• Title/Summary/Keyword: Microwave process

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Study of Enhancing Dye Affinity of Fabric using Microwave

  • Kim, Ji-Hyun;Choi, In-Ryu
    • The International Journal of Costume Culture
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    • v.13 no.1
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    • pp.62-66
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    • 2010
  • Of all the ways that energy is consumed within textile industry, few are as high energy-expending as dyeing process. The energy consumption in dyeing process amounts to 77% of total fuel consumption, 54% of total electricity use. A technical development in terms of efficient saving energy and time as well is required in the process of dyeing textiles. Recently, dyeing experts are investigating new technologies can conserve energy grafting into microwaves, radio waves, infrared lights, etc. Dyeing industry in Korea, however, the research related to energy conservation has been rarely conducted. Accordingly, this study aims to examine the possibility where especially microwaves could be applied to reduce the energy use and enhance dyeing process skill. This study performs the experiment in which microwave is employed as heating condition in dyeing and figures out as color yield being promoted, bathochromic effect would be achieved. Applying microwaves in dyeing process is expected to lower the carbon emission, energy and time wasted, ultimately exalt economic efficiency.

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The Change of Ginsenoside Composition in American Ginseng (Panax quinquefolium) Extract by the Microwave and Vinegar Process (서양삼 추출물의 초단파 및 식초 처리에 의한 인삼 사포닌 성분 변화)

  • Jo, Hee Kyung;Gwak, Hyeon Hui;Im, Byung Ok;Cho, Soon Hyun;Ko, Sung Kwon
    • Korean Journal of Pharmacognosy
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    • v.45 no.2
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    • pp.107-112
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    • 2014
  • The purpose of this study is to develop a new preparation process of American ginseng (Panax quinquefolium) extract featuring high concentration of ginsenoside $Rg_3$, $Rg_5$, and $Rk_1$, Red ginseng special components. Chemical transformation from ginseng saponin glycosides to prosapogenin was analyzed by the HPLC. Extracts of American ginseng were processed under several treatment conditions of microwave and vinegar (about 14% acidity). The results showed that the quantity of ginsenoside $Rg_3$ increased by over 0.9% at the 20 minutes of the pH 2~4 vinegar and microwave American ginseng ethanol extract compared with other process times. The result of MAG-20 indicates that the American ginseng microwave and vinegar-processed American ginseng extracts (about 14% acidity) treated for 20 minutes produced the highest amount of ginsenoside $Rg_3$ (0.969%), $Rg_5$ (1.071%), and $Rk_1$ (0.247%). Besides, MAG-15 indicates that the microwave - and vinegar-processed American ginseng extracts (about 14% acidity) treated for 15 minutes produced the highest amount of ginsenoside $Rg_3$ (0.772%), $Rg_5$ (1.330%), and $Rk_1$ (0.386%). This indicates that American ginseng treated with microwave and vinegar had the quantity of the ginsenoside $Rg_3$ over 32 times the amount of the ginsenoside $Rg_3$ (which was not found in raw and American ginsengs) in the average commercial Red ginseng.

The Synthesis of Hydrated Aluminum Sulfate from Kaolin Using Microwave Energy (카올린으로부터 마이크로파 에너지를 이용한 무기고분자인 수화 황산 알루미늄의 합성)

  • Park, Seong Soo;Hwang, Eun Hee;Park, Hee Chan
    • Applied Chemistry for Engineering
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    • v.9 no.4
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    • pp.481-485
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    • 1998
  • Hydrated aluminum sulfate, an inorganic polymer, was synthesized from kaolin in $H_2SO_4$ solution using microwave energy. The maximum rates of alumina extracted from calcined kaolin were 72.8% in a conventional process ($80^{\circ}C$, 1M, and 180min) and 99.9% in a microwave process ($90^{\circ}C$, 1M, and 60 min). Compared with the conventional one, the hydrated aluminum sulfate synthesized under the microwave process had layer structure consisting of plate-shaped large grains. After synthesis and then calcination at $1100^{\circ}C$, both products on conventional and microwave processes were ${\gamma}-Al_2O_3$ with agglomerated powders of spherical shape. The specific area of the products in conventional and microwave processes were 113.5 and $106.6m^2/g$, and their average grain sizes were 46.5 an $26.3{\mu}m$, respectively.

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Characteristics of Microwave-Assisted Drying of Plant Cells of Taxus chinensis for Moisture Removal (수분 제거를 위한 식물세포 Taxus chinensis의 마이크로웨이브를 이용한 건조 특성)

  • Nam, Hyeon-Woo;Kim, Jin-Hyun
    • Applied Chemistry for Engineering
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    • v.31 no.2
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    • pp.208-214
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    • 2020
  • In this study, the characteristics and mechanism of microwave-assisted drying were investigated to improve the efficiency of the storage and extraction of biomass through the removal of moisture from plant cell Taxus chinensis. The efficiency of microwave-assisted drying increased with increasing microwave power. When the experimental data were fitted to typical drying kinetic models, the page and modified Page models were the most appropriate. The microwave-assisted drying was determined to be a spontaneous endothermic process, and randomness increased during the drying process. The effective diffusion coefficient (3.445 × 10-9~7.163 × 10-7 ㎡/s) and mass transfer coefficient (3.1529 × 10-5~1.2895 × 10-2 m/s) increased with increasing microwave power. The small Biot number (0.3890~0.7198) indicated that the mass transfer process was externally controlled.

Applicability on Microwave Technology to the Remediation of PAHs(Polynuclear Aromatic Hydrocarbons) Contaminated Soil (PAHs(Polynuclear Aromatic Hydrocarbons)에 오염된 토양 회복공정으로서 마이크로파의 적용성 검토연구)

  • 문경환;변자진;김덕찬
    • Journal of environmental and Sanitary engineering
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    • v.13 no.3
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    • pp.102-112
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    • 1998
  • The fate of polynuclear aromatic hydrocarbons(PAMs) in soil has drawn increasing concern due to their toxic, carcinogenic, and mutagenic effects. These compounds have been most commonly carried into the soil in solvent, as in a coal tar or cresote. This study has been focused on the applicability of microwave treatment of soils contaminated by PAHs. Studies have been conducted with soil(particle diameter $150~500{\mu}m$), which was spiked with naphthalene, acenaphthene, fluorene, anthracene and pyrene, with different moisture contents. According to the results of the research, up to 95% removal efficiency of naphthalene was observed in 10% moisturized soil for five minutes microwave inducing And the removal efficiency of acenaphthene and fluorene were observed to be 88.9%, 67.2% in 30% moisturized soil, respectively. Due to the low vapor pressure, anthracene and pyrene showed the low removal efficiency. In case the powdered activated carbon was added to the soil as a sensitizer, anthracene and pyrene were decomposed into a various by-products. Decomposition rates of anthracene and pyrene were increased with incresing addition of a PAC to the soil. It is concluded that the developement of a microwave process to remediate soils contaminated with PAHs is foreseeable. But additional studies are also needed regarding continuous microwave heating process.

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Study on the Preparation of Alumina Powders used os a Rubber Filler with a Microwave Extraction System (마이크로파에 의한 고무용 충전제로서의 Alumina Powder의 제조에 관한 연구)

  • Park, Chan-Young;Hwang, Eun-Hee;Han, Seong-Kee
    • Elastomers and Composites
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    • v.33 no.3
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    • pp.201-209
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    • 1998
  • Alumina powders used as a filler in rubber compounding was extracted from kaolin in $H_2SO_4$ solution employing conventional thermal and microwave energy resources. Maximum degrees of alumina extraction from kaolin were 72.8% at $80^{\circ}C$, 1M $H_2SO_4$, and 180min in the conventional thermal extraction process and were 99.0% at $90^{\circ}C$, 1M $H_2SO_4$,, and 60min in the microwave extraction one, respectively. The samples synthesized in both processes were analyzed by means of TG/DTA, XRD, SEM, Atomic Emission Spectroscopy, and BET method. Studies are presently under way to unravel the basic interaction mechanisms between microwave and alumina power for high rates of alumina extraction from kaolin in the microwave ex-traction process.

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One-step microwave synthesis of surface functionalized carbon fiber fabric by ZnO nanostructures

  • Ravi S. Rai;Vivek Bajpai
    • Advances in nano research
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    • v.14 no.6
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    • pp.557-573
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    • 2023
  • The rapid growth of zinc-oxide (ZnO) nanostructures (NSs) on woven carbon fiber (WCF) is reported in this study employing a microwave-aided chemical bath deposition process. The effects of different process parameters such as molar concentration, microwave duration and microwave power on morphologies and growth rate of the ZnO on WCF were studied. Furthermore, an attempt has been taken to study influence of different type of growth solutions on ZnO morphologies and growth rates. The surface functionalization of WCF fabrics is achieved by successful growth of crystalline ZnO on fiber surface in a very short duration through one-step microwave synthesis. The morphological, structural and compositional studies of ZnO-modified WCF are evaluated using field-emission scanning electron microscopy, X-ray diffraction and energy dispersive X-ray spectroscopy respectively. Good amount of zinc and oxygen has been seen in the surface of WCF. The presence of the wurtzite phase of ZnO having crystallite size 30-40 nm calculated using the Debye Scherrer method enhances the surface characteristics of WCF fabrics. The UV-VIS spectroscopy is used to investigate optical properties of ZnO-modified WCF samples by absorbance, transmittance and reflectance spectra. The variation of different parameters such as dielectric constants, optical conductivity, refractive index and extinction coefficient are examined that revealed the enhancement of optical characteristics of carbon fiber for wide applications in optoelectronic devices, carbon fiber composites and photonics.

Microwave Dielectric Properties of Low-temperature Sintered $MgCo_2(VO_4)_2$ Ceramics Synthesized by Sol-Gel process (졸-겔 공정에 의해 제조된 저온소결 $MgCo_2(VO_4)_2$ 세라믹스의 마이크로파 유전특성)

  • Lee, Ji-Hun;Bang, Jae-Cheol
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.06a
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    • pp.288-289
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    • 2006
  • We studied the effect of sol-gel processing and sintering temperature on the microwave properties of $MgCo_2(VO_4)_2$ system(MCV) which is applicable to LTCC(low-temperature cofired ceramics). The MCV was synthesized by sol-gel process using solution that contains precursor molecules for Mg, Co, and V. SEM analysis shows that the average particle size is ${\sim}1{\mu}m$ and size distribution is very uniform compared to the one prepared by conventional solid-state reaction process. Highly dense samples were obtained at the sintering temperature range of $750^{\circ}C{\sim}930^{\circ}C$. The maximum $Q{\times}f_0$ value of 55,700GHz, dielectric constant(${\varepsilon}_r$) of 10.41 and temperature coefficient(${\tau}_f$) of $-85ppm/^{\circ}C$ was obtained at the sintering temperature of $930^{\circ}C$. The superior microwave properties of sol-gel processed MCV relative to conventional solid-state reaction processed one is remarkable especially at lower sintering temperatures such as $750^{\circ}C$ and $800^{\circ}C$.

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Changes in ginsenoside composition of ginseng berry extracts after a microwave and vinegar process

  • Kim, Shin-Jung;Kim, Ju-Duck;Ko, Sung-Kwon
    • Journal of Ginseng Research
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    • v.37 no.3
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    • pp.269-272
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    • 2013
  • MGB-20 findings show that the ginseng berry extracts that had been processed with microwave and vinegar for 20 min peaked in the level of ginsenoside Rg2 (2.28%) and Rh1 (1.28%). MGB-1 peaked in the level of ginsenoside Rg3 (1.13%) in the ginseng berry extract processed with microwave and vinegar for 1 min.

Effects of Ceramic Coating for Microwave Blanching on Vegetables (전자레인지의 Ceramic Coating이 채소류의 마이크로파 데치기에 미치는 영향)

  • Kum, Jun-Seok;Han, Ouk
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.25 no.6
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    • pp.951-957
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    • 1996
  • Changes in quality of blanched vegetables(carrot, green onion, spinach) by microwave heating were evaluated. Ceramic coating treatment(CCT) within microwave oven caused the reduction of blanching time and Hunter's L, a, b values of vegetables. Also, CCT showed the higher cutting force compared to NCCT after microwave heating. Photomicrographs of cross-section of blanched vegetables after heating in ceramic coated microwave oven showed better appearance than those in nonceramic coated microwave oven. CCT process improved retention of vitamin C.

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