• Title/Summary/Keyword: Micro-hybrid composite

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Microhardness and microleakage of composite resin according to the change of curing light intensity

  • Park, Soo-Man;Shin, Dong-Hoon
    • Proceedings of the KACD Conference
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    • 2001.11a
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    • pp.586.2-586
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    • 2001
  • The selection of a curing light is a multifactorial decision. While each method of polymerization presents unique clinical benefits, the optimal light-curing technique remains to be determined. The objective of this study was to check the difference of micro hardness and microleakage according to various light intensity (50, 100, 200, 300, 400, 600 ㎽/$\textrm{cm}^2$) and curing time (10, 20, 40 seconds). A3 color of two composite resin, hybrid type DenFil and submicron type Esthet X were tested.(중략)

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BMP-2 Immoblized in BCP-Chitosan-Hyaluronic Acid Hybrid Scaffold for Bone Tissue Engineering

  • Nath, Subrata Deb;Abueva, Celine;Sarkar, Swapan Kumar;Lee, Byong Taek
    • Korean Journal of Materials Research
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    • v.24 no.12
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    • pp.704-709
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    • 2014
  • In this study, we fabricated a novel micro porous hybrid scaffold of biphasic calcium phosphate (BCP) and a polylectrolyte complex (PEC) of chitosan (CS) and hyaluronic acid (HA). The fabrication process included loading of CS-HA PEC in a bare BCP scaffold followed by lypophilization. SEM observation and porosimetry revealed that the scaffold was full of micro and macro pores with total porosity of more than 60 % and pore size in the range of $20{\sim}200{\mu}m$. The composite scaffold was mechanically stronger than the bare BCP scaffold and was significantly stronger than the CS-HA PEC polymer scaffold. Bone morphogenetic growth factor (BMP-2) was immobilized in CS-HA PEC in order to integrate the osteoinductive potentiality required for osteogenesis. The BCP frame, prepared by sponge replica, worked as a physical barrier that prolonged the BMP-2 release significantly. The preliminary biocompatibility data show improved biological performance of the BMP-2 immobilized hybrid scaffold in the presence of rabbit bone marrow stem cells (rBMSC).

A study on ceramic and metal composite material joining for micro filter using thermal spray and laser welding (용사법과 레이저 용접을 이용한 복합소재 미세필터 연구)

  • Song, In-Gyu;Choi, Hae-Woon;Kim, Joo-Han;Yun, Bong-Han;Park, Jung-Eon
    • Proceedings of the KWS Conference
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    • 2010.05a
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    • pp.32-38
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    • 2010
  • Hybrid material(ceramic+metal) processes were developed for micro filter using ceramics coating at metal filter surface by thermal spray method, micro hole drilling at ceramic coated filter surface by femtosecond laser, and fiber laser direct welding of ceramic and metal (SUS304, SM45C) by capillary effect. Thermal spray process was used for ceramic powders and metal filters. The used ceramic powders were $Al_2O_3+40TiO_2$(Metco 131VF) powder of maximum particle size $5{\mu}m$ and ${Al_2O_3}99+$(Metco 54NS) power of maximum particle size 45m. Ceramic coated filters using thermal spray method had a great influence on powder material, particle size and coating thickness but had a fine performance as a micro filter. CW fiber laser was used to drill the top ceramic layer and melt the bottom metal layer for joining applications.

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Monitoring of Debonding Failure of Reinforced Concrete(RC) Beams Retrofitted with Hybrid Composites by Optical FBG Sensor (Hybrid 복합재료 보강 철근콘크리트 보의 광섬유센서를 이용한 부착파괴 모니터링)

  • Kim, Ki-Soo;Kim, Jong-Woo;Jho, Yoon-Bum;Min, Jung-Hyun;Shin, Yeong-Soo;Jung, Chul
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2002.10a
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    • pp.208-211
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    • 2002
  • In RC beams strengthened with Epoxy-Bonded Fiber, debonding failure happens frequently. Moreover, through the life cycle, it is difficult to recognize clacks and deflections on the surface of concrete members strengthened with Epoxy- Bonded Fiber. For these reasons, we must always monitor the state of RC beams. The Optical FBG sensor is broadly accepted as a structural health monitoring device. The main objective of this paper is that it's possible to monitoring the debonding failure of R.C. beams strengthened with Epoxy-Bonded Fiber. For that, we fixed two Optical FBG sensors at the center of the beam and another two sensors in the end of Epoxy-Bonded Fiber, According to the comparison micro-strain between embeded sensor in concrete and that on the fiber surface, we can find the point which debonding failure occurs

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SELF-ADHESION OF LOW-VISCOSITY COMPOSITES TO DENTIN SURFACE (상아질에 대한 저점도 복합레진의 자가접착에 관한 연구)

  • Cho, Tae-Hee;Choi, Kyoung-Kyu;Park, Sang-Hyuk;Park, Sang-Jin
    • Restorative Dentistry and Endodontics
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    • v.28 no.3
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    • pp.209-221
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    • 2003
  • The objectiveness of this study was to evaluate whether low-viscosity composite can bond effectively to dentin surface without bonding resin. The low-viscosity composites being 50wt% filler content were made by the inclusion of bonding resin of two self-etching systems(Cleafil SE Bond, Unifil Bond) varied with contents as 0, 10, 20, 30, 40, 50wt%. Exposed dentin surfaces of extracted 3rd molars are used. Dentin bond strengths were measured. The tests were carried out with a micro-shear device placed testing machine at a CHS of 1mm/min after a low-viscosity composite was filled into an iris cut from micro tygon tubing with internal diameter approximately 0.8mm and height of 1.0mm. 1 Flexural strength and modulus was increased with the addition of bonding resin. 2. Micro-shear bond strength to dentin was improved according to content of bonding resin irrespective of applying or not bonding resin in bonding procedure, and that of Clearfil SE Bond groups was higher than Unifil Bond. 3. There were no significant difference whether use of each bonding resin in bonding procedure for S-40, S-50, U-50(p>0.05). 4. In SEM examination, resin was well infiltrated into dentin after primed with self-etching primer only for S-50 and U-50 in spite of the formation of thinner hybrid layer. Low viscosity composite including some functional monomer may be used as dentin bonding resin without an intermediary bonding agent. It makes a simplified bonding procedure and foresees the possibility of self-adhesive restorative material.

Synthesis of Polymer-Carbon Nanotubes Composite Nanoparticles and Their Applications into Forming Hybrid Composite Thin Films (폴리머-탄소나노튜브 복합체 에어로졸 입자의 생성 및 이를 이용한 하이브리드 복합체 박막 제조)

  • Kim, Whi-Dong;Ahn, Ji-Young;Kim, Soo Hyung
    • Particle and aerosol research
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    • v.6 no.2
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    • pp.61-67
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    • 2010
  • In this paper, we describe a new method to form polymer thin films, in which carbon nanotubes (CNTs) are homogeneously distributed so that they can strengthen the mechanical property of resulting polymer film. To do so, we first homogeneously mixed CNTs with polymer in a DMF solvent. With the assistance of ultrasonic nebulizer, the polymer/CNT solution was then aerosolized into micro-sized droplets and finally turned into solidified polymer/CNT composite particles by gas-phase drying process. As the results of SEM and TEM analysis, CNTs were found to be homogeneously immobilized in the polymer matrix particles due to rapid drying process in the gas phase. For comparison purpose, (i) the polymer/CNTs composite particles prepared by aerosol processing method and (ii) polymer/CNTs sheets prepared by simple solution-evaporation method were employed to form polymer/CNTs composite thin films using a hot press. As the result, the aerosol processing of composite particles was found to be a much more effective method to form homogeneously distributed-CNTs in the polymer matrix thin film.

Effect of hybrid polypropylene-steel fibres on strength characteristics of UHPFRC

  • Nuaklong, Peem;Chittanurak, Jithaporn;Jongvivatsakul, Pitcha;Pansuk, Withit;Lenwari, Akhrawat;Likitlersuang, Suched
    • Advances in concrete construction
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    • v.10 no.1
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    • pp.1-11
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    • 2020
  • This study intends to produce an ultra-high performance fibre reinforced concrete (UHPFRC) made with hybrid fibres (i.e., steel and polypropylene). Compressive and tensile strength characteristics of the hybrid fibres UHPFRC are considered. A total of 14 fibre-reinforced composites (FRCs) with different fibre contents or types of fibres were prepared and tested in order to determine a suitable hybrid fibre combination. The compressive and tensile strengths of each concrete at 7 days were determined. The results showed that a hybrid mix of micro-polypropylene and steel fibres exhibited good compromising performances and is the ideal reinforcement mixture in a strong, cost-effective UHPFRC. In addition, maximum compressive strength of 167 MPa was achieved for UHPFRC using 1.5% steel fibres blended with 0.5% macro-polypropylene fibres.

Effect of Micro-bolt Reinforcement for Composite Scarf Joint (복합재 스카프 조인트에서의 마이크로 볼트 보강에 대한 타당성 연구)

  • Lee, Gwang-Eun;Sung, Jung-Won;Kweon, Jin-Hwe
    • Composites Research
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    • v.32 no.1
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    • pp.37-44
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    • 2019
  • The reinforcement effect of micro-bolt for a bonded scarf joint was investigated. Three scarf ratios of 1/10, 1/20, and 1/30 were considered to examine the effect of scarf patch configuration on joint strength. To maintain the same density of micro-bolt, 16, 32, and 48 bolts were installed in the scarf joint specimens with scarf ratios of 1/10, 1/20, and 1/30, respectively. Tests were also carried out on the joints that are bonded with only adhesive and that are fastened with only micro-bolts to obtain reference values. The average failure loads of the adhesive joints with scarf ratios of 1/10, 1/20, and 1/30 were 29.7, 39.6, and 44.8 kN, respectively. In case of micro-bolt reinforcement, the failure loads at the same scarf ratios were 28.4, 37.2, and 40.1 kN, respectively, which corresponds to 96, 94, and 90% of the pure adhesive joint failure loads. In the case of using only micro-bolts, the failure loads were only 13-25% of the average failure loads of pure adhesive joints. Fatigue test was also conducted for the joints with scarf ratio of 1/10. The results show that the fatigue strength of hybrid joints using both adhesive and microbolts together slightly increased compared to the fatigue strength of adhesive joint, but the rate of increase was small to 2-3%. Through this study, it was confirmed that the reinforcement effect of micro-bolt is negligible in the scarf joints where shear stress is dominating the failure, unlike in the structure where peel stress is dominant.

POLYMERIZATION ABILITY OF SEVERAL LIGHT CURING SOURCES ON COMPOSITE RESIN (광원에 따른 중합광의 복합레진 중합 능력 비교)

  • Shin, Hye-Jin;Kim, Jin-Woo;Cho, Kyung-Mo
    • Restorative Dentistry and Endodontics
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    • v.28 no.2
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    • pp.156-161
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    • 2003
  • The purpose of this study is to evaluate the polymerization ability of three different light sources by microhardness test. Stainless steel molds of 1, 2, 3, 4 and 5 mm in thickness of 7 mm in diameter were prepared. The hybrid composite Z100 was packed into the hole of the mold and curing light was activated for designated time. Three different light sources, conventional halogen, light emitting diode, and plasma arc, were used for curing of composite. Two different curing times applied ; one is to follow the manufacturers recommendation and the other is to extend the curing time of LED and plasma arc for balancing the light energy with halogen. Immediately after curing, the Vickers hardness was measured at the bottom of specimen. The results were as follows. 1 The composite cured with LED showed equal to higher microhardnesss than halogen. 2. The composite was cured with plasma arc by manufacturers recommendation showed lowest micro-hardness at all thickness. However, when curing time was extended, microhardness was higher than the others. In conclusion, this study suggested that plasma arc needs properly extended curing time.