• 제목/요약/키워드: Microstructure properties

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ZrO2-Ag의 복합화 공정에 따른 기계적 특성 및 미세조직 평가 (A Study of Mechanical Properties and Microstructure of ZrO2-Ag Depending on the Composite Route)

  • 여인철;한재길;강인철
    • 한국분말재료학회지
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    • 제19권6호
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    • pp.416-423
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    • 2012
  • This paper introduces an effect of a preparing $ZrO_2$-Ag composite on its mechanical properties and microstructure. In present study, $ZrO_2$-Ag was prepared by reduction-deposition route and wetting dispersive milling method, respectively. Two type of Ag powders (nano Ag and micron Ag size, respectively) were dispersed into $ZrO_2$ powder during wetting dispersive milling in D.I. water. Each sample was sintered at $1450^{\circ}C$ for 2hr in atmosphere, and then several mechanical tests and analysis of microstructure were carried out by bending test, hardness, fracture toughness and fracture surface microstructure. As for microstructure, the Ag coated $ZrO_2$ showed homogeneously dispersed Ag in $ZrO_2$ in where pore defect did not appear. However, $ZrO_2$-nano Ag and $ZrO_2$-micro Ag composite appeared Ag aggregation and its pore defect, which carried out low mechanical property and wide error function value.

슬래그 혼합 시멘트의 물서에 미치는 황산염과 염화물의 영향 (The influence of sulphates and chlorides on the properties of slag blended cement)

  • 성진욱;이승헌;김창은
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 1999년도 학회창립 10주년 기념 1999년도 가을 학술발표회 논문집
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    • pp.127-130
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    • 1999
  • Physical properties and microstructure of slag blended cement were investigated to evaluate the influence of sulphates and chlorides. The compressive strength developed as high chloride content dust and gypsum added and accordingly the microstructure modification was showed. The deviation of pore size distribution and hydrates was also observed. From these results we discussed optimum condition of gypsum and high chloride content dust leading to physical properties in this study.

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The Influence of Production Process Parameters on Properties W-Ag, Mo-Ag Composites

  • Lezanski, Jan;Madej, Marcin
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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    • pp.1200-1201
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    • 2006
  • Attempts have been made to describe the influence of production process parameters on the microstructure and properties of W-Ag and Mo-Ag composites. The compositions of powder mixtures are W+30% Ag and Mo+30%Ag. Silver additions assists densification during sintering by a liquid phase sintering process. The main goal of this work is to compare properties and microstructure of as-sintered and as-infiltrated composites.

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Al 6061-T6 합금의 MIG 용접 후 열처리조건에 따른 미세조직 및 기계적 물성 분석 (Analysis of Microstructure and Mechanical Properties According to Heat Treatment Conditions in GMAW for Al 6061-T6 Alloy)

  • 김찬규;조영태;정윤교;강신현
    • Journal of Welding and Joining
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    • 제34권4호
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    • pp.34-39
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    • 2016
  • Recently, aluminum alloy has used various industry, such as automobile, shipbuilding and aircraft because of characteristics of low density and high corrosion resistance. Al 6061-T6 is heat treatment materials so it has high strength and mostly used for assembly by mechanical fastening such as a bolting and riveting. In GMA (Gas Metal Arc) welding of alloy, some defects which are hot cracking, porosity, low-mechanical properties and large heat affected zone is generated, because of high heat conductivity. It reduces mechanical properties. In this study, the major factor effected on properties are analyzed after welding in Al 6061-T6 in GMAW, then optimize heat treatment conditions. Plate of Al 6061-T6 with a thickness of 12 mm is welded in V groove and applied welding method is butt joint. Mechanical properties and microstructure are analyzed according to heat treatment condition. Tensile strength, microstructure and Hardness are evaluated. Result of research appears that Al 6061-T6 applied heat treatment show outstanding mechanical properties.

STD11 금형강 재열처리에 따른 미세조직 및 기계적 특성 (Microstructure and Mechanical Properties of STD11 Steel According to Reheat Treatment)

  • 박기연;권의표;허기호
    • 한국재료학회지
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    • 제32권3호
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    • pp.139-145
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    • 2022
  • Reheat treatment process of mold is necessary when partial machining of the mold is required, such as shape correction for an existing mold. If defects such as cracks or significant deterioration of mechanical properties of the mold occur during reheat treatment, it is impossible to reuse the mold. In this study, reheat treatment was performed up to two times for STD11 tool steel, and microstructure and mechanical properties according to the reheat treatment were evaluated. Carbide fraction and grain size of prior austenite were almost unchanged after the reheat treatment. Hardness and impact toughness increased significantly after QT treatment, and these properties were maintained without significant change even after the reheat treatment. It is concluded that up to two iterations of reheat treatment does not cause deterioration of properties of STD11 tool steel. Based on these results, a mold for a face-lifted front bumper was manufactured through machining and reheat-treating of an existing mold.

분말야금공법으로 제조된 CAD/CAM용 Co-Cr-Mo 합금의 미세조직 및 기계적 특성 (Microstructure and Mechanical Properties of Co-Cr-Mo alloy for CAD/CAM Applications fabricated by Powder Metallurgy Process)

  • 차성수
    • 대한치과기공학회지
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    • 제37권4호
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    • pp.235-242
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    • 2015
  • Purpose: The aims of this study are compare with microstructure and mechanical properties of Co-Cr-Mo alloys fabricated by powder metallurgy(P/M) process and casting process respectively. Methods: Microstructure and micro-hardness were tested by SEM and Vickers Hardness Tester. The sintered specimen was produced by furnace-coolling after sintering, however the casting specimen were produced thru air-cooling and water-cooling after the casting. For observation of phase transformation during sintering, DSC analyzing was carried out. Results: Mean pore size of sintered Co-Cr-Mo alloy was $4.32{\mu}m$ and that of casting alloy was $1.63{\mu}m$. Hardness of sintered alloy was lower than water-quenched casting alloy. Conclusion: Proper sintering temperature of Co-Cr-Mo alloy was above $1,200^{\circ}C$ and pore size of casting specimen were finer than sintered specimen, but hardness were similar.

단조소입법으로 제조된 컨넥팅로드의 기계적 특성에 관한 연구 (A Study on the Mechanical Properties of Connecting Rod Manufactured by Direct Quenching)

  • 최문일;강성수
    • 소성∙가공
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    • 제6권5호
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    • pp.435-445
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    • 1997
  • In order to study the manufacturing possibility of connecting rod by direct quenching method, the difference between connecting rod by direct quenching and that by general heat treatment were investigated by observing microstructure, by measuring mechanical properties, by conducting fatigue testing, and by measuring the amount of tool wear in actual cutting. Connecting rod manufactured by direct quenching had better fatigue life than that by general heat treatment, which was due to homogeneous microstructure, and higher strength. The amount of cutting tool wear of connecting rod by direct quenching was higher than that by general heat treatment, which was due to low machinability and high toughness of tempered martensite microstructure. Therefore it will be added the study of heat treatment and cutting condition for manufacturing by direct quenching.

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초미세립 순-타이타늄의 미세조직과 인장물성 (Microstructure and Tensile Properties of Ultrafine Grain Pure-Titanium)

  • 고영건;안정용;신동혁;이종수
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2006년도 춘계학술대회 논문집
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    • pp.215-218
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    • 2006
  • A study was made to investigate microstructural evolution and mechanical properties of ultra-fine grained (UFG) pure-Ti produced by equal channel angular (ECA) pressings. The deformed structures were analyzed by finite element method and transmission electron microscopy with the increment of straining. After 4 isothermal ECA pressings, initial coarse grains ($30{\mu}m$) were significantly refined to ${\sim}0.3{\mu}m$ with homogeneous distribution of microstructure which was resulted from $180^{\circ}$ rotation of the sample between pressings. UFG pure-Ti exhibited the considerable improvement in yield strength while losing strain hardening capacity as compared to coarse grained microstructure at ambient temperature, which was mainly attributed to ultra-fine grain microstructure with non-equilibrium grain boundaries.

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하소온도에 따른 Mg-페라이트 소결체의 미세구조 및 전기.자기적 특성 연구 (Microstructure, Electric, and Magnetic Properties of Mg-Ferrite with Various Calcination Temperature)

  • 김성재;정명득;백종규
    • 한국세라믹학회지
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    • 제32권1호
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    • pp.1-10
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    • 1995
  • Effects of calcination temperature on microstructure and electric-magnetic properties of Mg-ferrite were investigated. As the calcination temperature increase, the green density and the sintered density increase due to the enhancement of densification of calcined powder. The grain size in the sintered ferrite increases with increasing the calcination temperatures from 800 to 100$0^{\circ}C$, but decreases from 1000 to 120$0^{\circ}C$. The resistivity decreases with increasing the calcination temperatures from 800 to 110$0^{\circ}C$, but increases from 1100 to 120$0^{\circ}C$ due to the microstructure which consists of small, uniform grian size and pores at grain boundaries. Magnetization increases slightly due to the increasement of the sintered density while Curie temperature is almost constant regardless of calcination temperatures.

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HIC용 $RuO_2$ 후막저항체에서 유리의 물리적 성질이 TCR에 미치는 영향 (Effects of Physical Properties of Glass on the TCR of $RuO_2$ Thick Film Resistors for Hybrid Integrated Circuits (HIC))

  • 이병수;이준
    • 한국세라믹학회지
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    • 제30권11호
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    • pp.974-978
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    • 1993
  • Glass viscosity effects on the electrical properties and microstructure of RuO2 based thick film resistors (TFR) using alumina modified lead borosilicate glasses were studied. AT 85$0^{\circ}C$, the glass viscosities were increased from 4.24Pa.s to 51.5Pa.s when the alumina was added from none to 14 weight percent to the standard glass of 63% PbO, 25% B2O3 and 12% SiO2. The resistivities of resistors were generally decreased and the microstructure development was retarded as the viscosity of the glass increased. This is contrary to the generally accepted thought that the low resistivity is due to fast microstructure development kinetics in TFR. Even though the glass viscosity retards the microstructure development kinetics, the overall network formations are favored for higher viscosity of glass, such that the sheet resistivities were decreased as the glass viscosity increased.

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