• 한국진공학회:학술대회논문집
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• 한국진공학회 2016년도 제50회 동계 정기학술대회 초록집
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• pp.290.1-290.1
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• 2016

Grapehen, a single atomic layer of graphite, has been in the spotlight and researched in vaious fields, because its fine mechanical, electrical properties, flexibility and transparence. Synthesis methods for large-area graphene such as chemical vaper deposition (CVD) and mechanical, chemical exfoliation have been reported. In particular, chemical exfoliation method receive attention due to low cost process. Chemical exfoliation method require reduction of graphene oxide in the process of exfoliation such as chemical reduction by strong reductant, thermal reduction on high temperature, and optical reduction via ultraviolet light exposure. Among these reduction methods, optical reduction is free from damage by strong reductant and high temperature. However, optical reduction is economically infeasible because the high cost of short-wavelength ultraviolet light sorce. In this paper, we make graphene-oxide and lanthanoid ion mixture aqueous solution which has highly optical absorbency in selective wevelength region. Sequentially, we synthesize reduced graphene oxide (RGO) using the solution and visible laser beam. Concretely, graphene oxide is made by modified hummer's method and mix with 1 ml each ultraviolet ray absorbent Gd3+ ion, Green laser absorbent Tb3+ ion, Red laser absorbent Eu3+ ion. After that, we revivify graphene oxide by laser exposure of 300 ~ 800 nm layser 1mW/cm2 +. We demonstrate reproducibility and repeatability of RGO through FT-IR, UV-VIS, Low temperature PL, SEM, XPS and electrical measurement.

• 한국세라믹학회지
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• 제23권3호
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• pp.9-14
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• 1986

$\beta$-SiC bonded SiC bodies were prepared from various conditions such as several compositions of(Si+C)/$\alpha$ -SiC ratio and different firing schedules and were respectively investigated compressive strength MOR and mi-crostructure. One firing schedule which produced the specimens that had $\beta$-SiC neck form with the highest strength was selected and experimented by each firing temperature. results obtained are as follows : 1) The amount of (Si+C) for th highest MOR of SiC-(Si+C) sintered body is 20wt% 2) By adding 20wt% content of (Si+C) and heating up to 1, 500 with soaking 3hrs respectively at 1,150$^{\circ}C$ 1,250$^{\circ}C$ 1,350$^{\circ}C$ and 1,400$^{\circ}C$ the highest MOR of fired specimen was resulted and its microstructure of ma-trix was composed of close $\beta$-SiC neck. 3) Microstructure of $\beta$-SiC were different greatly from each other by firing time and/or quantity of adding mix-ture and it was confirmed that they were composed of neck particle-like and heterogeneous texture. 4)$\beta$-SiC synthesis proceed rapidly at the temperature between 1,250$^{\circ}C$ and 1,350$^{\circ}C$ 5) All of the properties of 85 SiC-20(Si+C) specimen improved according to increasing temperature above 1,350$^{\circ}C$.

• 한국건축시공학회지
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• 제4권2호
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• pp.113-118
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• 2004

This study is a basic experiment on quality management of the compression strength of high strength concrete, aiming. at quality management of high strength mass concrete by giving the temperature hysteresis of the mass test pieces to managerial test pieces. Different from ordinary concrete, high strength concrete generally shows the temperature high rising caused by hydration heat inside the concrete. It is known that, in mass concrete, thermal stress occurs due to the difference in temperature between the inside and the outside, which causes a significant difference in compression strength between structure beams and managerial test pieces. It is also reported that there is a large difference between the compression strength of cylindrical managerial test pieces of standard underwater curing and the strength of structure beam concrete. Thus, this study made concrete test pieces in an optimal mix ratio for each strength level, and also created thermal insulation curing box and managerial test pieces. Then it carried out comparative analysis in relation to core strength and suggested equipment and a technique that can control the strength of high strength concrete mass more conveniently and accurately.

• 한국농공학회지
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• 제41권5호
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• pp.104-105
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• 1999

This study was performend to examine Poisson's ration of polymer-modified asphalt concrete due to temperature variatino . Asphalt binder used in this study was an AC85-100, penetration grade of 85-100, and polymer for modifying asphalt were domestic LDPE(Low-density polyethylene) and SBS(Styrene-butadiene-styrene). Aggregate was a crushed gneiss which was most widely used in the middle part of Korea. Using these materias, asphalt mixture slab(340mm$\times$240mm$\times$80mm) with optimum asphalt content from mix design was made and cut into square pillar (80mm$\times$80mm$\times$160mm). Poisson's ration was measured in various temperture (-15$^{\circ}C$, -1$0^{\circ}C$, -5$^{\circ}C$,$0^{\circ}C$,5$^{\circ}C$,1$0^{\circ}C$ and 2$0^{\circ}C$) under the load of one axis repeated compression mode. Poisson's ration of normal asphalt polymer modified asphalt mixtures in normal temperatures. This indicated that AP mixture was more susceptible to temperature effects. From regression aalysis of experimental results, the difference of Poisson's ration between normal and low temperature showed that polymer modified asphalt mixture were lower than AP mixture except for SBS modified asplat mixture.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 2008년도 춘계 학술발표회 제20권1호
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• pp.181-184
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• 2008

콘크리트는 비교적 내화성이 있는 재료이다. 그러나 화재 등의 고온에 장기 노출될 경우는 콘크리트 강도 등이 급격하게 저하하는 현상이 발생한다. 이와 같은 경우, 저강도 콘크리트를 일반 비파괴검사 강도추정식을 이용하여 추정하는 것은 적절하지 않다. 이 문제를 해결하기 위해 각종 배합조건의 콘크리트시편을 200, 400, 600, $800^{\circ}C$의 온도변화 조건에서 가열한 후, 초음파속도와 콘크리트강도간의 상관관계를 분석하였다. 아울러 이들 결과를 통해 고온에서 손상된 콘크리트 비파괴검사 강도추정식을 제안하였다.

• 반도체디스플레이기술학회지
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• 제15권1호
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• pp.41-46
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• 2016

In this study, gas flow and temperature distribution in the multi-wafer planetary CVD reactor for the Si epitaxial growth were analyzed. Although the structure of the reactor was simplified as the first step of the study, the three-dimensional analysis was performed taking all these considerations of the revolution of the susceptor and the rotation of satellites into account. From the analyses, a reasonable velocity field and temperature field were obtained. However, it was found that analyses including the upper structure of the reactor were required in order to obtain more realistic temperature results. DCS mole fraction above the satellite surface and the susceptor surface without satellite was compared in order to check the gas species mixing. We found that satellite rotation helped gases to mix in the reactor.

• Tribology and Lubricants
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• 제37권2호
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• pp.41-47
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• 2021

An experimental device was developed for analysis of hydraulic oil characteristics with dielectric constant sensors. Online analysis is the most effective method of the three methods used for analyzing lubricant oils. This is because it can monitor the machine condition effectively using oil sensors in real time without requiring excellent analysis skill and eliminates human errors. Determining the oil quality usually requires complex laboratory equipment for measuring factors such as density, viscosity, base number, acid number, water content, additive, and wear debris. However, the electric constant is another indicator of oil quality that can be measured on-site. The electric constant is the ratio of the capacitance of a capacitor using that material as a dielectric, compared with a similar capacitor that has a vacuum as its dielectric. The electric constant affects the factors such as the base oil, additive, temperature, electric field frequency, water content, and contaminants. In this study, the tendency of the electric constant is investigated with a variation of temperature, water content, and dust weight. The experimental device can control working temperature and mix the contaminants with oil. A machine condition monitoring program developed to analyze hydraulic oil is described. This program provides graph and digital values with variation of time. Moreover, it includes an alarm system for when the oil condition is bad.

• 콘크리트학회지
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• 제8권3호
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• pp.197-207
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• 1996

성숙도는 콘크리트의 양생 온도이력에서 구해지는 것으로 초기강도 예측을 위한 하나의 유용한 지표가 될 수 있다. 즉 성숙도 이론은 배합이 동일할 때 성숙도 값이 같으면 강도값은 같다는 이론이다. 본 연구에서는 성숙도 법칙의 이론적 전개과정을 살펴보고 그 값을 계산하기 위하여 가장 널리 알려진 Nurse-Saul함수를 검토하였다. 또한 성숙도 함수와 기준온도(datum temperature) 설정을 위한 일련의 포괄적인 실험연구를 수행하였다. 성숙도를 강도값에 연관시키기 위한 여러 가지 성숙도-강도함수를 비교해보고 그 장단점을 분석해 보았으며 이를 통하여 유용한 강도예측함수를 제안하였다. 성숙도 이론의 적용에 있어서 고려해야 할 변수들을 도출하기 위하여 양생조건과 시멘트의 종류, 그리고 물-시멘트비등을 달리 하였으며 이 경우에는 습도나 초기양생온도 등이 변수로 채택되었다. 마지막으로 제안된 함수의 타당성과 정확성을 검증하기 위하여 콘크리트 슬래브를 타설하고 시간단계별로 콘크리트 코아를 채취하여 예측된 강도값과 비교하여 보았다. 본 논문은 실제 콘크리트 구조물의 초기강도 예측을 위해 매우 유용할 것으로 사료되며 현장품질관리에 효율적으로 활용할 수 있을 것으로 기대된다.

• 한국식품영양과학회지
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• 제42권11호
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• pp.1848-1856
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• 2013

녹차, 토마토, 호박가루 첨가와 사출구 온도, $CO_2$ 가스 주입에 따라 압출성형물의 물리적 특성에 미치는 영향을 분석하기 위해 비기계적에너지, 팽화특성, 기계적 특성, 색도, 수분용해지수와 수분흡착지수, 미세구조를 분석하였다. 수분함량 27%, 스크루 회전속도 100 rpm, 원료 사입량 100 g/min, 사출구 3 mm 원형으로 고정하였고, 사출구 온도(60, 80, $100^{\circ}C$), $CO_2$ 가스 주입량(0, 150 mL/min)으로 조절하였다. 원료는 알파현미 25%, 현미가루 50%와 당류 16%에 녹차, 토마토, 호박을 각각 9%씩 혼합하여 사용하였다. 비기계적 에너지 투입량은 사출구 온도 $100^{\circ}C$, $CO_2$ 가스 주입량 150 mL/min, 호박가루를 첨가했을 때 52.67 kJ/kg으로 가장 낮은 비기계적 에너지 투입량을 나타내었다. $CO_2$ 가스를 주입하지 않은 경우 사출구 온도는 직경팽화율에 큰 영향을 주지 않았으나 직경팽화율은 $60^{\circ}C$에서 $CO_2$ 가스를 주입함에 따라 증가하였다. $CO_2$ 가스 주입량이 증가할수록 비길이는 증가하는 경향을 나타냈으며, 녹차 첨가 시 사출구 온도와 $CO_2$ 가스 주입량이 증가할수록 밀도는 감소하는 경향을 나타내었다. 특히 사출구 온도 $60^{\circ}C$에서 $CO_2$ 가스 주입 시 $100^{\circ}C$에서 $CO_2$ 가스를 주입하지 않을 때와 비슷한 기공의 크기와 수를 보여주었다. 모든 사출구 온도에서 $CO_2$ 가스 주입시 파괴력은 감소하였다. 수분용해지수는 사출구 온도증가 시 감소하고 $CO_2$ 가스 주입 시에는 증가하는 경향을 나타내었으며, 수분흡착지수는 사출구 온도와 $CO_2$ 가스 주입량이 증가할수록 증가하였다. 사출구 온도 $60^{\circ}C$에서 $CO_2$ 가스 주입을 통한 저온 압출성형은 생식 제조에 적용할 수 있는 가능성을 나타내고 있다.

• 한국주조공학회지
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• 제40권2호
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• pp.16-24
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• 2020

The effect of a heat treatment on the microstructure and mechanical properties of Inconel 713C alloy vacuum investment castings were investigated. The microstructure of the as-cast state was observed, showing well-developed dendrite structures and distributed carbide particles and solidified massive precipitates in the grain or grain boundary during solidification, in this case the γ′ phase and MC particles. During a heat treatment, the γ phase matrix was reinforced by solid solution elements, carbide particles from the film morphology precipitated along the grain boundary, and many micro-precipitates of second γ′ phases 0.2 ㎛~2 ㎛ in size were newly formed in the γ phase matrix according to SEM-EDS analysis results. The tensile strength at a high temperature (850℃) decreased slightly becoming comparable with the room-temperature result, while the hardness value of the specimen after the vacuum heat treatment increased by approximately 19%, becoming similar to that of the as-cast condition. However, the impact values at room temperature and low temperature (-196℃) were approximated; this alloy was mostly not affected by an impact at a low temperature. In the observations of the fracture surface morphologies of the specimens after the tensile tests, the fractures at room temperature were a mix of brittle and ductile fractures, and an intergranular fracture in the inter-dendrite structure and some dimples in the matrix were observed, whereas the fractures at high temperatures were ductile fractures, with many dimples arising due to precipitation. It was found that a reinforced matrix and precipitates of carbide and the γ′ phase due to the heat treatment had significant effects, contributing greatly to the excellent mechanical properties.