• Proceedings of the Korean Nuclear Society Conference
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• 1997.05b
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• pp.189-194
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• 1997

니켈기 전열관 소재에서 결정립계의 misorientation을 분석하였다. 일반적으로 대부분의 결정립계에서 석출물을 관찰 할 수 있지만 쌍정과 만나게 되면서 석출물의 분포가 갑작스럽게 변하는 것을 관찰 할 수 있다. 이러한 현상은 결정립계의 구조와 에너지에 관련되는 결정립계의 misorientation 특성에 갑작스런 변화가 생겨나기 때문이라. 이러한 결정립계의 misorientation 특성은 T.E.M (Transmission Electro Microscope)에서 얻은 각 결정립의 Kikuchi pattern을 이용하여 분석하었다. 석출물을 갖는 결정립계들은 random high angle 결정립계이고 석출물이 존재하지않는 결정립계들은 특정한 C.S.L ( Coincidence Site Lattice) 결정립계이었다.

• Korean Journal of Metals and Materials
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• v.46 no.9
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• pp.554-562
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• 2008

The distribution and prediction interval for the misorientation angle of grain boundary at which $Cr_2N$ was precipitated during heating at $900^{\circ}C$ for $10^4$ sec were newly estimated, and followed by the estimation of mathematical and median rank methods. The probability density function of the misorientation angle can be estimated by a statistical analysis. And then the ($1-{\alpha}$)100% prediction interval of misorientation angle obtained by the estimated probability density function. If the estimated probability density function was symmetric then a prediction interval for the misorientation angle could be derived by the estimated probability density function. In the case of non-symmetric probability density function, the prediction interval could be obtained from the cumulative distribution function of the estimated probability density function. In this paper, 95, 99 and 99.73% prediction interval obtained by probability density function method and cumulative distribution function method and compared with the former results by median rank regression or mathematical method.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 1993.10a
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• pp.660-665
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• 1993

An elastic model is developed to predict the average thermal residual stresses in the matrix and fiber of a misoriented short fiber composite. The thermal residual stresses are induced by the mismatch in the coefficient of the thermal expansion of the matrix and fiber when the composite is subjected to a uniform temperature change. The model considers two special cases of fiber misorientation ; two-dimensional in-plane and three-dimensional axisymmetric. The analytical formulation of the model is based on Eshelby's equivalent inclusion method and is nuque in that it is able to account for interactions among fibers. The model is more general than past models and it is able to treat prior analyses of the simpler composite systems as extram cases. The present model is to investigate the effects of fiber volume fraction, distribution type, distribution cut-off angle, and aspect ratio on thermal residual stress for both in-plane and axisymmetric fiber misorientation. Fiber volum fraction, aspect ratio, and disturbution cut-off angle are shown to have more significant effects on the magnitude of the thermal residual stress than fiber distrubution type for both in-plane and axisymmetric misorientation.

• 한국초전도학회:학술대회논문집
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• v.10
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• pp.99-102
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• 2000

We have studied the effects of d-wave symmetry on the critical current of YBa$_2$Cu$_3$O$_7$ step-edge Josephson junctions. The critical current along various misorientation angle was measured and analyzed with the concept of grain-boundary junctions with d-wave symmetry. Experimental results of c-oriented YBCO step-edge junctions with various in-plane misorientation angles were qualitatively in good agreement with the theory. The out-of-plane misorientation angle is usually formed between two grains with the c axes perpendicular to each other and is normally not controllable.

• Journal of the Korean Society for Nondestructive Testing
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• v.5 no.2
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• pp.34-41
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• 1986

The ultrasonical characteristics of inclined planar reflectors is investigated by the maximum amplitude method. The reflected ultrasound is varied by the reflector size, shape, inclination and using transducers. It was found that the detecting ability for planar reflectors was decreased with increasing transducer size and misorientation angle and increased with decreasing ultrasonic frequency, also the misorientation angle of planar reflectors affected significantly for the measurement of refklector size.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2003.05a
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• pp.49-52
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• 2003

The effects of nitrogen on the deformation behavior of duplex stainless steel have been studied The variation of strength was correlated with the characteristic microstructures. Analysis based on Hall-Petch relation confirmed that nitrogen enhances phase-boundary strengthening effect. The evolution of dislocation structure, slip traces, and misorientation distribution during deformation were also characterized to elucidate the effect of nitrogen on inelastic deformation mechanism.

• Journal of Welding and Joining
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• v.20 no.5
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• pp.93-98
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• 2002

The effect of bonding misfit on single crystallization of transient liquid phase (TLP) bonded joints of single crystal superalloy CMSX-2 was investigated using MBF-80 insert metal. The bonding misfit was defined by (100) twist angle (rotating angle) at bonded interface. TLP bonding of specimens was carried out at 1523K for 1.8ks in vacuum. The post-bond heat treatment consisted of the solution and sequential two step aging treatment was conducted in the Ar atmosphere. The crystallographic orientation analysis across the TLP bonded joints was conducted three dimensionally using the electron back scattering pattern (EBSP) method. EBSP analyses f3r the bonded and post bonded heat treated specimens were conducted. All bonded joints had misorientation centering around the bonded interface for as-bonded and post-bond heat treated specimens with rotating angle. The average misorientation angle between both solid phases in bonded interlayer was almost identical to the rotating angle at bonded interface. HRTEM observation revealed that the atom arrangement of both solid phases in bonded interlayer was quite different across the bonded interface. It followed that grain boundary was formed in bonded interface. It was confirmed that epitaxial growth of the solid phase occurred from the base metal substrates during TLP bonding and single crystallization could not be achieved in joints with rotating angle.

• 한국전자현미경학회:학술대회논문집
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• 1993.06a
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• pp.33-33
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• 1993

• Proceedings of the Computational Structural Engineering Institute Conference
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• 2009.04a
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• pp.38-41
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• 2009

Debonding behavior of symmetric tilt bicrystal interfaces with <100> misorientation axis is investigated through molecular dynamics simulations. FCC single crystal copper is considered in each grain and the model is idealized as a grain boundary under mechanical loading. Embedded-Atom Method potential is chosen to calculate the interatomic forces between atoms. Constrained tensile deformations are applied to a variety of misorientation angles in order to estimate the effect of grain boundary angle on local peak stress. A new parameter of symmetric grain-boundary structure is introduced and refines the correlation between grain boundary angle and local peak stress.

• Proceedings of the Computational Structural Engineering Institute Conference
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• 2011.04a
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• pp.269-272
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• 2011

새로운 재료의 개발과 사용 중인 기존재료의 손상을 판단하기 위해서 변형 중 재료 거동을 정확히 파악하는 것이 중요하다. 하지만, 대부분의 공학 재료는 다결정으로 이루어져 결정 상호작용의 규명이 복잡하여 정밀한 분석이 어렵다. 고에너지 X-ray 회절실험법을 이용한 다결정 고체 거동의 측정기법이 발전함에 따라 해석을 통한 실험법의 검증 및 추가 분석 방법에 대해서도 연구가 활발히 진행되고 있다. 본 연구에서는 특정 결정과 주변 결정 간의 결정간 방위차(intergranular misorientation)의 상호작용에 의한 결정 거동 영향을 조사하였다. 결정간 방위차를 정의하고 결정 응력 방향 변화를 단결정 항복면 꼭지점과 방향과 비교함으로써 결정간 방위차의 변화에 대한 결정 응력 변화를 분석하였다. 소성 발생이 증가함에 따라 결정 응력의 방향은 단결정 항복면 꼭지점으로 이동하지만 결정간 방위차에 의해서 응력 분포가 변화함을 정량적으로 확인하였다.