• Title/Summary/Keyword: Microstructural & Mechanical properties

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Mechanical and microstructural study of rice husk ash geopolymer paste with ultrafine slag

  • Parveen, Parveen;Jindal, Bharat Bhushan;Junaid, M. Talha;Saloni, Saloni
    • Advances in concrete construction
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    • 제8권3호
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    • pp.217-223
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    • 2019
  • This paper presents the mechanical and microstructural properties of the geopolymer paste which was developed by utilizing the industrial by-products, rice husk ash (RHA) and ultra-fine slag. Ultra-fine slag particles with average particle size in the range of 4 to 5 microns. RHA is partially replaced with ultra-fine slag at different levels of 0 to 50%. Sodium silicate to sodium hydroxide ratio of 1.0 and alkaline liquid to binder (AL/B) ratio of 0.60 is taken. Setting time, compressive, flexural strengths were studied up to the age of 90 days with different concentrations of NaOH. The microstructure of the hybrid geopolymer paste was studied by performing the SEM, EDS, and XRD on the broken samples. RHA based geopolymer paste blended with ultrafine slag resulted in high compressive and flexural strengths and increased setting times of the paste. Strength increased with the increase in NaOH concentration at all ages. The ultra-small particles of the slag acted as a micro-filler into the paste and enhanced the properties by improving the CASH, NASH, and CSH. The maximum compressive strength of 70MPa was achieved at 30% slag content with 16M NaOH. The results of XRD, SEM, and EDS at 30% replacement of RHA with ultra-fine slag densified the paste microstructure.

Mechanical and microstructural investigations on cement-treated expansive organic subgrade soil

  • Nazerke Sagidullina;Jong Kim;Alfrendo Satyanaga;Taeseo Ku;Sung-Woo Moon
    • Geomechanics and Engineering
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    • 제38권4호
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    • pp.353-366
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    • 2024
  • Organic soils pose significant challenges in geotechnical engineering due to their high compressibility and low stability, which can result in issues like differential settlement, rutting, and pavement deformation. This study explores effective methods for stabilizing organic soils. Rather than conventional ordinary Portland cement (OPC), the focus is on using environmentally friendly calcium sulfoaluminate (CSA) cement, known for its rapid setting, high early strength development, and environmental benefits. Mechanical behavior is analyzed through 1-D free swell, unconfined compressive strength (UCS), and bender element (BE) tests. Microstructural analyses, including Fourier transform infrared spectroscopy (FTIR) and scanning electron microscopy (SEM), characterize the soil mixed with CSA cement. Experimental results demonstrate improved soil properties with increasing cement dosage and curing periods. A notable strength increase is observed in soil samples with 15% cement content, with UCS doubling after 7 days. This trend aligns with shear wave velocity results from the BE test. SEM and FTIR spectroscopy reveal how CSA cement hydration forms hydrated calcium silicate gel and ettringite, enhancing soil properties. CSA cement is recommended for reinforcing organic subgrade soil due to its eco-friendly nature and rapid strength gain, contributing to improved durability.

ADI의 기계적 성질에 미치는 합금원소 및 열처리의 영향 (The Effect of Alloying Elements and Heat Treatment on Mechanical Properties of ADI)

  • 김석원;;우기도
    • 열처리공학회지
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    • 제11권2호
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    • pp.121-130
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    • 1998
  • The effects of alloying elements(Mo, Cu, Ni) and austempering temperature conditions on the microstructural morphologies and mechanical properties in austempered ductile cast iron has been investigated. The austempering at $350^{\circ}C$ for 2hrs after austenitizing at $900^{\circ}C$ for 2hrs in all specimens with various alloying elements was optimum because the good combination of tensile and yield strength, hardness and impact value was obtained. The microstructures of these ADIs treated by a forementioned austempering condition are nearly a mixture type of needle and feathery bainite. Among those alloys, Mo-Cu alloyed DCI had the best optimum mechanical properties of hardness and toughness for automobile parts by austempering treatment for 2hrs at $900^{\circ}C$ followed by $350^{\circ}C$ for 2hrs.

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Steel nitriding optimization through multi-objective and FEM analysis

  • Cavaliere, Pasquale;Perrone, Angelo;Silvello, Alessio
    • Journal of Computational Design and Engineering
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    • 제3권1호
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    • pp.71-90
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    • 2016
  • Steel nitriding is a thermo-chemical process leading to surface hardening and improvement in fatigue properties. The process is strongly influenced by many different variables such as steel composition, nitrogen potential, temperature, time, and quenching media. In the present study, the influence of such parameters affecting physic-chemical and mechanical properties of nitride steels was evaluated. The aim was to streamline the process by numerical-experimental analysis allowing defining the optimal conditions for the success of the process. Input parameters-output results correlations were calculated through the employment of a multi-objective optimization software, modeFRONTIER (Esteco). The mechanical and microstructural results belonging to the nitriding process, performed with different processing conditions for various steels, are presented. The data were employed to obtain the analytical equations describing nitriding behavior as a function of nitriding parameters and steel composition. The obtained model was validated, through control designs, and optimized by taking into account physical and processing conditions.

오스템퍼링 처리가 열간압연롤용 NICI재 및 DCI재의 미세조직 및 기계적 성질에 미치는 영향 (The Effect of Austempering Treatment on Microstructure and Mechanical Properties of NICI and DCI for Rolls Used in Hot Rolling Mill)

  • 김재진;오석중;유국종;;백응률
    • 한국주조공학회지
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    • 제29권6호
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    • pp.251-256
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    • 2009
  • The effect of austempering treatment on mechanical properties of nodular indefinite chilled iron(NICI) and ductile cast iron(DCI) was investigated. In microstructural observation, matrix phase(pearlite and ferrite) was changed to ausferrite after austempering treatment both DCI and NICI. In case of NICI, decomposition of cementite($Fe_3C$) during austempering treatment was induced. After austempering treatment, mechanical properties such as hardness, tensile strength and impact toughness was improved in NICI and DCI. The wear resistance is slightly decreased because of decomposition of cementite during austempering treatment in NICI but impact toughness and strength is dramatically increased.

자기적 방법에 의한 0.85% 탄소강의 열처리에 따른 미세조직 및 기계적 성질 평가 (Evaluation of Microstructures and Mechanical Property of Variously Heat Treated 0.85% Carbon Steel by Magnetic Method)

  • 변재원;권숙인
    • 한국재료학회지
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    • 제13권2호
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    • pp.81-87
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    • 2003
  • Microstructures and mechanical properties of variously heat treated 0.85% carbon steel(eutectoid steel) were evaluated by magnetic property measurements. Microstructural analysis (pearlite interstellar spacing), measurement of mechanical properties(Rockwell hardness, yield stress, fracture stress) and magnetic properties(coercivity, remanence, hysteresis loss, saturation magnetization) were performed to clarify mutual relationships among these parameters. Water quenched specimens with martensite structure showed much higher coercivity and remanence than air cooled or furnace cooled specimens with pearlite structure. The linear dependence of coercivity and remanence on pearlite interlamellar spacing as well as on Rockwell hardness, yield stress and fracture stress was observed in the pearlitic steel. Hysteresis loss and saturation magnetization showed no distinct trend with pearlite interlamellar spacing.

Mechanical Properties and Surface Characteristics of Ti-25Ta-xHf Alloys

  • Park, Seon-Yeong;Kim, Jeong-Jae;Choe, Han-Cheol
    • 한국표면공학회:학술대회논문집
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    • 한국표면공학회 2014년도 추계학술대회 논문집
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    • pp.187-187
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    • 2014
  • In this study, we investigated mechanical properties and surface characteristics of Ti-25Ta-xHf alloys. The samples were manufactured for composition of Ti-25Ta-xHf(x=0 to 15 wt. %) alloys. Each alloy was melted twenty times in an arc-melting vacuum furnace. The microstructural phases and phase transformation of Ti-25Ta-xHf alloys were identified with the aid of an XRF, XRD and DSC. And mechanical properties were investigated using Vickers hardness, nanoindentation, and tensile test.

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고망간 오스테나이트계 강판의 자동차 부품 적용성 연구 (A Study on the Application of High Manganese Austenitic Steel Sheet to Automobile Parts)

  • 정연일;채수홍;김소연;홍승현;임종대
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2009년도 춘계학술대회 논문집
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    • pp.393-396
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    • 2009
  • The mechanical properties, press formability and texture of a TWIP steel were investigated. This steel combines both high strength and high ductility due to so called TWIP effect which are related to the microstructural changes. The formation of twins during deformation leads to an increase of its mechanical properties. In this study, the texture and mechanical properties evolutions of a TWIP steel subjected to tensile tests and press trials at room temperature were investigated in relation to the feasibility of the application to automotive body parts.

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Cu 첨가량이 Al2O3/Cu 나노복합재료의 미세조직과 기계적 성질에 미치는 영향 (Effect of Cu content on Microstructure and Mechanical Properties of Al2O3/Cu Nanocomposites)

  • 오승탁;윤세중
    • 한국분말재료학회지
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    • 제13권1호
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    • pp.33-38
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    • 2006
  • The effect of Cu content on microstructure and mechanical properties of nano-sized Cu dispersed $Al_2O_3(Al_2O_3/Cu)$ nanocomposites was investigated. The nanocomposites with Cu content of 2.5 to 10 vol% were prepared by reduction and hot-pressing of $Al_2O_3/CuO$ powder mixtures. The nanocomposites with Cu content of 2.5 and 5vol% exhibited the maximum fracture strength of 820MPa and enhanced toughness compared with monolithic $Al_2O_3$. The strengthening was mainly attributed to the refinement of $Al_2O_3$ matrix grains. The toughening mechanism was discussed by the observed microstructural feature based on crack bridging.

내마모 구조 코팅용 Cr-Al-Si-N 코팅막의 미세구조와 기계적 특성에 관한 연구 (Microstructure and Mechanical Properties of Cr-Al-Si-N Coatings for Wear Resistant and Structural Applications)

  • 강동식;김광호
    • 한국재료학회지
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    • 제15권11호
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    • pp.730-734
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    • 2005
  • Cr-Al-Si-N coatings were deposited on WC-Co substrates by a hybrid coating system of arc ion plating and DC magnet :on sputtering technique in $N_2/Ar$ mixture. The Cr-tll-Si-N coatings were synthesized with different Si contents. Their microstructure and mechanical properties were systematically investigated. The average size of crystallites largely decreases with the increase of Si content compared with Cr-Al-N. The microhardness of Cr-Al-Si-N coatings largely increases from 24 to 55 GPa. The enhanced hardness is believed to originate from the microstructural change by the fine composite microstructure of Cr-Al-N coatings with Si addition. The average friction coefficient of Cr-Al-Si-N coatings decreases from 0.84 to 0.45 with increasing Si content up to $16\;at.\%$.