• Title/Summary/Keyword: Modulus Measurement

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Mechanical Properties of High Stressed Silicon Nitride Beam Measured by Quasi-static and Dynamic Techniques

  • Shin, Dong Hoon;Kim, Hakseong;McAllister, Kirstie;Lee, Sangik;Kang, Il-Suk;Park, Bae Ho;Campbell, Eleanor E.B.;Lee, Sang Wook
    • Proceedings of the Korean Vacuum Society Conference
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    • 2016.02a
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    • pp.361.1-361.1
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    • 2016
  • Due to their high sensitivity, fast response, small energy consumption and ease of integration, nanoelectromechanical systems (NEMS) have attracted much interest in various applications such as high speed memory devices, energy harvesting devices, frequency tunable RF receivers, and ultra sensitive mass sensors. Since the device performance of NEMS is closely related with the mechanical and flexural properties of the material in NEMS, analysis of the mechanical and flexural properties such as intrinsic tensile stress and Young's modulus is a crucial factor for designing the NEMS structures. In the present work, the intrinsic mechanical properties of highly stressed silicon nitride (SiN) beams are investigated as a function of the beam length using two different techniques: (i) dynamic flexural measurement using optical interferometry and (ii) quasi-static flexural measurement using atomic force microscopy. The reliability of the results is analysed by comparing the results from the two different measurement techniques. In addition, the mass density, Young's modulus and internal stress of the SiN beams are estimated by combining the techniques, and the prospect of SiN based NEMS for application in high sensitive mass sensors is discussed.

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Rheological Properties and Cure Kinetics of Cycloaliphatic/DGEBA Epoxy Blend System Initiated by Cationic Latent Curing Agent (잠재성 경화제를 이용한 Cycloaliphatic/DGEBA계 에폭시 블렌드 시스템의 유변학적 특성 및 경화 동력학)

  • 곽근호;박수진;이재락;김영근
    • The Korean Journal of Rheology
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    • v.10 no.4
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    • pp.227-233
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    • 1998
  • The effects of 1 mol% N-benzylpyrazinium hexafluoroantimonate(BPH) as a thermal latent initiator and blend compositions composed of cycloaliphatic and DGEBA epoxies were investigated in the rheological properties and cure kinetics. Latent properties were performed by measurement of the conversion as a function of reaction time using isothermal DSC at $150^{\circ}C$ and $50^{\circ}C$ Rheological properties of the blend systems were investigated in terms of isothermal experiments using a rheometer. The gelation time was obtained from the evaluation of storage modulus (G'), loss modulus (G") and damping factor (tan$\delta$)). Cross-linking activation energy ($E_c$) was also determined from the Arrhenius equation based on gel time and curing temperature. As a result, the gel time and cross-linking activation energy increased with increasing DGEBA composition. The cure activation energies ($E_a$) were obtained by Kissinger method using dynamic DSC thermograms. In this work, the cure activation energy decreased with increasing CAE concentration, which might be resulted from the short repeat units, simple side-groups and viscosity of reaction media.edia.

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Measurement of Dynamic Elastic Constants of RPV Steel Weld due to Localized Microstructural Variation (원자로 용접부의 국부적 미세조직 변화에 따른 동적탄성계수 측정)

  • Cheong, Yong-Moo;Kim, Joo-Hag;Hong, Jun-Hwa;Jung, Hyun-Kyu
    • Journal of the Korean Society for Nondestructive Testing
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    • v.20 no.5
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    • pp.390-396
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    • 2000
  • The dynamic elastic constants of the simulated weld HAZ (heat-affected zone) of SA 508 Class 3 reactor pressure vessel (RPV) steel were investigated by resonant ultrasound spectroscopy (RUS). The resonance frequencies of rectangular parallelepiped samples woe calculated from the initial estimates of elastic stiffness $c_{11},\;c_{12}\;and\;c_{44}$ with an assumption of isotropic property, dimension and density. Through the comparison of calculated resonant frequencies with the measured resonant frequencies by RUS, very accurate elastic constants of SA 508 Class 3 steel were determined by iteration and convergence processes. Clear differences of Youngs modulus and shear modulus were shown from samples with different thermal cycles and microstructures. Youngs modulus and shear modulus of samples with fine-grained bainite were higher than those with coarse-grained tempered martensite. This tendency was confirmed from other results such as micro-hardness test.

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An Experimental Study on the mechanical and Shrinkage Properties of Concrete Using High Fineness Fly ash (고분말도 플라이애쉬를 사용한 콘크리트의 역학 및 수축특성에 관한 실험적 연구)

  • Lee, Ji-Hwan;Bae, Pil-Sik;Kim, Sung-Soo;Kim, Jae-Hwan;Lee, Sang-Soo;Song, Ha-Young
    • Proceedings of the Korea Concrete Institute Conference
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    • 2008.04a
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    • pp.725-728
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    • 2008
  • This study was to establish 3 levels of high fineness fly ash like 4000, 6000, and 8000 class and 30% replacement ratio in order to analyze mechanics and shrinkage properties of concrete by using high fineness fly ash. Furthermore, this study was to make a plan in two levels of water-binder ratio like 40% and 50%. In addition, as a result of measurement by the establishment of combined condition of ternary system as 20% replacement ratio level of three sorts of ground granulated blast furnace slag, there was a tendency to be equal or higher to the plain concrete as the fineness of fly ash increased in strength property. Simultaneously, this study had a tendency in the relationship between the compressive strength and elastic modulus that the more the fineness of fly ash, the more the elastic modulus increased a little. In addition, this study had a tendency that the more elastic modulus moved to the long-term aged one, the more it increased definitely. The effect on the fineness of fly ash remained at a low level in the drying shrinkage. This study has shown that the more the fineness increased, the more the elastic modulus decreased.

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Settlement Behavior Characteristics of CFRD in Construction Period - Case of Daegok Dam - (콘크리트 표면 차수벽형 석괴댐의 축조 중 침하거동 특성 - 대곡댐을 중심으로 -)

  • Park Han-Gyu;Kim Yong-Seong;Seo Min-Woo;Lim Heui-Dae
    • Journal of the Korean Geotechnical Society
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    • v.21 no.7
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    • pp.91-105
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    • 2005
  • In this study, the deformation behavior of Daegok dam during the construction was analyzed based on the measurement data and a comparative analysis with foreign CFRD measurements was performed. From measuring settlements of Daegok dam with depth, overall behavior was evaluated to be consistent with measured data of other CFRD dams. In addition, construction modulus, void ratio and shape factor were also evaluated to be major factors in predicting the settlement behavior during construction of CFRD-typed dam from measured data of 38 CFRD-typed dams, and the maximum internal settlement is proportional to the void ratio. From the relationship between the maximum internal settlement and the height of a dam, 26 dams were assessed to have its relative modulus ranging between 0.001 and 0.01. In case of general CFRD, the average modulus of maximum internal settlement to the height of a dam is estimated to be 0.005. In case of a low void ratio, the construction modulus was high with its shape factor below 4. On the other hand, in case of a high void ratio, the relative settlement rate was high with its shape factor more than 4.

Evaluation of Modulus of Elasticity of Wood Exposed to Accelerated Weathering Test by Measuring Ultrasonic Transmission Time (촉진 열화 목재의 초음파 전달 시간 측정을 통한 탄성 계수의 평가)

  • Park, Chun-Young;Kim, Gwang-Chul
    • Journal of the Korean Wood Science and Technology
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    • v.42 no.3
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    • pp.275-281
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    • 2014
  • In this study, accelerated weathering test was performed with wood, a major material for wooden cultural building. In order to evaluate the deterioration of wood, ultrasonic transmission times were measured to evaluate dynamic modulus of elasticity (MOE), which was verified by determining static MOE using three-point bending test. Ultrasonic transmission time was decreased with an increase in the weathering time levels (0, 500, 1000 hours) while it increased in 1500 and 2000 hours. Distribution of dynamic and static MOE was similar to that of the ultrasonic transmission time measurements. The results mean that the measurement of ultrasonic transmission time was very effective to evaluate MOE of wooden cultural buildings for their preservation and management. This method could be utilized to assess wooden cultural buildings as a way of preserving them in a scientific manner.

Prediction on the Performance of Polymer-Based Mechanical Low-Pass Filters for High-G Accelerometers (고충격 가속도센서용 고분자 기반 기계식 저역통과필터의 성능 예측)

  • Sehwan Song;Junyong Jang;Youlim Lee;Hanseong Jo;Sang-Hee Yoon
    • Journal of the Korea Institute of Military Science and Technology
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    • v.26 no.3
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    • pp.262-272
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    • 2023
  • A polymer-based mechanical low-pass filter(m-LPF) for high-g accelerometers makes it possible to remove high-frequency transient noises from acceleration signals, thus ensuring repeatable and reliable measurement on high-g acceleration. We establish a prediction model for performance of m-LPF by combining a fundamental vibration model with the fractional derivative standard linear solid(FD SLS) model describing the storage modulus and loss modulus of polymers. Here, the FD SLS model is modified to consider the effect of m-LPF shape factor (i.e., thickness) on storage modulus and loss modulus. The prediction accuracy is verified by comparing the displacement transmissibility(or cut-off frequency) estimated using our model with that measured from 3 kinds of polymers(polysulfide rubber(PSR), silicone rubber(SR), and polydimethylsiloxane(PDMS)). Our findings will contribute a significant growth of m-LPF for high-g accelerometers.

Understanding the Viscoelastic Properties and Surface Characterization of woodflour-Polypropylene Composites (목분-폴리프로필렌 복합재의 점탄성적 성질과 표면특성)

  • Son, Jungil;Gardner, Douglas J.
    • Journal of Adhesion and Interface
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    • v.3 no.4
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    • pp.1-9
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    • 2002
  • The main goal of this study was to analyze the effect of process additives, i.e. maleated polypropylene (MAPP), and nucleating agent on the viscoelastic properties of different types of extruded polypropylene-wood plastic composites manufactured from either PP homopolymer, high crystallinity PP or PP impact copolymer using dynamic mechanical thermal analysis. And also, the esterification reaction between wood flour and maleated polypropylene, and its role in determining the mechanical properties of wood flour-polypropylene composites was investigated. The wood plastic composites were manufactured using 60% pine wood flour and 40% polypropylene on a Davis-Standard $Woodtruder^{TM}$. Dynamic mechanical thermal properties, polymer damping peaks(than ${\delta}$), storage modulus (E') and loss modulus (E") were measured using a dynamic mechanical thermal analyzer. XPS (X-ray Photoelectron Spectroscopy), also known as ESCA (Electron Spectroscopy for Chemical Analysis) study of wood flour treated with MAPP was performed to obtain information on the chemical nature of wood fiber before and after treatment. To analyze the effect of frequency on the dynamic mechanical properties of the various composites, DMA tests were performed over a temperature range of -20 to $100^{\circ}C$, at four different frequencies (1, 5, 10 and 25 Hz), and at a heating rate of $5^{\circ}C/min$. From these results, the activation energy of the various composite was measured using an Arrhenius relationship to investigate the effect of maleated PP and nucleating agent on the measurement of the interphase between the wood and plastic of the extruded polypropylene wood plastic composites.

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Nanoindentation과 유한요소해석을 통한 표면처리강판의 박막 경도 및 탄성계수 측정

  • 고영호;이정민;김병민;고대철
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2004.05a
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    • pp.142-142
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    • 2004
  • 박막으로 표면처리한 다양한 강판이 자동차 차체와 부품, 가전제품 등의 제조를 위해 여러 가지 판재 성형공정에 적용되고 있으나, 제품 개발기간과 비용 감소, 성형과정에서 표면 코팅층의 특성 변화로 인해 성형성 열화와 성형불량을 줄이면서, 제품의 고정밀화, 고품질화를 실현하기 위해서는 코팅층에 대한 기계적 특성과 마찰거동을 명확히 규명하는 것이 반드시 필요하다 현재 나노 마이크로 수준인 코팅층의 기계적 물성치를 측정하기 위해 가장 널리 사용되는 방법은 나노 인덴테이션이다.(중략)

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