• 제목/요약/키워드: Morphology and Size

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전동볼밀의 복합재 제조공정에서 각종 실험조건에 따른 입자형상 변화 및 DEM 시뮬레이션을 통한 밀링 효율의 고찰 - 회전속도, 매체크기, 매체재질의 영향 (Particle Morphology Behavior and Milling Efficiency by DEM Simulation during Milling Process for Composites Fabrication by Traditional Ball Mill on Various Experimental Conditions - Effect of Rotation Speed, Ball Size, and Ball Material)

  • 보르 암갈란;바춘흘루 이치커;자갈사이항 바트체첵;이재현;최희규
    • Korean Chemical Engineering Research
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    • 제56권2호
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    • pp.191-203
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    • 2018
  • 이 연구는 각각 크기와 재질이 다른 3 가지 종류의 분쇄 매체를 이용하여 회전속도와 밀링 시간의 따른 구리 (Cu) 분말의 형상변화의 과정에 미치는 영향을 관찰하고, 볼 움직임의 DEM시뮬레이션을 행하였다. 전동볼밀에서 볼 움직임의 3차원 시뮬레이션을 통해 분쇄 메커니즘을 규명하기 위하여 분쇄매체의 힘, 운동에너지, 매체 운동속도 등을 계산하였다. 시뮬레이션에서는 회전속도, 볼 재질, 운동속도, 마찰계수 등을 실제 실험조건과 동일하게 조건을 맞추어 투입되는 에너지의 변화량도 계산하였다. 주사전자현미경 결과를 살펴보면 볼 직경이 작을 때 입자형상이 불규칙한 형태에서 구형 형태로 변화하는 것을 알 수 있었다.

New record of five Euplotes species(Protozoa, Ciliophora) collected from South Korea

  • Jeong Hyeon Yeo;Pablo Quintela-Alonso;Jae-Ho Jung
    • Journal of Species Research
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    • 제12권3호
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    • pp.203-211
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    • 2023
  • Five ciliate species of Euplotes were isolated from fresh and coastal water during a sampling survey to identify unrecorded ciliates in South Korea. Their morphology was investigated using live observation, protargol and "wet" silver nitrate staining methods. Brief descriptions and microphotographs of each species and a comparison with related species are provided. Euplotes focardii is characterized by an average size of 65×47 ㎛ after protargol impregnation, 6 dorsal and 3 ventral ridges and dorsal argyrome pattern of double-eurystomus type. Euplotes nobilii shows an average size of 34×20 ㎛ after protargol staining, 6 dorsal and 3 ventral ridges and dorsal argyrome pattern of double-patella type. Euplotes octocarinatus, the only freshwater species described in the present study, is characterized by an average size of 66×46 ㎛ after protargol impregnation, 6 dorsal and 3 ventral ridges and dorsal argyrome pattern of double-patella type. Euplotes petzi has an average size of 43×30 ㎛ after protargol staining, a macronucleus hook-shaped and dorsal argyrome pattern in double-patella type. Euplotes raikovi is characterized by an average size of 40×24 ㎛ after protargol staining, 6 dorsal and 3 ventral ridges and dorsal argyrome pattern of double-patella type.

초미세 발포 사출 시 핵 생성장치를 이용한 셀 크기의 변화 (Cell morphology of microcellular foaming injection molding products with pressure drop rate)

  • 김학빈;차성운
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 2004년도 추계학술대회 논문집
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    • pp.491-495
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    • 2004
  • The industries use polymer materials for many purposes for they have many merits. The costs of these materials take up too great a proportion of the overall cost of products that use these materials as their major material. It is advantage for polymer industries to reduce these costs. The microcellular foaming process was developed in the early 1980s to solve this problem and proved to be quite successful. Microcellular foaming process uses inert gases such as $CO_2$, $N_2$. As these gases solve into polymer matrices, many properties are changed. The microcellular foaming process makes the glass transition temperature of polymers to low, and diminish the residual stress of polymer matrices. Besides, the microcellular foaming process has several merits, impact strength elevation, thermal insulation, noise insulation, and raw material saving etc. This characteristic of microcellular foaming process has influenced by cell morphology. The cell morphology means cell size and cell density. The cell morphology has influenced by many factors. The examples of factor are pressure drop rate, foaming temperature, foaming time, saturation pressure, saturation time etc. Among their factors, pressure drop rate is the most important factor for cell morphology in microcellular foaming injection molding process. This paper describes about the cell morphology change in accordance with the pressure drop rate of microcellular foaming injection molding process.

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Polymerized complex법에 의한 ZnWO4 nanopower의 제조 (Synthesis of ZnWO4 Nanopowders by Polymerized complex Method)

  • 류정호;임창성;오근호
    • 한국세라믹학회지
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    • 제39권3호
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    • pp.321-326
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    • 2002
  • 착체중합법을 사용하여 nano-size의 ZnWO$_4$ powder를 제조하였다. 금속이온물질로서 znic nitrate와 tungstic acid를 사용하였으며 용매는 ethylene glycol을 사용하였다. 300$^{\circ}$C부터 600$^{\circ}$C의 온도 영역에서 하소한 분말에 대해 열분해 및 결정화 과정, 분말의 형상, 입도 변화 양상을 분석하였다. 일반적인 고상합성시에 필요한 온도보다 현저히 낮은 온도인 400$^{\circ}$C에서 ZnWO$_4$상이 생성되었으며, 600$^{\circ}$C에서 완전한 경정상을 얻을 수 있었다. 합성된 분말은 400$^{\circ}$C와 500$^{\circ}$C에서 원형과 silk-worm 형태가 혼합된 입자 형상을 나타내었고, 600$^{\circ}$C에서보다 균질한 양상을 나타내었다. 합성된 분말의 입자 크기는 400$^{\circ}$C∼600$^{\circ}$C의 온도영역에서 19.9∼24.2nm 정도로 매우 미세하였으며, 하소 온도가 증가함에 따라 분말의 결정상과 입도가 증가하는 것을 확인하였다.

적외선 영상에서 모폴로지와 가우시안 거리함수를 이용한 소형표적 검출 (Small Target Detection using Morphology and Gaussian Distance Function in Infrared Images)

  • 박준재;안상호;김종호;김상균
    • 한국산업정보학회논문지
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    • 제17권4호
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    • pp.61-70
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    • 2012
  • 본 논문에서는 모폴로지 연산을 기반으로 소형 표적 후보를 찾고, 변형된 가우시안 거리 함수를 이용해서 소형 표적을 검출하는 방법을 제안한다. 기존의 소형 표적 검출 방법은 예측 필터를 이용하는 방법과 모폴로지를 이용하는 방법이 있다. 예측필터를 이용하는 방법의 경우 최소 오차 수렴 시간이 오래 걸리고, 모폴로지를 이용하는 방법의 경우 클러터에 취약하고, 소형 표적의 크기를 고려하여 구조요소의 크기를 선정해야 하는 단점이 있다. 본 논문에서는 기존 연구 방법의 단점을 보완한 강인한 소형 표적 검출 방법을 제안한다. 제안하는 방법은 먼저 미디언 필터를 사용해서 클러터를 제거한다. 다음으로 다양한 크기의 구조 요소를 이용해 닫힘 연산과 열림 연산을 수행하고, 닫힘 연산 결과와 열림 연산 결과를 차 연산 하여 표적 후보 화소를 구한다. 정확한 소형 표적을 검출하기 위해 표적 후보 영역에서 가우시안 거리 함수를 이용하여 표적을 검출한다. 제안한 방법은 클러터에 민감하지 않고, 98%의 검출율을 보였다.

Influence of inorganic composition and filler particle morphology on the mechanical properties of self-adhesive resin cements

  • Marina Rodrigues Santi ;Rodrigo Barros Esteves Lins;Beatriz Ometto Sahadi;Giovanna Correa Denucci;Gabriela Soffner ;Luis Roberto Marcondes Martins
    • Restorative Dentistry and Endodontics
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    • 제47권3호
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    • pp.32.1-32.11
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    • 2022
  • Objectives: This study aimed to evaluate the influence of inorganic composition and filler particle morphology on the mechanical properties of different self-adhesive resin cements (SARCs). Materials and Methods: Three SARCs including RelyX Unicem-2 (RUN), Maxcem Elite (MAX), and Calibra Universal (CAL) were tested. Rectangular bar-shaped specimens were prepared for flexural strength (FS) and flexural modulus (FM) and determined by a 3-point bending test. The Knoop microhardness (KHN) and top/bottom microhardness ratio (%KHN) were conducted on the top and bottom faces of disc-shaped samples. Sorption (Wsp) and solubility (Wsl) were evaluated after 24 hours of water immersion. Filler morphology was analyzed by scanning electron microscopy and X-ray energy dispersive spectroscopy (EDS). FS, FM, %KHN, Wsp, Wsl, and EDS results were submitted to 1-way analysis of variance and Tukey's post-hoc test, and KHN also to paired t-test (α = 0.05). Results: SARC-CAL presented the highest FS value, and SARC-RUN presented the highest FM. SARC-MAX and RUN showed the lowest Wsp and Wsl values. KHN values decreased from top to bottom and the SARCs did not differ statistically. Also, all resin cements presented carbon, aluminum, and silica in their composition. SARC-MAX and RUN showed irregular and splintered particles while CAL presented small and regular size particles. Conclusions: A higher mechanical strength can be achieved by a reduced spread in grit size and the filler morphology can influence the KHN, as well as photoinitiators in the composition. Wsp and Wsl can be correlated with ions diffusion of inorganic particles.

Effects of Particle Size of Barley on Intestinal Morphology, Growth Performance and Nutrient Digestibility in Pigs

  • Morel, P.C.H.;Cottam, Y.H.
    • Asian-Australasian Journal of Animal Sciences
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    • 제20권11호
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    • pp.1738-1745
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    • 2007
  • A growth trial and a digestibility trial were conducted to examine the effect of feed particle size on the performance, nutrient digestibility, gastric ulceration and intestinal morphology in pigs fed barley-based diets. Barley was processed through a hammer mill to achieve four diets varying in particle size (average particle $size{\pm}standard $deviation): coarse ($1,100{\pm}2.19\;{\mu}m$), medium ($785{\pm}2.23\;{\mu}m$), fine ($434{\pm}1.70\;{\mu}m$) and mixed (1/3 of coarse, medium and fine) ($789{\pm}2.45\;{\mu}m$). Sixty-four entire male pigs were used in the growth trial and the diets were fed ad libitum between 31 kg and 87 kg live weight. Following slaughter, stomach and ileal tissues were scored for integrity (ulceration or damage) and histological measurements taken. Twenty-four entire male pigs were used in the digestibility trial, which involved total faecal collection. Over the entire growth phase, there were no differences (p>0.05) in average daily gain and feed conversion ratio between pigs fed diets of different particle size. Pigs fed the coarse and medium diets had lower (p<0.05) stomach ulceration scores (0.20 and 0.25, respectively, on a scale from 0 to 3) than those fed the mixed (0.69) or the fine diets (1.87). The stomachs of all animals fed the fine diet had lesions and stomach ulcerations were present only in this group. Pigs fed the fine diet had thicker (p<0.001) ileal epithelial cell layer with no differences (p>0.05) being observed for villous height or crypt depth. Faecal digestibility coefficients of neutral and acid detergent fibre were the highest (p<0.05) for the mixed diet, intermediate for the fine and coarse diets and the lowest for the medium diet. A similar numerical trend (p = 0.103) was observed for the apparent faecal energy digestibility coefficient. It is concluded that, with barley based diets, a variation in average particle size between $400{\mu}m$ and $1,100{\mu}m$ had no effect on pig performance but the fine dietary particle size affected the integrity of the stomach, as well as the structure of the small intestine, thus compromising overall gut health. Our data also demonstrate that changes in particle size distribution during the digestion process, rather than average particle size or particle size variation, are related to apparent faecal digestibility.

인산을 이용한 n-type GaN의 습식식각을 통한 표면 Morphology 변화 (Evolution of Surface Morphology During Wet-Etching of N-type GaN Using Phosphoric Acidic Solutions)

  • 김재관;김택승;조영제;이지면
    • 대한금속재료학회지
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    • 제46권3호
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    • pp.169-173
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    • 2008
  • 본 논문에서는 인산을 이용하여을 인산을 이용하여 nGaN을 습식식각 할때의 표면식각 진행 특성을 조사 하였다. 인산을 이용한 고온에서의 식각은 diffusion rate limited regime을 통하여 이루어짐을 확인 하였으며, 또한 초기식각은 lateral 크기가 $20{\mu}m$에서 $5{\mu}m$ 정도인 bimodal 형태의 hexagonal 모양의 hole과 pits이 형성되며, 식각이 진행됨에 따라 표면에 형성된 hexagonal hole 등이 적층구조로 형성되거나 혹은 laterally 병합되며 식각됨을 관찰 하였다. 또한 PL 분석을 통하여 표면 거칠기 증가로 인한 extraction efficiency의 향상도 관찰할 수 있었다. 이러한 결과로부터 인산을 이용한 습식식각을 통하여 GaN의 표면 texturing 공정이 이용 가능할 수 있을 것으로 예상 된다.

Morphology control of inkjet-printed small-molecule organic thin-film transistors with bank structures

  • Kim, Yong-Hoon;Park, Sung-Kyu
    • Journal of Information Display
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    • 제12권4호
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    • pp.199-203
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    • 2011
  • Reported herein is the film morphology control of inkjet-printed 6,13-bis(triisopropylsilylethynyl) pentacene (TIPS-pentacene) organic thin-film transistors for the improvement of their performance and of the device-to-device uniformity. The morphology of the inkjetted TIPS-pentacene films was significantly influenced by the bank geometry such as the bank shapes and confinement area for the channel region. A specific confinement size led to the formation of uniform TIPS-pentacene channel layers and better electrical properties, which suggests that the ink volume and the solid concentration of the organic-semiconductor solutions should be considered in designing the bank geometry.

Pressure Effects on the Morphology Development of C/C Composites During Carbonization

  • Joo, Hyeok-Jong;Ryu, Seung-Hee;Ha, Hun-Seung
    • Carbon letters
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    • 제1권3_4호
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    • pp.158-164
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    • 2001
  • It is well known that the fabrication process of carbon/carbon composites is very complex. Above all, the carbonization process have major effect on the morphology development of carbon matrix. Carbon/carbon composites of 4-directional fiber preform were fabricated using the coal tar based pitch as a matrix precursor in this study. According to carbonization pressure of 1 bar, 100 bar, 600 bar, and 900 bar, morphological changes of cokes and matrix of composites were discussed. As the carbonization pressure increased to 600 bar, the flow pattern morphology of bulk mesophse was well developed. On the contrary, mosaic pattern morphology was found in case of 900 bar of carbonization pressure. It is confirmed that the carbonization pressure have profound effect on the degree of graphitization and crystal size of carbon matrix. Even in the highly densified carbon/carbon composites, large voids were still found in the matrix pocket region.

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