• Title/Summary/Keyword: Micro pore size

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The effect of micro pore on the characteristics of crack tip plastic zone in concrete

  • Haeri, Hadi;Sarfarazi, V.
    • Computers and Concrete
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    • v.17 no.1
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    • pp.107-127
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    • 2016
  • Concrete is a heterogeneous material containing many weaknesses such as micro-cracks, pores and grain boundaries. The crack growth mechanism and failure behavior of concrete structures depend on the plastic deformation created by these weaknesses. In this article the non-linear finite element method is used to analyze the effect of presence of micro pore near a crack tip on both of the characteristics of crack tip plastic zone (its shape and size) and crack growth properties (such as crack growth length and crack initiation angle) under pure shear loading. The FE Code Franc2D/L is used to carry out these objectives. The effects of the crack-pore configurations and the spacing between micro pore and pre-excising crack tip on the characteristics of crack tip plastic zone and crack growth properties is highlighted. Based on the obtained results, the relative distance between the crack tip and the micro pore affects in very significant way the shape and the size of the crack tip plastic zone. Furthermore, crack growth length and crack initiation angle are mostly influenced by size and shape of plastic zone ahead of crack tip. Also the effects of pore decrease on the crack tip by variation of pore situation from linear to perpendicular configuration. The critical position for a micro pore is in front of the crack tip.

Micro-porous Nickel Produced by Powder Metallurgy

  • Yamada, Y.;Li, Y.C.;Banno, T.;Xie, Z.K.;Wen, C.E.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.602-603
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    • 2006
  • Micro-porous nickel (Ni) with an open cell structure was fabricated by powder metallurgy. The pore size of the micro-porous Ni approximated $30{\mu}m$ and $150{\mu}m$. For comparison, porous Ni with a macro-porous structure were also prepared by both powder metallurgy (pore size $800{\mu}m$) and the traditional chemical vapour deposition method (pore size $1300{\mu}m$). The mechanical properties of the micro-and macro-porous Ni samples were evaluated using compressive tests. Results indicate that the micro-porous Ni samples exhibited significantly enhanced mechanical properties, compared to those of the macro-porous Ni samples.

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Identification and Three-Dimensional Characterization of Micropore Networks Developed in Granite using Micro-Focus X-ray CT

  • Choo, Chang-Oh;Takahashi, Manabu;Jeong, Gyo-Cheol
    • The Journal of Engineering Geology
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    • v.24 no.2
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    • pp.179-189
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    • 2014
  • We analyzed the three-dimensional distribution of micropores and internal structures in both fresh and weathered granite using micro-focus X-ray computed tomography (micro-CT). Results show that the pore radius in fresh granite is mostly in the range of $17-50{\mu}m$, the throat radius is in the range of $5-25{\mu}m$, and the coordination number (CN) of pores is less than 10. In contrast, the pore radius in weathered granite is mostly in the range of $20-80{\mu}m$, the throat radius is in the range of $8-30{\mu}m$, and the CN is less than 12. In general, a positive linear relationship exists between pore radius and CN. In addition, both the size and the density of pores increase with an increasing degree of rock weathering. The size of the throats that connect the pores also increases with an increasing degree of weathering, which induces fracture propagation in rocks. Micro-CT is a powerful and versatile approach for investigating the three-dimensional distributions of pores and fracture structures in rocks, and for quantitatively assessing the degree of pore connectivity.

Development of the Experimental Apparatus to Measure a Pore Size of Micro-pore Fabrics Used for a Bedding to Block the House Dust Mite Allergen (집먼지 진드기 알레르겐 차단 침구에 사용되는 극세 공극 직물의 공극 측정을 위한 입자 투과 실험 장치의 개발)

  • Kim, Donhue
    • Korean Chemical Engineering Research
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    • v.60 no.4
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    • pp.557-563
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    • 2022
  • In order to measure the allergen penetration of micropore fabrics, it is necessary to develop a convenient and appropriate experimental method for measuring a pore size of micropore fabrics. In this study, a simple and economical experimental apparatus was developed for the analysis of the pore size of micropore fabrics by measuring the weight reduction rate. In addition, the allergen blocking properties was evaluated by measuring the pore sizes of various fabrics. According to this study, the size of the pores of the microporous fabric could be obtained by measuring the weight reduction rates. In addition, higher weight reduction rate was obtained as the suction pressure passing through the particle permeation device decreased and the suction time was increased. It is expected that the developed experimental method and apparatus can be utilized as an experimental standard for quality control methods to verify the effectiveness of micropore fabrics used for house dust mite blocking bedding.

The Analysis of the Micro-structure of Oxygen Plasma Treated PET Using a Nitrogen Porosimeter (Nitrogen Porosimeter를 이용한 산소 플라즈마 처리 PET의 미세구조 분석)

  • 김병인;김태경;조규민;임용진
    • Textile Coloration and Finishing
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    • v.11 no.6
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    • pp.1-6
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    • 1999
  • The porosities of PET fibers were investigated using a nitrogen porosimeter according to oxygen plasma treatment and dyeing with a disperse dye, and they were discussed in terms of the change of internal micro-structure of the PET fiber. The total pore volume, surface area and average pore size of the plasma treated PET fibers increased expectably compared with the untreated sample. The PET fibers treated with oxygen plasma and then dyed with a disperse dye were increased significantly in the surface area and the total pore volume comparing with those of plasma treated only, but decreased in the average pore size. The increase of the surface area, after dyeing, of the plasma treated PET fibers was due to addition of the surface area of the dye itself to that of the PET fiber. The increase of the total pore volume of the plasma treated PET fibers by dyeing, which is the opposite result to the general idea that the pore volume of fibers would be reduced by occupation of dye molecules in the pores, could be explained by the free-volume model. This is that the amorphous region in the fiber expanded by occupation of dye molecules, and the marginal space surrounding dyes was generated as many smaller pores, and the decrease of the average pore size of the dyed sample also could be explained The decrease of the average pore size was caused by the splitting of a larger pore into smaller pores.

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Porosity and pore size distribution in high-viscosity and conventional glass ionomer cements: a micro-computed tomography study

  • Aline Borburema Neves ;Laisa Inara Gracindo Lopes;Tamiris Gomes Bergstrom;Aline Saddock Sa da Silva ;Ricardo Tadeu Lopes ;Aline de Almeida Neves
    • Restorative Dentistry and Endodontics
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    • v.46 no.4
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    • pp.57.1-57.9
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    • 2021
  • Objectives: This study aimed to compare and evaluate the porosity and pore size distribution of high-viscosity glass ionomer cements (HVGICs) and conventional glass ionomer cements (GICs) using micro-computed tomography (micro-CT). Materials and Methods: Forty cylindrical specimens (n = 10) were produced in standardized molds using HVGICs and conventional GICs (Ketac Molar Easymix, Vitro Molar, MaxxionR, and Riva Self-Cure). The specimens were prepared according to ISO 9917-1 standards, scanned in a high-energy micro-CT device, and reconstructed using specific parameters. After reconstruction, segmentation procedures, and image analysis, total porosity and pore size distribution were obtained for specimens in each group. After checking the normality of the data distribution, the Kruskal-Wallis test followed by the Student-Newman-Keuls test was used to detect differences in porosity among the experimental groups with a 5% significance level. Results: Ketac Molar Easymix showed statistically significantly lower total porosity (0.15%) than MaxxionR (0.62%), Riva (0.42%), and Vitro Molar (0.57%). The pore size in all experimental cements was within the small-size range (< 0.01 mm3), but Vitro Molar showed statistically significantly more pores/defects with a larger size (> 0.01 mm3). Conclusions: Major differences in porosity and pore size were identified among the evaluated GICs. Among these, the Ketac Molar Easymix HVGIC showed the lowest porosity and void size.

Effect of Ca Implantation on the Sintering and Crack Healing Behavior of High Purity $Al_2$O$_3$ Using Micro-Lithographic Technique -II. Hexagonal Ligaments and Type of Healing (Ion Implantation으로 Ca를 첨가한 단결정 $Al_2$O$_3$의 Crck-Like Pore의 Healing 거동-H. Hexagonal Ligaments and Type of Healing)

  • 김배연
    • Journal of the Korean Ceramic Society
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    • v.36 no.8
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    • pp.813-819
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    • 1999
  • Inner crack-like pores with controlled amount of Ca impurity level in the high purity alumina single crystal sapphire had been created by micro-fabrication technique which includes ion implantation photo-lithography Ar ion milling and hot press technique. The morphological change and the healing of crack-like pore in the Ca doped high purity single crystal alumina during high temperature heat treatment in vacuum were observed using optical microscopy. The hexagonal bridging ligaments were developed and the size of hexagonal bridging ligaments had been increased with temperature and Ca amount and had grown to their corner rounded. It appeared that the hexagonal bridging ligaments would have an equilbrium size with temperature and the amount of Ca addition. Three kinds of crack-like pore healing type were observed. Edge regression and ligament growth were observed from relatively low temperature in the crack-like pore. Edge regression were found in almost all of the crack-like pore but the ligament growth were found only in the several crack-like pores accelerating heating very fast. Flow type healing was observed above $1800^{\circ}C$ and It healed the crack-like pore very slowly.

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Effect of Adsorbent Pore Characteristics on the Removal Efficiency of Smoke Components. (흡착제 세공 특성이 담배연기성분 제거에 미치는 영향)

  • 이영택;김영호;신창호;임광수
    • Journal of the Korean Society of Tobacco Science
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    • v.14 no.1
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    • pp.87-93
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    • 1992
  • The adsorption efficiency of some adsorbents for the organic solvents and gas phase of smoke was investigated. 1. Specific surface area of activated carbon increased to 1900 mfg with increased activation time. 2. Adsorption efficiency of benzene and acetone increased with increasing total surface area. Adsorption capacity for gas phase such as hydrogen cyanide, aldehyde was proportional to the micro pore surface area under 20A. 3. The removal efficiency of particulate matter of smoke was higher with the adsorbents of relatively higher pore size compared to that of micro pore.

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Development of Scent Display Device using Micro-pore Piezo Actuator (마이크로 다공성 압전 진동자를 이용한 발향장치 설계)

  • Lee, Young-Joon;Lim, Seung-Ju;Kim, Min-Ku;Lee, Hae-Lyong;Kim, Jeong-Do
    • Journal of Sensor Science and Technology
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    • v.25 no.6
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    • pp.399-405
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    • 2016
  • Scent diffuser using micro-pore piezo actuator achieved a commercial success because of its cheap production cost, but it is easy to be use for IT-based contents due to difficulty of scent intensity control. To solve this problem, we control the emission amount of scent diffuser by changing amplitude and frequency of input voltage applied to micro-pore piezo actuator. And, we analyzed the effect of density of cotton core on emission amount and a relationship between hole-size of mesh in piezo actuator and viscosity of scents to design a mechanically optimal scent device.

Basic Analysis on Fractal Characteristics of Cement Paste Incorporating Ground Granulated Blast Furnace Slag (고로슬래그 미분말 혼입 시멘트 페이스트의 프랙탈 특성에 관한 기초적 분석)

  • Kim, Jiyoung;Choi, Young Cheol;Choi, Seongcheol
    • Journal of the Korea Concrete Institute
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    • v.29 no.1
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    • pp.101-107
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    • 2017
  • This study aimed to conduct the basic analysis on the fractal characteristics of cementitious materials. The pore structure of cement paste incorporating ground granulated blast furnace slag (GGBFS) was measured using mercury intrusion porosimetry (MIP) and the fractal characteristics were investigated using different models. Because the pore structure of GGBFS-blended cement paste is an irregular system in the various range from nanometer to millimeter, the characteristics of pore region in the different scale may not be adequately described when the fractal dimension was calculated over the whole scale range. While Zhang and Li model enabled analyzing the fraction dimension of pore structure over the three divided scale ranges of micro, small capillary and macro regions, Ji el al. model refined analysis on the fractal characteristics of micro pore region consisting of micro I region corresponding to gel pores and micro II region corresponding to small capillary pores. As the pore size decreased, both models suggested that the pore surface of micro region became more irregular than macro region and the complexity of pores increased.