• Title/Summary/Keyword: Microstructural & Mechanical properties

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Microstructural and Piezoelectric Properties of Low Temperature Sintering PMN-PZT Ceramics with the Variations of Sintering Times (저온소결 PMN-PZT 압전세라믹의 소성시간에 따른 미세구조 및 압전특성)

  • Yoo, Ju-Hyun;Lee, Chang-Bae;Lee, Sang-Ho;Paik, Dong-Soo;Jeong, Yeong-Ho;Im, In-Ho
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.18 no.3
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    • pp.237-242
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    • 2005
  • In this paper, in order to develop the low temperature sintering ceramics for multilayer piezoelectric transformer, PMN-PZT ceramics were manufactured with the variations of sintering times, and their microstructural, piezoelectric and dielectric properties were investigated. Li$_2$CO$_3$ and Bi$_2$O$_3$ were used as sintering aids and the specimens were sintered during 30, 60, 90, 120, 150, and 180 minutes, respectively. At the specimen sintered during 90 minute, mechanical quality factor(Qm), electro-mechanical coupling factor(kp) and dielectric constant were showed the optimum values of 2,356, 0.504 and 1,266, respectively.

Microstructure and Mechanical Properties of Nanocrystalline TiN Films Through Increasing Substrate Bias (기판 바이어스 인가에 따른 나노결정질 TiN 코팅 막의 미세구조와 기계적 성질변화)

  • Chun, Sung-Yong
    • Journal of the Korean Ceramic Society
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    • v.47 no.6
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    • pp.479-484
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    • 2010
  • Microstructural and mechanical properties of the TiN films deposited on Si substrates under various substrate bias voltages by a reactive magnetron sputtering have been studied. It was found that the crystallographic texture, microstructural morphology and mechanical property of the TiN films were strongly depended on the substrate bias voltage. TiN films deposited without bias exhibited a mixed (200)-(111) texture with a strong (200) texture, which subsequently changed to a strong (111) texture with increasing bias voltage. It is also observed that the crystallite size decreases with increasing bias voltage, which corresponds to the increasing diffraction peak width of XRD patterns. The average surface roughness was calculated from AFM images of the films; these results indicated that the average surface roughness was increased with an increase in the bias voltage of the coatings.

Successive recycled coarse aggregate effect on mechanical behavior and microstructural characteristics of concrete

  • Ashish, Deepankar K.;Saini, Preeti
    • Computers and Concrete
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    • v.21 no.1
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    • pp.39-46
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    • 2018
  • With the increase in industrialization and urbanization, growing demand has enhanced rate of new constructions and old demolitions. To avoid serious environmental impacts and hazards recycled concrete aggregates (RCA) is being adopted in all over the world. This paper investigates successive recycled coarse aggregates (SRCA) in which old concrete made with RCA in form of concrete cubes was used. The cubes were crushed to prepare new concrete using aggregates from crushing of old concrete, used as SRCA. The mechanical behavior of concrete was determined containing SRCA; the properties of SRCA were evaluated and then compared with natural aggregates (NA). Replacement of NA with SRCA in ratio upto 100% by weight was studied for workability, mechanical properties and microstructural analysis. It was observed that with the increase in replacement ratio workability and compressive strength decreased but in acceptable limits so SRCA can be used in low strength concretes rather than high strength concrete structures.

Evolution of Microstructure and Mechanical Properties of a Ni Base Superalloy during Thermal Exposure (니켈기 초내열합금의 열간노출에 따른 미세조직 및 기계적 특성 변화)

  • Kim, In-Soo;Choi, Baig-Gyu;Jung, Joong-Eun;Do, Jeong-Hyeon;Jung, In-Yong;Jo, Chang-Yong
    • Journal of Korea Foundry Society
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    • v.36 no.5
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    • pp.159-166
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    • 2016
  • The microstructural evolution of a cast Ni base superalloy, IN738LC, has been investigated after long term exposure at several temperatures. Most of the fine secondary ${\gamma}^{\prime}$ particles resolved after 2000 hour exposure at $816^{\circ}C$. At higher temperatures of $871^{\circ}C$ and $927^{\circ}C$, secondary ${\gamma}^{\prime}$ resolved after 1000 hours of exposure, and cuboidal primary ${\gamma}^{\prime}$ grew with exposure time. During the thermal exposure, ${\sigma}$ phase formed at all tested temperatures, and ${\eta}$ phase was observed around interdendritic regions due to carbide degeneration. The influence of microstructural evolution during thermal exposure on the mechanical properties has been analyzed. The effects of ${\gamma}^{\prime}$ particle growth are more pronounced on the high temperature creep properties than on the room temperature tensile properties.

Mechanical Properties of Sintered and HIPed Silicon Nitride (상압소결과 열간정수압소결 질화규소의 기계적 성질)

  • 김창삼;하정수;이준근
    • Journal of the Korean Ceramic Society
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    • v.24 no.3
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    • pp.223-226
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    • 1987
  • Among many densification routes for silicon nitride, HIP(hot isostatic pressing) is becomming more popular these days, mainly due to the fact that it can produce highly reliable products with superior mechanical properties. This study involves in sintering of silicon nitride followed by HIP which requires no canning. Various property changes curing sintering and HIP are observed and analyzed in terms of microstructural changes. Porosity decrease and enhanced interlocking of grains by HIP are considered to be the major causes for improved mechanical properties of silicon nitride.

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Effect of Primary Si on Mechanical Properties in Hypereutectic Al-Si Alloy Produced by Gravity Die Casting (금형주조한 Al-Si 과공정합금의 초정 Si 입자거동에 따른 기계적 성질 변화)

  • 김억수
    • Transactions of Materials Processing
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    • v.13 no.7
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    • pp.608-613
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    • 2004
  • Mechanical properties of hypereutectic Al-Si alloy are influenced by the size and distribution of primary Si. To investigate the effects of P addition and holding time, hypereutectic Al-Si alloys with various amount of P content were produced in the lab. Then, the size and distribution of primary Si were examined respectively. Mechanical properties of hardness, tensile strength and wear resistance were analyzed in conjunction with the microstructural variations in alloys.

Evaluation of Mechanical Property and Microstructure of Forged and T6-treated 6061 Aluminum Alloy Wheel (자동차 휠용 6061 Al합금의 단조 및 T6 열처리 전후의 미세조직과 기계적 특성 평가)

  • Lee, J.H.;Jeong, H.S.;Yeom, J.T.;Kim, J.H.;Park, N.K.;Lee, Y.T.;Lee, D.G.
    • Transactions of Materials Processing
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    • v.16 no.5 s.95
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    • pp.354-359
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    • 2007
  • Effects of forging and mechanical properties of 6061 aluminum alloy wheel for automobiles were investigated in the present study. Microstructural and tensile characteristics of automobile wheel after hot forging process using dynamic screw press were analyzed to evaluate effect of metal flow on mechanical properties. The results showed advanced mechanical properties of 6061 alloy wheel because of $Mg_2Si$ precipitation by T6, elongated grain by forging, and work hardening by dense metal flow, etc. Hot compression tests were conducted in order to characterize high temperature compression deformation behaviors and microstructural variation in the range of $300{\sim}450^{\circ}C$, in the strain rate range of $10^{-3}{\sim}10^1\;sec^{-1}$. As strain rate increased, maximum compression stress increased but it was shown the reverse linear relation between temperature and maximum stress irrelevant to strain rate variation. On the other hand, temperature and yield stress didn't have any linear relation and its relation showed big deviation by a function of strain rate and test temperature.

Microstructural and Mechanical Property Evaluation of the Ferritic-Martensitic Steel under Liquid Sodium Environment (액체소듐 환경에서 Ferritic-Martensitic강의 미세조직 및 기계적 성질 평가)

  • Kim, Jun Hwan;Kim, Jong Man;Kim, Sung Ho;Lee, Chan Bock
    • Korean Journal of Metals and Materials
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    • v.48 no.10
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    • pp.914-921
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    • 2010
  • Studies were carried out to assess the microstructural and mechanical properties of ferriticmartensitic steel under a flowing sodium environment. HT9 (12Cr-MoVW) and Gr.92 (9Cr-MoVNbW) steel were exposed to liquid sodium at $650^{\circ}C$ containing dissolved oxygen of 20 ppm for 2333 hours and evaluations of the microstructure as well as the mechanical properties of the microhardness and nanoindentation were carried out. The result showed that both HT9 and Gr.92 exhibited macroscopic weight loss caused by general corrosion as well as localized types such as intergranular corrosion and pitting. Decarburization at the steel surface took place as the test proceeded. As the Cr content increased, dissolution and decarburization were suppressed. Assessment of the actual cladding geometry revealed that an aging process rather than decarburization governed the mechanical properties, which resulted in a decrease of the microhardness and yield stress.

Effects of Nanoclay and Glass Fiber on the Microstructural, Mechanical, Thermal, and Water Absorption Properties of Recycled WPCs

  • Seo, Young-Rok;Kim, Birm-June;Lee, Sun-Young
    • Journal of the Korean Wood Science and Technology
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    • v.47 no.4
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    • pp.472-485
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    • 2019
  • When wood plastic composites (WPCs) have been used for a certain period of time, they become waste materials and should be recycled to reduce their environmental impact. Waste WPCs can be transformed into reinforced composites, in which fillers are used to improve their performance. In this study, recycled WPCs were prepared using different proportions of waste WPCs, nanoclay, and glass fiber. The effects of nanoclay and glass fiber on the microstructural, mechanical, thermal, and water absorption properties of the recycled WPCs were investigated. X-ray diffraction showed that the nanoclay intercalates in the WPCs. Additionally, scanning electron micrographs revealed that the glass fiber is adequately dispersed. According to the analysis of mechanical properties, the simultaneous incorporation of nanoclay and glass fiber improved both tensile and flexural strengths. However, as the amount of fillers increases, their dispersion becomes limited and the tensile and flexural modulus were not further improved. The synergistic effect of nanoclay and glass fiber in recycled WPCs enhanced the thermal stability and crystallinity ($X_c$). Also, the presence of nanoclay improved the water absorption properties. The results suggested that recycled WPCs reinforced with nanoclay and glass fiber improved the deteriorated performance, showing the potential of recycled waste WPCs.

Expert Design Evaluation System for injection Molding

  • Kim, Sang-Gook;Huh, Yong-Jeong
    • International Journal of Precision Engineering and Manufacturing
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    • v.2 no.1
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    • pp.62-75
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    • 2001
  • The design and manufacture of injection molded polymeric parts with desired properties is a costly process dominated by empiricism including repeated modification of actual tooling. This paper presents and expert design evaluation system which can predict the mechanical performance of a molded product and diagnose the design before the actual mold is machined. The knowledge-based system synergistically combines a rule-based expert system with CAE programs. An iterative boundary pressure reflection method(IBPR) is developed to automate the cavity filling simulation program and to predict thermo-mechanical properties of a molded part precisely. Mathematical models of weldline and frozen-in molecular orientation are established to determine the spatial variation of microstructural anisotropies of a molded part from the result of cavity filling simulation. The strength ellipse is devised as and index which represents th spatial distribution of the microstructural anisotropies of a molded part, Heuristic knowledge of injection molding, flow simulation, and mechanical performance prediction is formalized as rules of an expert consultation system. The expert system interprets the analytical results of the process simulation, predicts the performance, evaluates the design and generates recommendations for optimal design alternative.

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