• Title/Summary/Keyword: Multi-coating

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Analysis of Multi-layered Thin Film Using ATR FT-IR and pyro-GC/MS (ATR FT-IR과 pyro-GC/MS를 이용한 다층박막필름의 분석)

  • Park, Sung Il;Lee, Jung-Hyun;Lee, Myung Cheon
    • Journal of Adhesion and Interface
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    • v.20 no.3
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    • pp.102-109
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    • 2019
  • The material constitution of multi-layered thin film coated on the PET base film was analyzed using ATR FT-IR and pyro GC/MS combination. The cross section of the film was acquired by cracking the film after dipping in liquid nitrogen and was observed using optical microscope. Total thickness of the coated film was $70{\mu}m$ and three layers were observed. Since each layers were too thin to analyze directly except the surface layer, analyzable area of each layers were exposed by using a proper solvent and were investigated using ATR FT-IR and pyro GC/MS. Results shows that three layers were commonly consisted of urethane-acrylate copolymers. Also, inorganic and/or metal inclusions detected by XPS and SEM-EDAX were exhibited by nano size $SiO_2$ particles in layer(1) and aluminum flakes in layer(2).

Analysis of Performance of Multi-functioned frictional force measuring instrument using adaptive smoothing (적응화 평활화법을 이용한 다기능 마찰력 측정기의 성능 분석)

  • Kim, Tae-Soo;Kim, Gwang-Su
    • The Journal of Korea Institute of Information, Electronics, and Communication Technology
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    • v.12 no.2
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    • pp.113-119
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    • 2019
  • We have developed the multi-functioned friction measuring instrument for the previous research. In here, we improved the performance of friction measuring instrument by applying the adaptive smoothing method and analyzed the friction of plate and monitoring function of friction surface through scratch tests. We substituted lubricant steel plate to lubricant oil used for reducing the friction when fabricating steel plate because lubricant oil was regarded as one of the major causes for the environmental pollution. In particular, the functions of various plate such as galvannealed steel sheets were analyzed because friction coefficient could be changed depending on the type of organic/inorganic plate or state of coating layer. Therefore, we demonstrated that adaptive smoothing method could enhance the accuracy of measuring instrument which eliminate the noise. As a result of using the method, it showed the reduction rate 0.0417% for the friction coefficient 0.16.

A Study on the Preparation and Dielectric Properties of the PLZT Thin Films. (PLZT박막의 제조 및 유전 특성에 관한 연구)

  • 박준열;박인길;이성갑;이영희
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1995.05a
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    • pp.187-191
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    • 1995
  • Thin film of the (Pb$\_$1-x/La.sub x/)(Zr$\_$0.25/Ti/Sub 0.48/) O$_3$(x=0~13[at%]) were prepared by Sol - Gel method. Multi-layer PLZT thin films were fabricated by spin-coating on Pt/Ti/SiO$_2$/Si substrate. The crystallinity and microstructure of the films were investigated with the sintering condition. At the sintering temperature of of 600[$^{\circ}C$], the perovskite phase was dominat. PLZT(11/52/48)thin films sintered at 600[$^{\circ}C$], 1[hr] had good dielectric constant (1236), dielectric loss (2.2[%]), remanent polarization (1.38[${\mu}$C/$\textrm{cm}^2$] and coercive field(16.86[ kV/cm]) respectively.

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Synthesis and Characterization of Alumina Composite Membrane by Al Evaporation and Thermal Oxidation (알루미늄의 진공증발과 열산화에 의한 알루미나 복합분리막의 제조 및 특성분석)

  • 이동호;최두진;현상훈
    • Journal of the Korean Ceramic Society
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    • v.32 no.3
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    • pp.349-358
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    • 1995
  • The ceramic composite membrane was synthesized by thermal oxidation after evaporation of Al on the support prepared by slip casting process. Oxidation was performed at $700^{\circ}C$ and 80$0^{\circ}C$ under dry oxygen atmosphere. It was considered as optimum oxidation condition that the membrane showed a knudsen behaviro. A further oxidation resulted in an increase of gas permeability because top layer became densified. Then, a multi-layered composite membrane was synthesized through a sol-gel method, evaporation and thermal oxidation of Al coating processes. While the membrane was thermally stable up to 80$0^{\circ}C$, gas permeability was rapidly decreased even at a slight amount of deposition of Al.

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Numerical Study of Metal Particle Behaviors and Flow Characteristics in Flame Spray Process (화염 스프레이 공정에서 미세 금속 입자의 거동 및 유동 특성에 대한 수치해석 연구)

  • Shin, Dong-Hwan;Lee, Jae-Bin;Lee, Seong-Hyuk
    • Journal of ILASS-Korea
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    • v.16 no.1
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    • pp.37-43
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    • 2011
  • The present study conducted computational simulation for multiphase flow in the flame spray coating process with commercially available Ni-Cr powders. The flows in a flame spray gun is characterized by very complex phenomena including combustion, turbulent flows, and convective and radiative heat transfer. In this study, we used a commercial computational fluid dynamics (CFD) code of Fluent (ver. 6.3.26) to predict gas dynamics involving combustion, gas and particle temperature distributions, and multi-dimensional particle trajectories with the use of the discrete phase model (DPM). We also examined the effect of particle size on the flame spray process. It was found that particle velocity and gas temperature decreased rapidly in the radial direction, and they were substantially affected by the particle size.

Integration and Control Technology of GaAs Bonding System using DeviceNet (DeviceNet 을 채용한 GaAs 본딩 시스템의 통합 제어기술)

  • 송준엽;이승우;임선종;김원경;배영걸
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2004.10a
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    • pp.1376-1379
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    • 2004
  • This study is designed integration and control system of GaAs bonding system consisted of multi-processing using DeviceNet and GEM-Protocol. Developing bonding system is composed of resin coating, pre-baking pre-aligner, bonding, material handler(flip robot), and wafer cassette, etc. This system has process-fluent of each a process and share information using GEM-protocol. This study devised virtual bonding simulator to control and to monitor bonding system efficiently. Also we can verify optimizing of system previously through a virtual bonding simulator.

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Optimization for Thermal spray Process by Taguchi Method (다구찌 기법을 이용한 용사코팅의 공정 최적화)

  • Kim, K.T.;Kim, Y.S.
    • Journal of Power System Engineering
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    • v.16 no.2
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    • pp.54-59
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    • 2012
  • In the present study, process optimization for thermal-sprayed Ni-based alloy coating has been performed using Taguchi method and analysis of variance(ANOVA). Ni-based alloy coatings were fabricated by flame spray process on steel substrate, and the hardness test and wear test were performed. Experiments were designed as per Taguchi's L9 orthogonal array and tests were conducted with different Oxygen gas flow, Acetylene gas flow, Powder feed rate and Spray distance. Multi response signal to noise ratio (MRSN) was calculated for the response variables and the optimum combination level of factors was obtained simultaneously using Taguchi's parametric design.

Rheological Perspectives on Direct Printing Processes

  • An, Gyeong-Hyeon
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2011.05a
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    • pp.1.2-1.2
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    • 2011
  • With recent advances in materials and products, materials processing experiences new challenges. More particles and polymers in material side and thinner and faster deformations in processing side. It happens in most emergying industries such as manufacturing of batteries, solar cells, multi-layer chips, displays, printed electronics, to list a few. In most cases, they are manufactured by coating or printing process, which is defined as a process in which gas is replaced by liquid on a substrate. In this sense, casting, inkjet printing, and roll-to-roll printing are all included. The printing process consists of three unit processes. As the materials used in the above mentioned applications typically contain a large amount of particles with polymers and solvents, they continuously change microstructures during preparation, flow, and even drying. However, little is known about the flow characteristics of such complex fluids and less is known about how to design and control the process. Therefore, for better control of the process and for better quality of the product, we need to understand the flow characteristics of these complex fluids under extremely fast flow environment.

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Preparation and Evaluation of Proliposome (프로리포솜의 제조 및 평가)

  • Chung, Dae-Sik;Shim, Chang-Koo;Lee, Min-Hwa;Kim, Shin-Keun
    • YAKHAK HOEJI
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    • v.32 no.4
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    • pp.234-238
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    • 1988
  • Proliposome of Sudan IV was prepared according to Payne et al. and evaluated for it's size distribution, surface characteristics and conversion to liposome in aqueous medium. The manufacturing procedures for proliposomes involve the coating of phospholipid solution with Sudan IV on the surface of sorbitol particle in rotary vacuum evaporator. As a result, dry, free flowing and stable proliposome was obtained and multi-lamellar liposome of sudan IV was formed spontaneously when water were added to this. Proliposomes were expected as a probable answer for the physical instability of conventional liposomes.

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Surface free-energy and hydrophobicity of MWCNT using glow plasma at low pressure (저진공 글로플라즈마를 이용한 탄소나노튜브의 표면 자유에너지와 소수성 특성)

  • Cho, Soon-Gook;Lee, Kun-A;Kim, Jung-Won;Ko, Kwang-Cheol
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2010.06a
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    • pp.123-123
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    • 2010
  • The hydrophobic coating for multi-walled nanotubes was treated with toluene and trimethylchlorosilane glow discharge plasma under low pressure, and the hydrophobic surface of the treated MWCNT was investigates. In order to investigate the effects of -CH components from the toluene and TMCS glow plasma, we conducted on the total surface free energies of the MWCNT powder, which was calculated by measuring the contact angle between the cushion of MWCNT powder and the probe liquids. The total surface free energies were determined by Owens-Wendt equation and drastically decreased.

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