase was formed in both the ribbons and the multilayered specimens. The formed 1-2-3 phases were not texturized in all the ribbons, but slightly texturized in the multilayered specimens. $J_{c}$ was not achieved in all the ribbons at 77K and zero magnetic field. Among the multilayered specimens, YB $a_2$C $u_3$A $g_{15}$ and YbB $a_2$C $u_3$A $g_{16}$ showed $J_{c}$ of 260 and 180A/$\textrm{cm}^2$, respectively. YB $a_2$C $u_3$A $g_{15}$ and YbB $a_2$C $u_3$A $g_{16}$ are considered to be the appropriate compositions in producing textured superconducting oxides with improved $J_{c}$ by pressing. Onset critical temperature ( $T_{on}$ ) of the multilayered YB $a_2$C $u_3$A $g_{15}$ was 92K while those of YbB $a_2$C $u_3$A $g_{x}$(x=5 , 16 and 53) were 88~90K. , 16 and 53) were 88~90K.

  • PDF

A Study of Localized Corrosion Mechanisms in the Multilayered Coatings by Cathodic Arc Deposition (음극아크증착법으로 합성한 다층박막의 국부부식 기구에 관한 연구)

  • 김호건;안승호;이정호;김정구;한전건
    • Journal of the Korean institute of surface engineering
    • /
    • v.36 no.4
    • /
    • pp.301-306
    • /
    • 2003
  • Multilayered WC-Ti/suv $1-x/Al_{x}$ N coatings were deposited on AISI D2 steel using cathodic arc deposition (CAD) method. These coatings contain structural defects such as pores or droplets. Thus, the substrate is not completely isolated from the corrosive environment. The growth defects (pores, pinholes) in the coatings are detrimental to corrosion resistance of the coatings used in severe corrosion environments. The localized corrosion behavior of the coatings was studied in deaerated 3.5 wt.% NaCl solution using electrochemical techniques (potentiodynamic polarization test) and surface analyses (GDOES, SEM, AES, TEM). The porosity was calculated from the result of potentiodynamic polarization test of the uncoated and coated specimens. The calculated porosity is higher in the $WC-Ti_{0.6}$ $Al_{0.4}$ N than others, which is closely related to the packing factor. The positive effects of greater packing factor act on inhibiting the passage of the corrosive electrolyte to the substrate and lowering the localized corrosion kinetics. From the electrochemical tests and surface analyses, the major corrosion mechanisms can be classified into two basic categories: localized corrosion and galvanic corrosion.

A Study on Piezoelectric and Strain Properties Using PMN-PT-PZ Ceramics with Ba Substitution (Ba 치환된 PMN-PT-PZ계 세라믹스의 압전 및 변위특성)

  • Ji, Seung-Han;Lee, Neung-Heon;Park, Kwang-Hyun;Park, Chong-Gook;Lee, Deok-Chool
    • Proceedings of the KIEE Conference
    • /
    • 1993.07b
    • /
    • pp.1113-1115
    • /
    • 1993
  • Piezoelectric Actuator samples were fabricated using PMN-PT-PZ ceramics with Barium substitution, and the strain properties of them were investigated. The tartest Piezoelectric coefficient and electromechanical coupling coefficient were observed at the sintering temperature $1250^{\circ}C$, Barium 5mol%. In the case of Multilayered specimens, they showed considerable strain and small hysteresis than single round type.

  • PDF

Change of Mechanical Properties of Clad Steel According to the Welding Process Design (용접 공정 디자인에 따른 클래드강의 기계적 성질 변화)

  • Lee, Jung-Hyun;Park, Jaw-Won
    • Journal of the Korean Society of Manufacturing Technology Engineers
    • /
    • v.22 no.3
    • /
    • pp.372-379
    • /
    • 2013
  • In this study, we investigated the traits of the clad metals used in hot-rolled clad steel plates. We examined the sensitization and mechanical properties of STS 316 steel plate and carbon steel (A516) under the specific circumstances of post heat treatment and whether a weld was multilayered and thick or repeated because of repairs. The test conditions were as follows. The clad steel plates were butt-welded using FCAW/SAW, and the heat treatment was conducted at $625^{\circ}C$, for 80, 160, 320, 640, or 1280 min. The change in the corrosion resistance was evaluated in these specimens. In the case of the carbon steel (A516), as the heat treatment time increased, the annealing effect caused the tensile strength to decrease. The micro- hardness gradually increased and then decreased after 640 min. The elongation and contraction of the area increased gradually. An oxalic acid etch test and EPR test on STS316, a clad metal, showed a STEP structure and no sensitization. From the test results for the multi-layered and repair welds, it could be concluded that there is no effect on the corrosion resistance of clad metals. In summary, the purpose of this study was to suggest some considerations when developing on-site techniques and evaluate the sensitization of stainless steels.

Efficient Layered Manufacturing Method of Metallic Sandwich Panel with Pyramidal Truss Structures using Infrared Brazing and its Mechanical Characteristics (피라미드 트러스형 금속 샌드위치 판재의 적외선 브레이징을 이용한 효율적 적층식 제작 및 특성에 관한 연구)

  • Lee, Se-Hee;Seong, Dae-Yong;Yang, Dong-Yol
    • Journal of the Korean Society for Precision Engineering
    • /
    • v.27 no.8
    • /
    • pp.76-83
    • /
    • 2010
  • Metallic sandwich panels with pyramidal truss structures are high-stiffness and high-strength materials with low weight. In particular, bulk structures have enough space for additional multi-functionalities. In this work, in order to fabricate 3-D structures efficiently, Layered Manufacturing Method (LMM) which was composed of three steps, including crimping process, stacking process and bonding process using rapid infrared brazing, was proposed. The joining time was drastically reduced by employing infrared brazing of which heating rate and cooling rate were faster than those of conventional furnace brazing. By controlling the initial cooling rate slowly, the bonding strength was improved up to the level of strength by conventional vacuum brazing. The observation of infrared brazed specimens by optical microscope and SEM showed no defect on the joining sections. The experiments of 1-layered pyramidal structures and 2-layered pyramidal structures subject to 3-point bending were conducted to determine structural advantages of multilayered structures. From the results, the multi-layered structure has superior mechanical properties to the single-layered structure.