• 한국환경농학회지
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• 제13권1호
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• pp.76-82
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• 1994

Metalaxyl을 ELISA기법을 이용하여 분석하기 위하여 metalaxyl-HSA를 합성하고 이에 대한 항체를 생산하여 competitive indirect ELISA를 위한 최적조건을 조사하였다. Metalaxyl-protein conjugate는 metalaxyl을 가수분해시켜 생성된 metalaxyl acid에 단백질(HSA, OA)을 mixed anhydride방법이나 EDC 첨가방법으로 조제하였고 생성된 항체의 역가는 1:16,000으로 나타났다. Coating Ag의 최적농도는 $8\;{\mu}g/ml$, 배양시간은 $4\;^{\circ}C$에서 1시간 이상, $20\;^{\circ}C$와 $37\;^{\circ}C$에서는 4시간으로 나타났으며 항체의 희석배수는 1:2,000이 최적으로 나타났다. 항원과 항체의 혼합비율은 0.5 ml의 항원에 대해 1 ml의 항체가 최적이었으며 이 혼합액의 배양시간은 1시간, antirabbit Ig G-peroxidase conjugate의 배양시간은 30분이 최적으로 나타났다.

• Journal of Ceramic Processing Research
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• 제13권spc2호
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• pp.341-345
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• 2012

[Li0.055(K0.5Na0.5)0.945](Nb1-xTax)O3 (0.05 ≤ x ≤ 0.25) ceramics were prepared by the partial sol-gel (PSG) method to improve the microstructure homogeneity of Ta5+ ion and were compared to those prepared by the conventional mixed oxide (CMO) method. For the PSG method, Ta(OC2H5)5 was directly reacted with calcined [Li0.055(K0.5Na0.5)0.945]NbO3 powders and the specimens sintered at 1100 ℃ for 5 hrs showed a single phase with a perovskite structure. Compared to the specimens prepared by conventional mixed oxide powders, the relative ratio of tetragonal phase to orthorhombic phase of the sintered specimens prepared by Ta(OC2H5)5 was larger than that of the sintered specimens prepared by Ta2O5. The electromechanical coupling factor (kp), piezoelectric constant (d33) and dielectric constant (εr) of the sintered specimens were increased with Ta5+ content. These results could be attributed to the decrease of the orthorhombic-tetragonal polymorphic phase transition temperature (To-t), which could be evaluated by oxygen octahedral distortion. Strain of the sintered specimens prepared by the PSG method was higher than that of specimens prepared by the CMO method due to the increase of relative density. The effects of crystal structure on the strain characteristics of the specimens were also discussed.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2009년도 하계학술대회 논문집
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• pp.160-161
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• 2009

In this study, in order to develop the lead free piezoelectric ceramics with excellent piezoelectric properties, (Na,K)$NbO_3$ ceramics according to the amount CuO addition were fabricated using a conventional mixed oxide process and their piezoelectric and dielectric characteristics were investigated. At the 0.8mol% CuO added composition, density, electromechanical coupling factor(kp), echanical quality factor(Qm), dielectric constant$(\varepsilon_r$) and piezoelectric constant($d_{33}$) showed the optimum value of $4.459g/cm^3$, 0.469, 540, 410, 69.57pC/N, respectively.

• 한국전자파학회논문지
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• 제11권7호
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• pp.1204-1210
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• 2000

슬롯 개구를 통해 평향평판 도파관 내부를 결합되어지는 전자파 펄스(EMP)의 과도 응답을 해석하기 위한 방법을 제안하였다. 개구의 미지 등가 면 자기전류밀도에 대한 혼합 포텐셜 적분 방정식(MPIE)을 세웠고 평행평판 도파관 영역에서의 백터 및 스칼라 포텐셜 그린함수를 개선된 북소영상법을 사용하였을 때 closed form 그림함수를 사용한 결과를 계산시간을 현저히 줄일 수 있었고 본 논문이 제안한 방법의 타당성을 확인하기 위해 기존 방법의 해석결과와 비교해 보았을때 본 논문의 해석결과와 비교적 잘 일치함을 알 수 있었다.

• 한국염색가공학회지
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• 제28권4호
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• pp.280-289
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• 2016

Silica microgel was prepared by sol-gel process and then functional groups, epoxy group and ethoxy group, were introduced on the particle by coupling treatment with 3-glysidoxypropyltrimethoxysilane. The functional silica microgel(functional SiGel) formation was identified using FT-IR spectrometry. Phase stability for DMF solution of functional SiGel, PU resin and pigment was evaluated by Turbiscan Lab. And physical properties of artificial suede including hand values, morphology and dyeing fastness were investigated. The mean particle size and the specific surface area of the functional SiGel were $0.77{\mu}m$ and $380m^2/g$. Mixture containing the functional SiGel, PU resin and pigment was more stable than the functional SiGel-free mixed solution. Artificial suede prepared by the functional SiGel had appearance and feeling close to natural suede. The migration fastness, the solvent wicking fastness and rubbing fastness of the artificial suede were enhanced to 4~5 grades, 4~5 grades and 3~4 grades, respectively.

• Transactions on Electrical and Electronic Materials
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• 제15권4호
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• pp.226-229
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• 2014

In this study, lead-free $(Ba_{0.85}Ca_{0.15})(Ti_{1-x}Zr_x)O_3$ ceramics and a bimorph-type piezoelectric actuator were fabricated using the normal oxide-mixed sintering method, and their dielectric properties, microstructure, and displacement properties were investigated. From the results of X-ray diffraction, the pattern of the specimen has a pure perovskite structure. In addition, no secondary impurity phases were found. The excellent piezoelectric coefficient of $d_{33}=454pC/N$, the electromechanical coupling factor $k_p=0.51$, the dielectric constant ${\varepsilon}_r=3,657$, the mechanical quality factor $Q_m=239$, and $T_c$(Tetragonal-Cubic) =$90^{\circ}C$ were shown at x= 0.085. ${\Delta}k_p/k_p20^{\circ}C$ and ${\Delta}f_r/f_r20^{\circ}C$ showed the maximum value of -0.255 and 0.111 at $-20^{\circ}C$ and $80^{\circ}C$, respectively. The maximum total-displacement was $60{\mu}m$ under the input voltage of 50 V. As a result, it is considered that lead-free $(Ba_{0.85}Ca_{0.15})(Ti_{1-x}Zr_x)O_3$ ceramics is a promising candidate for piezoelectric actuator application for x= 0.085.

• Earthquakes and Structures
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• 제15권3호
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• pp.243-251
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• 2018

The dynamic responses of a rocking wall-moment frame (RWMF) with a post-tensioned cable are investigated. The nonlinear equations of motions are developed, which can be categorized as a single-degree-of-freedom (SDOF) model. The model is validated through comparison of the rocking response of the rigid rocking wall (RRW) and displacement of the moment frame (MF) against that obtained from Finite Element analysis when subjected ground motion excitation. A comprehensive parametric analysis is carried out to determine the seismic performance factors of the RWMF systems under near-fault trigonometric pulse excitation. The horizontal displacement of the RWMF system is compared with that of MF structures without RRW, revealing the damping effect of the RRW. Frame displacement spectra excited by trigonometric pulses and recorded earthquake ground motions are constructed. The effects of pulse type, mass ratio, frame stiffness, and wall slenderness variations on the displacement spectra are presented. The paper shows that the coupling with a RRW has mixed results on suppressing the maximum displacement response of the frame.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2002년도 하계학술대회 논문집 Vol.3 No.2
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• pp.556-560
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• 2002

The rheological characteristics of PNN-PZT ceramics with high electromechanical coupling factor and electricstrictive constant was investigated. Green sheets of piezoelectric PNN-PZT ceramics were made by tape-casting method with controlling the mixing ratio of a dispersant, an organic binder, and a plasticizer. When the dispersant content was 1 wt.%, the slurry showed the best rheological characteristics for tape casting. The amounts of the plasticizer and the binder was simultaneously varied in the ranges of 1.5~18 and 3~9 wt.%, respectively. When both the plasticizer and binder of 6 wt.% mixed in the solution, respectiveley, the highest green density of the sheet was obtained without macrodefects. Multilyered structures of PNN-PZT/Ag-Pd were successfully fabricated using the optimized tape casting condition. The polarization behavior of these actuators seemed to similar to typical electricstrictive polarization behavior. The multilayer ceramic actuator is about $0.6{\times}10^{-3}$ of strain.

• 전자공학회논문지 IE
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• 제49권2호
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• pp.24-29
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• 2012

자동차 배기음은 음성과 무관한 거의 독립적인 음원이라고 볼 수 있다. 따라서 자동차 배기음과 섞인 음성 신호의 경우에 두 음원에 대한 사전 정보가 없는 상황이므로 Blind Source Separation 의 한 방법인 Independent Component Analysis를 이용하여 분리해 내었다. 스테레오 마이크를 통해 섞여 들어 온 두 음원을 분리해 내기 위해 Maximum Likelyhood Estimation을 이용하여 각 신호들 사이의 독립성을 최대화 하는 방향으로 분리하였다. 분리된 신호는 어느 쪽이 음성 신호인지 알 수 없으므로 주파수 영역에서 자기 공분산을 구한 후 이 공분산 값들의 기울기를 이용하여 음성 신호와 자동차 배기음 신호을 구분하였으며 이 두 알고리즘을 결합하여 음성 신호 잡음 제거기를 구현하였다.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 1992년도 추계학술대회 논문집
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• pp.38-41
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• 1992

Pb(Zr,Ti)$O_3$ powders were synthesized by the partial oxalate method and the modified partial oxalate method, where the difference between the two is the use of pre-reacted (Zr,Ti)$O_2$ in the former method. When compared with conventional mixed oxide method, calcination temperature can be reduced to less than $700^{\circ}C$ by both partial oxalate methods, and the resulting particle size was finer and more uniform. Using partial oxalate-derived PZT powders, sintering temperatures can also be reduced as low as $950^{\circ}C$ without sacrificing desired dielectric and piezoelectric properties, such as relative permittivity, electromechanical coupling factor, and piezoelectric coefficient. Two partial oxalate methods yield ceramics with almost the same physical and electrical properties, so that the step of producing ZTO powder does not seem to be necessary.