• Title/Summary/Keyword: Microwave heat

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Effect of Microwave Vacuum Heating on Inactivation of Enzymes (마이크로파 진공가열방법이 효소의 불활성화에 미치는 영향)

  • Moon, Eun-Kyung;Han, Ki-Young;Kim, Suk-Shin;Kim, Sang-Young;Noh, Bong-Soo
    • Korean Journal of Food Science and Technology
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    • v.29 no.2
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    • pp.284-291
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    • 1997
  • Microwave vacuum heating method (2450 MHz) was used for a low intensity of heat treatments. High vacuum under the microwave heating could bring low temperature condition. Inactivation of ${\alpha}-amylase,\;{\beta}-amylase$, glucoamylase and peroxidase by microwave vacuum heating were investigated at 60-$80^{\circ}C$. It was compared with conventional heating. The heating condition of microwave vacuum heating was confirmed by the destruction of ascorbic acid. When thermal inactivations of the enzymes by microwave vacuum heating were determined, it was less effective than that of conventional method at the initial stage of heating. It was due to a lag time of microwave heating. However, the heating time for complete inactivation of the enzymes by microwave vacuum heating could be reduced comparing with that of conventional heating. Optimum conditions for inactivation of the enzymes could be obtained by microwave vacuum heating.

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Microwave sintering of Fly Ash substituted body (석탄회가 첨가된 점토의 마이크로파를 이용한 소결)

  • 김석범;한정환;김유택
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.8 no.3
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    • pp.513-517
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    • 1998
  • Fly ashes mixed with clay as 70:30 weight percent were sintered by microwave energy and a 2.45 Ghz kitchen model microwave oven was used. Samples were sintered at $1,150^{\circ}C$ and kept at that temperature up to 50 minutes by 10 minutes intervals. Microstructures were taken by Scanning Electron Microscope (SEM) and Energy Dispersive Spectrometry (EDS) analysis of a raw fly ash was taken. X-ray diffraction analysis was done, and compressive strengths and apparent densities were measured. Pore sizes of the samples became smaller as time passed by, but compressive strengths and apparent densities did not change much. Numerical analysis on the microwave heated system was carried out in order to figure out heat transfer phenomena in the cavity.

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Study of Space Charge of Metal/copper(Ⅱ)-phthalocyanine Interface (금속/copper(Ⅱ)-phthalocyanine 계면에서의 Space Charge 연구)

  • Park, Mie-Hwa;Yoo, Hyun-Jun;Yoo, HyungKun;Na, Seunguk;Kim, Sonshui;Lee, Kie-Jin
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.18 no.4
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    • pp.350-356
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    • 2005
  • We report the space charge and the surface potential of the interface between metal and copper(Ⅱ)-phthalocyanine(CuPc) thin films by measuring the microwave reflection coefficients S/sub 11/ of thin films using a near-field scanning microwave microscope(NSMM). CuPc thin films were prepared on Au and Al thin films using a thermal evaporation method. Two kinds of CuPc thin films were prepared by different substrate heating conditions; one was deposited on preheated substrate at 150。C and the other was annealed after deposition. The microwave reflection coefficients S/sub 11/ of CuPc thin films were changed by the dependence on grain alignment due to heat treatment conditions and depended on thickness of CuPc thin films. Electrical conductivity of interface between metal and organic CuPc was changed by the space charge of the interface. By comparing reflection coefficient S/sub 11/ we observed the electrical conductivity changes of CuPc thin films by the changes of surface potential and space charge at the interface.

Study of space charge of metal/copper(II)-phthalocyanine interface (금속/copper(II)-phthalocyanine interface에서의 space charge 연구)

  • Park, Mie-Hwa;Lim, Eun-Ju;Yoo, Hyun-Jun;Lee, Kie-Jin;Cha, Deok-Joon;Lee, Young-San
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2004.11a
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    • pp.526-530
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    • 2004
  • We report the space charge and the surface potential of the interface between metal and CuPc according to isotropic property and different metal by measuring the microwave reflection coefficients $S_{11}$ of copper(II)-phthalocyanine(CuPc) thin films by using a near-field microwave microscope(NSMM) in order to understand. CuPc thin films were prepared on gold and aluminium substrates using a thermal evaporation method. Two kinds of CuPc thin films were prepared. One was deposited on preheated substrate at $150^{\circ}C$ and the other was annealed after deposition by using thermal evaporation methods. The microwave reflection coefficients $S_{11}$ of CuPc thin films were changed by the dependence on the heat treatment conditions. By comparing reflection coefficient $S_{11}$ we measured electrical conductivity of CuPc thin films and studied this results with respect to the surface potential and space charge of the interface between metal and CuPc thin films.

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Analysis of Decontamination from Concrete by Microwave Power

  • Zi, Goang-Seup
    • Proceedings of the Korea Concrete Institute Conference
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    • 2004.11a
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    • pp.603-608
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    • 2004
  • The paper analyzes a scheme of decontamination of radionuclides from concrete structures, in which rapid microwave heating is used to spall off a thin contaminated surface layer. The analysis is split in two parts: (1) The hygrothermal part of the problem, which consists in calculating the evolution of the temperature and pore pressure fields, and (2) the fracturing part, which consists in predicting the stresses, deformations and fracturing. The rate of the distributed source of heat due to microwaves in concrete is calculated on the basis of the standing wave normally incident to the concrete wall with averaging over both the time period and the wavelength because of the very short time period of microwaves compared to the period of temperature waves and the heterogeneity of concrete. The reinforcing bars parallel to the surface arc treated as a smeared steel layer. The microplane model M4 is used as the constitutive model for nonlinear deformation and distributed fracturing of concrete. The aim of this study is to determine the required microwave power and predict whether and when the contaminated surface layer of concrete spalls off. The effects of wall thickness, reinforcing bars, microwave frequencies and power are studied numerically. As a byproduct of this analysis, the mechanism of spalling of rapidly heated concrete is clarified.

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Sterilization Effectiveness by Nominal and Absolute Filter in Pre-treatments of Honey (벌꿀의 전처리 공정 중 Nominal 및 Absolute Filter 적용을 통한 제균 효과에 관한 연구)

  • Kwon, Ki-Hyun;Cha, Hwan-Soo;Kim, Byeong-Sam;Sung, Jung-Min
    • Food Science and Preservation
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    • v.15 no.5
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    • pp.731-735
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    • 2008
  • The coliform group, Salmonella typhimurium and Staphylococcus were analyzed for eliminating of microorganism spore which could be embeded in honey and eradication of studied for heat resistance of thermoacidophilic bacteria was studied for marketing of honey after producing honey drink. The method for analyzing of heat resistance thermoacidophilic bacteria was membrane-seperated cell culture with $0.45\;{\mu}m$ micro-filter and vacuum aspirator. The results of bacteria, coliform group, Salmonella typhimurium and Staphylococcus was negative, but normal method such as sterilization with electrolyzed water, normal micro-filter, high-temperature heating and microwave did not have effect on heat resistance thermoacidophilic bacteria. Also, absolute type micro-filter of $0.45\;{\mu}m$ and $0.8\;{\mu}m$ microfilteration showed higher effect on heat resistance thermoacidophilic bacteria than micro-filter of normal type, showing negative results at all treatments.

Comparative Study of Properties of Dental Zirconia According to Microwave Sintering Method (마이크로웨이브 소결방법에 따른 치과용 지르코니아의 물리적 특성)

  • Kim, Tae-Suk;Yu, Chin-Ho;Kim, Gi-Chul;Park, Won-Uk;Seo, Jung-Il;Hwang, Kyu-Hong
    • Journal of Technologic Dentistry
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    • v.34 no.1
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    • pp.11-21
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    • 2012
  • Purpose: Densification and mechanical properties of dental zirconia ceramics were evaluated by different sintering methods. Materials and Methods: Y-TZP zirconia block(Kavo $Everest^{(R)}$ ZS blank, Kavo dental GmbH, Bismarckring, Germany) was used in this study. Sintering were performed in heat sintering furnace and microwave sintering furnace, and then experimented and analyzed on a change in densification according to the sintering time, a change in densification according to thickness, flexural strength and micro-structure in zirconia specimens. Results: Microwave sintering was very effective in considerable mechanical properties such as flexural strength and bulk density was drastically increased than conventional electric heating method. It is also shown that microwave sintering time was faster and more economical than common method to be present in qualities which equal or exceed. Conclusion: It will be important to seek the accurate sintering condition of dental zirconia by microwave sintering method and the continuous research is necessary for the study of relationship between sintering methods and mechanical properties.

Microwave Sintering of Silver Thick Film on Glass Substrate (유리기판 위에 Ag 후막의 마이크로웨이브 소결)

  • Hwang, Seong-Jin;Veronesi, Paolo;Leonelli, Cristina;Kim, Hyung-Sun
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2009.06a
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    • pp.22-22
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    • 2009
  • The silver thick film has been used in many industries such as display, chip, solar cell, automobile, and decoration with conventional heating. The silver thick film is fired with optimal time and temperature. However, decreasing the fabrication time is required due to high production power. Furthermore, there is a problem that silver in electrode is diffused throughout any substrates. For inhibiting the Ag diffusion and long fabrication time we considered a microwave heating. We investigated firing of silver thick film with conventional and microwave heating. The temperature of substrate was measured by thermal paper and the temperature of substrate was under $100\;^{\circ}C$ The shrinkage of electrode was measured with optical microscopy and optical profilometry. The shrinkage of electrode heat treated with microwave for 5min was similar to the that fired by the conventional heating for several hours. After firing by two types of heating, the diffusion of silver was determined using a optical microscope. The microstructure of sintered silver thick film was observed by SEM. Based on our results, the microwave heating should be a candidate heating source for the fabrication electronic devices in terms of saving the tact time and preventing the contamination of substrate.

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Microwave Cooking of Rice - The Optimum Condition of Power Level and Heating Time - (Microwave Oven을 이용한 취반에 관한 연구 -출력 및 가열시간의 최적화-)

  • Kim, Young-A;Kim, Hyun-sook
    • Korean journal of food and cookery science
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    • v.14 no.1
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    • pp.44-49
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    • 1998
  • The microwave cooking of rice was studied for the purpose of establishing optimum conditions of power level and heating time. Optimum volume of adding water was 290 ml per 173 g rice. The longer the rice was soaked, the better the cooked rice. However, we chose one hour as soaking time so that we might observe well the effects of power levels. The mode of microwave cooking consisted of 5 steps of power level; step 1: temperature ascendance, step 2: water absorption 1, step 3: water absorption 2, step 4: heat penetration, step 5: gelatinization completion. The quality of cooked rice was evaluated subjectively. As a result of the study, 3 optimum conditions were chosen as follows. 1) (7) 5:00-(1) 5:00-(2) 5:00-(2) 6:00-(7) 4:00, 2) (8) 4:25-(1) 5:00-(2) 5:00-(2) 5:00-(6) 4:00,3) (9) 3:40-(1) 5:00-(2) 5:00-(3) 6:00-(7) 2:00

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A Study on the Dieless Wire Drawing Using Microwave (마이크로웨이브를 이용한 Dieless Wire Drawing 에 대한 연구)

  • Huh You;Kim S.H.;Kim J.S.;Kim I.S.;Paik Y.N.
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2005.06a
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    • pp.942-945
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    • 2005
  • Micron-sized metal wires are widely used in industries such as filtration, catalyst and composite materials, etc. In the wire drawing process, the die that is used conventionally is an effective and, at the same time, sensitive component. However, a typical array of the dies has caused many problems in the wire drawing process, e.g., large frictional force on the interface between wire and the resulting high heat generation, precise adjustment of the dies, extended cooling system, die abrasion, etc.. Because of these problems, there have been many works that are aiming at improving the efficiency of wire drawing process by analyzing the die geometry and by applying advanced die material to prolong the die life or even at developing a dieless wire drawing system. This paper is dealing with developing a new wire drawing system that is applicable to reduce the wire drawing steps with high draw ratio. The new wire drawing system does not use the dies, but use the self-induced heater that works on the basis of the resonant phenomenon of wire material. The electromagnetic wave is the heating source. The results of the study on the diameter reduction and microwave flow analysis show that the heating effectiveness of the wire is influenced by the energy distribution in the microwave propagation chamber. We can obtain diameter-reduced wires by using microwave in the dieless drawing process. Microwave as a heating source is capable of producing wires without applying dies in wire drawing process.

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