• Advances in materials Research
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• v.3 no.4
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• pp.217-225
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• 2014

In this study, a forging steel alloyed with both Nb and V was used as experimental material and the hot deformation behavior has been studied for this steel by conducting the compressive deformation test at temperature of $900-1150^{\circ}C$ and strain rate of $0.01-0.01s^{-1}$ in a MMS-300 thermo-mechanical simulator. The microstructure evolution, particularly the dynamically recrystallized microstructure, of the experimental steel at elevated temperatures, strain rates and strain levels, was characterized by optical microstructural observation and the constitutive equation in association with the activation energy and Zener-Hollomon parameter. The curves of strain hardening rate versus stress were used to determine the critical strain and peak strain, and their relation was connected with Zener-Hollomon parameter. Under the conditions of processing temperature $900^{\circ}C$ and strain rate $0.01s^{-1}$, the dynamic recrystallization took place and the austenite grain size was refined from $164.5{\mu}m$ to $28.9{\mu}m$.

• Journal of Welding and Joining
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• v.35 no.1
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• pp.79-88
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• 2017

The effect of residual metallic sodium on the solidification cracking susceptibility of type 316FR stainless steel was investigated via transverse-Varestraint tests. And a solidification brittle temperature range (BTR) of type 316FR stainless steel was 37 K. However, the BTR expanded from 37 to 67 K, as the amount of metallic sodium at the specimen surface increased from 0 to $7.99mg/cm^2$. Microstructural observation of the weld metal suggested that metallic sodium existed in the weld metal, including in the cell boundaries, during welding solidification. Thermodynamic calculations suggested that sodium expanded the temperature range of solidliquid coexistence during welding solidification of the steel weld metal. Therefore, the increased solidification cracking susceptibility (i.e., expansion of the BTR) in the residual sodium environment was attributed to enhanced segregation of sodium during the welding solidification; this segregation, in turn, resulted in an expanded temperature range of solid-liquid coexistence.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.26 no.3
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• pp.528-536
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• 2002

As one step for the safety performance of LNG storage tank, the change in fracture toughness within the X-grooved weld heat-affected zone (HAZ) of newly developed 9% Ni steel, which was submerged arc (SA)-welded, was investigated. Both crack initiation fracture toughness and crack arrest fracture toughness were evaluated by the crack tip opening displacement (CTOD) tests and compact crack arrest (CCA) tests. As the evaluated region approached the fusion line, each test result shorted different tendency, that is, crack initiation toughness decreased while crack arrest toughness increased. The results were discussed through the observation of the microstructural change.

• Journal of Welding and Joining
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• v.22 no.5
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• pp.53-57
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• 2004

Friction stir weldability of AZ31B-H24, AZ61A-F and AZ91C-F Mg alloys were studied using microstructural observation and mechanical tests. The microstructure of stir zone(SZ) was coarse in AZ31B-H24 alloy whereas it was very fine both in AZ61A-F and AZ91C-F alloys. The hardness of SZ was remarkably increased by very fine recrystallized grains both in AZ61A-F and AZ91C-F alloys. On the other hand, the hardness of SZ was decreased in AZ31B-H24 due to the coarse microstructure. In SZ, AZ91C-F alloy showed very high hardness values because of dispersion hardening of $Mg_{17}$Al$_{12}$($\beta$ phase) and Al solid solution hardening. Because of more $Mg_{ 17}Al_{12}($\beta$ phase)$ intermetallic compounds, Mg alloy with high Al content showed poor mechanical properties.s.

• Korean Journal of Materials Research
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• v.11 no.11
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• pp.986-990
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• 2001

An optimum route to fabricate the $A1_2O_3/Fe-Ni$ alloy nanocomposites with sound microstructure and enhanced mechanical properties as well as magnetism was investigated. To prepare homogeneous nanocomposite powders of Fe-Ni alloy and $Al_2O_3$, the solution-chemistry routes using $Al_2O_3 \; Ni(NO_3)_2{\cdot}6H_2O$ and $Fe(NO_3)_3{\cdot}9H_2O$ powders were applied. Microstructural observation of the powder mixture revealed that the Fe-Ni alloy particles of about 20 nm in size were homogeneously surrounded $A1_2O_3$, forming nanocomposite powder. The hot-pressed composite showed improved fracture toughness and magnetic response. These results suggest that the synergy materials with an improved mechanical properties and excellent functionality can be fabricated by controlled powder preparation and consolidation processing.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.12 no.3
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• pp.7-12
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• 2013

In Die casting process, the problem of die degradation is often issued. In oder to increase of die life the material degradation of die steel was investigated using test core pins. Three test core pins were positioned in front of the gate entry and observed washout and soldering resistance during Mg die casting process. The test parameters are set as different commercial die materials, coatings condition and hardness of die surface. Usign 220t magnesium die casting machine was employed to cast AZ91 magnesium alloys. After 150 shots, macroscopic observation of die surface was carried out. Additional 50 cycles later, test pins were chemically cleaned with 5% HCl aqueous solution to find out the existence of washout and soldering layers. Microstructural characterization of die surface and the die roughness measurement were performed together. Computational simulation using AnyCasting program was also beneficial to correlate the extent of die damage with the position of test pin inside die cavity. As results, the optimal combination of die steel with productive coating as well as its hardness was drawn out. it will be helpful to decide the material and condition considering increasing of tool life.

• Journal of the Korean Society for Heat Treatment
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• v.26 no.3
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• pp.126-131
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• 2013

In this study, effects of silicon addition on the spheroidizing annealing of hyper-eutectoid steel was investigated. Heat treatment at various temperatures in the ${\gamma}+{\theta}$ region was also conducted in order to systematically control the kinetics of undissolved cementite. It was found that small amount of Si addition could increase both $A_1$ and $A_{cm}$ transformation temperature by both the JMat Pro evaluation and dilatometric measurement. It was also revealed by the microstructural observation that the volume fraction of retained cementite during heat treatment increased with decreasing temperature as well as increasing Si content. Based on the results obtained, it could be suggested that spheroidization at relatively higher temperature above $950^{\circ}C$ could be achieved by small addition of Si.

• Journal of Korea Foundry Society
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• v.35 no.4
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• pp.88-98
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• 2015

The effects of quenching and tempering temperatures on the tensile, impact and corrosion properties of A487 alloy cast with different C contents of 0.16, 0.19 to 0.23 wt.% were examined. The impact tests were conducted at $25^{\circ}C$ and $-60^{\circ}C$ and the immersion test was performed using 3.5% NaCl solution for 14 days. The quenching temperature affected the mechanical properties of A487 alloy cast, while the magnitude of change varied depending on the C content. The increase in tempering temperature showed the typical trend of decreasing tensile strength and increasing impact properties. The change in quenching and tempering temperature in this study did not affect the corrosion properties of A487 alloy significantly. The change in mechanical and corrosion properties of A487 with different C contents was discussed based on the microstructural and fractographic observation.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.26 no.2
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• pp.67-73
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• 2016

The degradation behaviors of TiN coating layers under thermo-mechanical stress were investigated in terms of comparison of finite element analysis (FEA) and experimental data. The coating specimen was designed to quarter cylinder model, and the pulsed laser ablation was assumed as heat flux condition. The FEA results showed that heat accumulation at the center of the laser-ablated spot occurred and principle stress was concentrated at the lower region of the coating layer. The microstructural observation revealed that surface melting and decrease of the coating thickness occurred in the TiN/Inconel 617 and the interfacial cracks formed in the TiN/Si. The delamination was caused by the mechanical stress from the center to the outside of the ablated spot as the FEA results expected. It was considered that the improvement of the thermal shock resistance was attributed to higher thermal conductivity of Si wafer than that of Inconel 617.

• Nuclear Engineering and Technology
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• v.46 no.3
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• pp.413-422
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• 2014

Presented in this study are the variations of microstructures and mechanical properties with tempering and Post-Weld Heat Treatment (PWHT) conditions for SA508 Gr.4N steel used as Reactor Pressure Vessel (RPV) material. The blocks of model alloy were austenitized at the conventional temperature of $880^{\circ}C$ then tempered and post-weld heat treated at four different conditions. The hardness and yield strength decrease with increased tempering and PWHT temperatures, but impact toughness is significantly improved, especially in the specimens tempered at $630^{\circ}C$. The sample tempered at $630^{\circ}C$ with PWHT at $610^{\circ}C$ shows optimum mechanical properties in hardness, strength, and toughness, excluding only the transition property in the low temperature region. The microstructural observation and quantitative analysis of carbide size distribution show that the variations of mechanical properties are caused by the under-tempering and carbide coarsening which occurred during the heat treatment process. The introduction of PWHT results in the deterioration of the ductile-brittle transition property by an increase of coarse carbides controlling cleavage initiation, especially in the tempered state at $630^{\circ}C$.