• Title/Summary/Keyword: Mixed grinding

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Thermoelctric Propretries of Bi2Te3 Fabricated by Mechanical Grinding-Mixing Process (기계적분쇄-혼합공정에 의해 제조된 Bi2Te3 소결체의 열전특성)

  • 이근길
    • Journal of Powder Materials
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    • v.7 no.1
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    • pp.6-11
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    • 2000
  • Two kinds of Bi2Te3 powders, pure Bi2Te3/2vol.%ZrO2, have been prepared by a mechanical grinding process process. Effect of mixing of the powders on thermoelectric of the sintered body has been investigated by measuring Seebeck Coeffcient, specific electric resistivity and thermal conductivity. With an increase in the weight fraction of the Bi2Te3/2vol.%ZrO2 powder from 0 to 40wt.%. Especially, the figure of merit of the mixedBi2Te3 sintered body increases and thereafter dedreases above 40wt.%. Especially. the figure of merit of the mixed Bi2Te3 sintered bodies with mixing of Bi2Te3/2vol.%ZrO2 powder increased about 1.3time in comparison with the value of the specimen before mixing. Mixing of two kinds of Bi2Te3 powders which have different theramal and electric propertries with each other seemed to be useful methob to increase the figure of merit of Bi2Te3 sintered body.

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A Study on the Improvement of Early-age Compressive Strength of Smart BFS Powder Added Cement Mortar (스마트 고로슬래그 미분말을 첨가한 시멘트 모르타르의 초기 압축강도 향상에 관한 연구)

  • Yi, Seong Tae;Noh, Jae Ho;Kim, Jin Hyung;Lee, Kang Jin
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.17 no.2
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    • pp.135-141
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    • 2013
  • In this study, to improve the early-age compressive strength of mortar, the compressive strength tests of mortar mixed smart BFS powder added powder of rapid setting additives milled by processing, using functional grinding aid, the power-typed rapid setting cement clinker developed by sintering industrial waste and by-products with much CaO-$SiO_2-Al_2O_3$ to cement were performed. From the tests, the followings are found that (1) for BFS early-age strength improvement test (Series I): early-age strength improvement of BFS mixed rapid setting additive milled after adding functional grinding aid, when the clinker is milled, is superior and (2) for OPC early-age strength improvement test (Series II): case of additive mixed rapid setting powder typed activator milled after adding functional grinding aid to Clinker-C showed the higher compressive strength.

Effect of Grinding on Solubility and Particle Size of Pefioxacin by Planetary Ball-Mill (유성볼밀을 이용한 난용성 Pefloxacin의 분쇄조작에 의한 입자 설계)

  • 임영근;김진우;최우식;야마모토;정해영
    • Journal of Life Science
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    • v.9 no.2
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    • pp.194-200
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    • 1999
  • Grinding aid is a necessary unit operation when the raw materials are handled in solid form, and the purpose is to improve the bioavailability by reducing the particle size. For the particle design of pefloxacin, the dry planetary ball-mill was used. With the drying process, 330 g of zirconia ball with its size of 2 mm in diameter and 10 g of pefloxacin were transferred to the pot and mixed well. The mixture was ground at 112 rpm (60 Hz) for 15, 30, and 60 min, respectively. The most satisfactory grinding products were generated at 15 min of grinding time for their particle size. The volume mean diameter $\X_50$ of the grinding products was 2.97 $\mu$m. X-ray diffraction (XRD), differential scanning calorimeter (DSC), and infrared spectroscopy (IR) patterns were relatively unchanged before pulverizing pefloxacin and in the progress of grinding. Thus, these results suggest that this pulverizing method can be used for grinding products without evident effect on stability of the drug pefloxacin. Dissolution test was carried out to set up the optimal detective condition against residual antibacteria of fish by HPLC. The grinding pefloxacin for 15 min is most effective in dissolution test.

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A Study on Physical Properties of Mortar Mixed with Fly-ash as Functions of Mill Types and Milling Times

  • Seo, Sung Kwan;Chu, Yong Sik;Shim, Kwang Bo;Jeong, Jae Hyun
    • Journal of the Korean Ceramic Society
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    • v.53 no.4
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    • pp.435-443
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    • 2016
  • Coal ash, a material generated from coal-fired power plants, can be classified as fly ash and bottom ash. The amount of domestic fly ash generation is almost 6.84 million tons per year, while the amount of bottom ash generation is 1.51 million tons. The fly ash is commonly used as a concrete admixture and a subsidiary raw material in cement fabrication process. And some amount of bottom ash is used as a material for embankment and block. However, the recyclable amount of the ash is limited since it could cause deterioration of physical properties. In Korea, the ashes are simply mixed and used as a replacement material for cement. In this study, an attempt was made to mechanically activate the ash by grinding process in order to increase recycling rates of the fly ash. Activated fly ash was prepared by controlling the mill types and the milling times and characteristics of the mortar containing the activated fly ash was analyzed. When the ash was ground by using a vibratory mill, physical properties of the mortar mixed with such fly ash were higher than the mortar mixed with fly ash ground by a planetary mill.

An Experimental Study on Frictional Characteristics of the Piston Ring (피스톤 링 마찰 특성의 실험적 연구)

  • Lee, Jae-Seon;Han, Dong-Chul
    • Transactions of the Korean Society of Automotive Engineers
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    • v.7 no.6
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    • pp.115-122
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    • 1999
  • A friction tester to measure friction force generated at the interface between the piston ring and the cylinder liner was developed. Modified piston ring is bar-shaped and 100mm long. Surface of the modified piston ring is machined by the profile grinding machine to be formed as a shape of an arc of a circle. Measured data are treated as mean effective friction force and power loss. From this test it can be confirmed that friction force is deeply affected by surface shape of the piston ring and viscosity of supplied oil. Friction force is deeply affected by surface shape of the piston ring and viscosity of supplied oil. Friction force is decreased and power loss is increased with increasing velocity. And it is known that region of mixed lubrication is broader than estimated with theoretical analysis. it is expected that this tester can be used as the optimization tool of the surface shape of the piston ring at the first stage of development of the piston rings.

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Effects of different surface treatments on the shear bond strength of veneering ceramic materials to zirconia

  • Abdullah, Adil Othman;Hui, Yu;Sun, Xudong;Pollington, Sarah;Muhammed, Fenik Kaml;Liu, Yi
    • The Journal of Advanced Prosthodontics
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    • v.11 no.1
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    • pp.65-74
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    • 2019
  • PURPOSE. To evaluate and compare the effect of different materials and techniques on the shear bond strength of veneering ceramic materials to zirconia. MATERIALS AND METHODS. 136 sintered zirconia cubes were prepared and randomly divided into four study groups according to corresponding methods of surface treatment and materials: GLN (grinding followed by laser scanning using Noritake Cerabien ZR), SLN (sandblasting followed by laser scanning using Noritake Cerabien ZR), GLV (grinding followed by laser scanning using VITA VM 9), and SLV (sandblasting followed by laser scanning using VITA VM 9). Spraying technique was performed to coat the core. Profilometer, SEM, XRD, EDS, universal testing machine, and stereomicroscope were used to record surface roughness Ra, surface morphology, phase transformation, elemental compositions, shear bond strength SBS values, and failure types, respectively. Specimens were investigated in unaged (not immersed in artificial saliva) and aged (stored in artificial saliva for a month) conditions to evaluate SBS values. RESULTS. Grinding and GLN as first and second surface treatments provided satisfactory Ra values in both conditions ($1.05{\pm}0.24{\mu}m$, $1.30{\pm}0.21{\mu}m$) compared to sandblasting and other groups (P<.05). The group GLN showed the highest SBS values in both conditions ($30.97{\pm}3.12MPa$, $29.09{\pm}4.17MPa$), while group SLV recorded the lowest ($23.96{\pm}3.60MPa$, $22.95{\pm}3.68Mpa$) (P<.05). Sandblasting showed phase transformation from t-m. Mixed failure type was the commonest among all groups. CONCLUSION. GLN showed to be a reliable method which provided satisfactory bond strength between the veneer ceramic and zirconia. This method might preserve the integrity of fixed dental crowns.

Chromatographic Separation of Xanthine Derivatives on Single and Mixed-Template Imprinted Polymers

  • Wang, Dexian;Hong, Seung-Pyo;Row, Kyung-Ho
    • Bulletin of the Korean Chemical Society
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    • v.25 no.3
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    • pp.357-360
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    • 2004
  • We developed in the present study molecular imprinted polymers (MIPs), using single templates (pentoxifylline, caffeine and theophylline) and mixed-templates (pentoxifylline-caffeine, pentoxifylline-theophylline and caffeine-theophylline). The MIPs were prepared with methacrylic acid (MAA) as the monomer, ethylene glycol dimetharylate (EGDMA) as the crosslinker and 2,2'-azobis(isobutyronitrile) (AIBN) as the initiator. The obtained polymer particles (particle size after grinding was about 25-35 ${\mu}$m) were packed into a HPLC column (3.9 mm i.d. ${\times}$ 150 mm). The selectivity and chromatographic characteristics of the MIPs were studied using acetonitrile as the mobile phase at a flow rate of 0.8 mL/min. UV detector wavelength was set at 270 nm. Different single template MIPs showed different molecular recognitions to the templates and the structurally analogues, according to the rigidity and steric hindrance of the compounds. Recognition was improved on the mixed-template MIPs as a result of the cooperation or sum effect of the templates, whereas on the pentoxifylline-theophylline imprinted polymer, the highest selectivity and affinity were obtained. Separations of the test compounds on different polymers were also investigated.

A Study on Conservation Materials of the Lacquer Wares : the Tohoe and Goksu (칠기 하지층 충진제의 특성 비교 : 토회와 곡수)

  • Jang, Eun Jeong;Park, Jung Hae;Kim, Soo Chul
    • Journal of Conservation Science
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    • v.31 no.2
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    • pp.125-130
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    • 2015
  • Specific techniques and materials in conservation of traditional lacquer has not been transmitted. This study aims to compare the basic characteristics of the filler which used in the base layer of lacquer conservation. Tohoe(a mixture of lacquer and Clay) and the three kinds of additives which is mixed with Tohoe and Goksu(a mixture of lacquer, wood powder and rice starch) are estimated in drying rate, impact resistance, abrasion. Among those samples, the more amount of clay causes fast dryness speed and worse cracks on the surface. The impact resistance is weakened at high amount of clay. There is no significant differences of impact resistance between both additives that is mixed with the samples and additives. The samples that are mixed with Goksu and additives show high impact resistance. In the polishing test, the more amount of filling powders show higher grinding degree and the sample that are mixed with wood powder and charcoal show higher degree as well. The highest grinding degree is Maekchil and Goksu but the lowest one is the sample of the rooftile powder mixture.

Physicochemical Properties of Non-waxy Rice Flour Affected by Grinding Methods and Steeping Times (제분방법 및 수침시간을 달리한 멥쌀가루의 이화학적 특성)

  • Kim, Rae-Young;Kim, Chang-Soon;Kim, Hyuk-Il
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.38 no.8
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    • pp.1076-1083
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    • 2009
  • The physicochemical properties of rice flour produced by 3 different grinding methods using various steeping times (3, 6, 9, and 12 hrs) were investigated. Roller mill gave coarse rice flour; the pin mill, intermediate flour; and mixed when both (roller & pin mills) were used. With the increase of steeping times, the rice flours became finer and the contents of crude protein, crude fat and crude ash decreased. Damaged starch was noticeably high in rice flour by roller & pin mills compared to those by roller or pin mills alone. Amylose contents, solubility and swelling power increased as the steeping times increased. Water binding capacity was the highest in roller & pin mills, followed by pin mill. In scanning electron microscope (SEM), pin mill showed distribution of separated fine particles of rice flours. The physicochemical properties of rice flours showed many differences by steeping times of rice and grinding methods. With sufficient steeping times, the rice flours obtained from pin mill were relatively fine having less damaged starch.