• 제목/요약/키워드: Micro crack

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마이크로 포커스 X-ray CT를 이용한 콘크리트 손상균열의 정량적 평가 (Quantitative Evaluation of Concrete Damage by X-ray CT Methods)

  • 정자혜
    • 지질공학
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    • 제28권3호
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    • pp.455-463
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    • 2018
  • 본 연구에서는 치핑작업중에 콘크리트에 발생할 수 있는 손상균열을 정량분석하기 위해 X-ray CT 이미지를 이용하는 방법을 제안하고자 한다. 이를 위해 치핑작업을 수행한 후, 균열이 발생한 콘크리트 블록을 코어링하여 직경 50 mm, 길이 100 mm의 시편을 준비하였다. 그 후 마이크로 포커스 X-ray CT 촬영을 하여 얻은 이미지를 3D 이미지로 재구성(reconstruction)하였다. 이렇게 얻어진 3D CT 이미지에 3DMA (3 Dimensional Medial axis Analysis)법을 적용하여, 손상 평가 파라메타로 시편의 위치에 따라 균열의 성질을 평가하여 손상을 분석하였다. 분석결과 치핑에 의한 손상은 치핑 표면으로부터 3 cm 깊이까지 발생한 것으로 나타났다. 또한 CT이미지 공간분석법에서 사용되는 여러 파라메타 중 공극률 지표(Porosity index), Burn number 그리고 Medial axis 의 파라메타를 이용해 치핑표면 근처의 손상 분석이 가능하다는 것이 확인되었다. 이 방법은 내부구조에 변화가 발생한 암석을 대상으로 한 연구에서도 비파괴 상태로 내부의 균열 평가, 가시화에 적용가능하다.

Nucleation and growth mechanism of nitride films deposited on glass by unbalanced magnetron sputtering

  • Jung, Min J.;Nam, Kyung H.;Han, Jeon G.
    • 한국표면공학회:학술대회논문집
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    • 한국표면공학회 2001년도 춘계학술발표회 초록집
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    • pp.14-14
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    • 2001
  • Nitride films such as TiN, CrN etc. deposited on glass by PVD processes have been developed for many industrial applications. These nitride films deposited on glass were widely used for not only decorative and optical coatings but also wear and corrosion resistance coatings employed as dies and molds made of glass for the example of lens forming molds. However, the major problem of nitride coatings on glass by PVD process is non-uniform film owing to pin-hole and micro crack. It is estimated that nonuniform coating is influenced by a different surface energy between metal nitrides and glass due to binding states. In this work, therefore, for the evaluation of nucleation and growth mechanism of nitride films on glass TiN and CrN film were synthesized on glass with various nitrogen partial pressure by unbalanced magnetron sputtering. Prior to deposition, for the examination of relationship between surface energy and film microstructure plasma pre-treatment process was carried out with various argon to hydrogen flow rate and substrate bias voltage, duty cycle and frequency by using pulsed DC power supply. Surface energy owing to the different plasma pre-treatment was calculated by the measurement of wetting angle and surface conditions of glass were investigated by X-ray Photoelectron Spectroscopy(XPS) and Atomic Force Microscope(AFM). The microstructure change of nitride films on glass with increase of film thickness were analyzed by X-Ray Diffraction(XRD) and Scanning Electron Microscopy(SEM).

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비전도성 접착제가 사용된 플립칩 패키지의 신뢰성에 관한 연구 (Characteristics of Reliability for Flip Chip Package with Non-conductive paste)

  • 노보인;이종범;원성호;정승부
    • 마이크로전자및패키징학회지
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    • 제14권4호
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    • pp.9-14
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    • 2007
  • 본 연구에서는 가속화 조건에서의 비전도성 접착제가 사용된 플립칩 패키지의 열적 신뢰성에 관하여 평가하였다. 실리콘 칩에 $17{\mu}m$두께의 Au 범프를 형성하고 무전해 Ni/Au 도금과 Cu 패드의 두께가 각각 $5{\mu}m$$25{\mu}m$로 형성된 연성 기판을 사용하여 플립칩 패키지를 형성하였다. 유리전이온도가 $72^{\circ}C$인 비전도성 접착제를 사용하여 플립칩을 접합시킨 후 열충격 시험과 항온항습 시험을 실시하였다. 열충격 싸이클과 항온항습 유지 시간이 증가할수록 플립칩 패키지의 전기 저항이 증가하는 것을 확인할 수 있었다. 이는 Au 범프와 Au 범프 사이의 균열, 칩과 비전도성 접착제 또는 기판과 비전도성 접착제 사이의 층간 분리에 의한 것으로 사료된다. 또한 항온항습 하에서의 전기 저항의 변화가 열충격하에서 보다 큰 것을 확인할 수 있었다. 따라서 비전도성 접착제가 사용된 플립칩 패키지는 온도보다 습기에 더욱 민감하다는 것을 알 수 있었다.

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변형 경화형 시멘트 복합체로 단면 대체된 콘크리트 보의 강도 및 균열손상 제어 특성 (Strength and Crack-Damage Control Characteristics of Concrete Beams Layered with Strain-Hardening Cement Composites (SHCCs))

  • 윤현도;김선우;전에스더;김윤수;장광수
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 2008년도 추계 학술발표회 제20권2호
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    • pp.269-272
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    • 2008
  • 본 연구에서는 취성적인 시멘트 복합체에 2%이내의 단섬유를 보강하여 균열하중이 이후에도 급격한 강도저하 없이 강재와 같은 변형경화 특성을 부여한 신개념의 건설재료인 변형 경화형 시멘트 복합체(SHCC)를 활용한 콘크리트 구조물의 균열제어성능 개선을 위한 방안을 모색하고자 한다. 본 연구에 활용된 SHCC는 물겹합재비 0.45의 시멘트 복합체에 1.3%의 PVA 섬유 및 0.2%의 PE 섬유를 보강하여 제조되었다. 단면 $100{\times}100mm$의 정사각형 단면을 갖는 무근 콘크리트 보와 인장측 하부면에서 30 및 50mm 두께의 콘크리트를 SHCC로 단면 대체한 보의 휨 및 균열진전 과정을 비교하여 본 연구에서 제조된 SHCC에 의한 균열제어성능을 평가하고자 하였다. 인장측 하부면을 SHCC로 대체한 콘크리트 보 실험체의 휨거동 특성 및 균열제어성능은 무근 콘크리트 보에 비하여 크게 개선되었다.

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핵연료 봉의 마찰변태구조 관찰과 프레팅 마멸 특성 (Observation of Tribologically Transformed Structures and fretting Wear Characteristics of Nuclear Fuel Cladding)

  • 김경호;이민구;이창규;위명용;김흥회
    • 대한기계학회논문집A
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    • 제26권12호
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    • pp.2581-2589
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    • 2002
  • In this research, fretting tests were conducted in air to investigate the wear characteristics of fuel cladding materials with the fretting parameters such as normal load, slip amplitude, frequency and the number of cycles. A high frequency fretting wear tester was designed for this experiment by KAERI. After the experiments, the wear volume and the shape of wear contour were measured by the surface roughness tester. Tribologically transformed structures(TTS) were analysed by means of optical and scanning electron microscopes to identify the main wear mechanisms. The results of this study showed that the wear volume were increased with increasing slip amplitude, and the shape of wear contour was transformed V-type to W-type. Also, it was found that the critical slip amplitude was 168${\mu}{\textrm}{m}$. These phenomena mean that wear mechanism transformed partial slip to gross slip to accelerate wear volume. The wear depth increased with an increase of friction coefficient due to increase of normal load and frequency. The fretting wear mechanisms were believed that, after adhesion and surface plastic deformation occurred by relative sliding motion on the contact between two specimens, TTS creation was induced by surface strain hardening and wear debris were detached from the contact surface which were produced by the micro crack propagation and creation.

자동차부품의 마이크로급 표면크랙 탐상을 위한 FEM 를 기반한 와전류 센서 디자인 및 적용 (Application and Design of Eddy Current based on FEM for NDE Inspection of Surface Cracks with Micro Class in Vehicular Parts)

  • 임광희;이슬기;김학준;송성진;우용득;나승우;황우채;이형호
    • 한국정밀공학회지
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    • 제32권6호
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    • pp.529-536
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    • 2015
  • A defect could be generated in bolts for a use of oil filters for the manufacturing process and then may affect to the safety and quality in bolts. Also, fine defects may be imbedded in oil filter system. So it is very important that such defects be investigated and screened during the multiple manufacturing processes. Therefore, in order effectively to evaluate the fine defects, the FEM simulations were performed to make characterization in the crack detection of the bolts and the parameters such as number of turns of the coil, the coil size, applied frequency were calculated based on the simulation results. Simulations were carried out for the defect signal of eddy current probe. Exciter and receiver were utilized. In this paper, the FEM simulations were performed in both bobbin-type and pancake-type probe, both probes were optimized under Eddy current FEM simulations and the results of calculation were discussed.

음향방출법에 의한 고강도 구조용 내화강의 열화특성에 관한 연구 (A Study on Degradation Characteristic of High Strength Fire Resistance Steel for Frame Structure by Acoustic Emission)

  • 김현수;강창룡;남기우;김부안
    • 열처리공학회지
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    • 제13권5호
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    • pp.309-317
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    • 2000
  • Demand for new nondestructive evaluations is growing to detect tensile crack growth behavior to predict long term performance of materials and structure in aggressive environments, especially when they are in non-visible area. Acoustic emission technique is well suited to these problems and has drawn a keen interests because of its dynamic detection ability, extreme sensitivity and location of growing defects. In this study, we investigated the strength of fire resistance steel for frame structure by tensile test after degradation treatment and analysed acoustic emission signals obtained from tensile test with time frequency analysis methods. In the T and TN specimens(under $600^{\circ}C$-10min ) consisting of ferrite and pearlite structure, most of acoustic emission events were produced near yield point, mainly due to the dislocation activities during the deformation. However, B specimen under $600^{\circ}C$-10min had a two peak which was attribute to the presence of martensite phase. The first peak is before yield point and the second after yield point. The sources of second acoustic emission peak were the debonding of martensite-martensite interface and the micro-cracking of brittle martensite phase. In $600^{\circ}C$-30min to $700^{\circ}C$-60min, many signals were observed before yield point and were decreased after yield point.

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촉진열화실험에 의한 소나무의 물성 및 조직 변화에 대한 연구 (Study on the Change of Physical and Anatomical Properties in the Pine Wood by Accelerated Weathering Test)

  • 김광철
    • 한국가구학회지
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    • 제23권3호
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    • pp.324-331
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    • 2012
  • The domestic pine was used to investigate the change of specific gravity, moisture contents, color and anatomical structure by accelerated weathering test (AWT). According to visual inspection, a few knot separation and looseness as well as considerable surface discoloration was found out. However, the crack and split of surface texture have been never occurred till the last step of AWT. On the whole, as the time of accelerated weathering test has increased, the specific gravity has decreased. Finally, after the 9th week of AWT, the specific gravity was 0.38 that reached to 82% compared to the control specimen. In case of moisture content (MC), it showed rising trend in its early stages, however, after 3th week of AWT it have displayed steady state. A deterioration of cell-wall components was not remarkably observed by scanning electron microscope (SEM), however the ray fractures of AWT specimen were observed more than those of control specimen. The full fracture of epithelial cell around resin canal was observed by optical microscope. The fracture of ray of 2th cycle AWT specimen was first, followed by 1th week and control group. A distortion of tracheid for early spring wood and fracture of epithelial cell were generally observed by a similar level, regardless of duration time of AWT. Therefore, it is obvious that increasing duration time of AWT does not affect the deterioration of micro-structure for wood members from this study. Although a considerable change of anatomical properties was not found, there is a need of further research to understand how will the changes of specific gravity and MC on the physical properties of wood member.

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A319 알루미늄 합금 표면에 Al-36%Si 합금분말의 레이저 클래딩에 의한 내마모성 향상 (Laser Cladding with Al-36%Si Powder Paste on A319 Al Alloy Surface to Improve Wear Resistance)

  • 이형근
    • Journal of Welding and Joining
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    • 제35권2호
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    • pp.58-62
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    • 2017
  • A319 aluminum alloy containing 6.5% Si and 3.5% Cu as major alloying elements has been widely used in machinery parts because of its excellent castability and crack resistance. However it needs more wear resistance to extend its usage to the severe wear environments. It has been known that hyper-eutectic Al-Si alloy having more than 12.6% Si contains pro-eutectic Si particles, which give better wear resistance and lubrication characteristics than hypo-eutectic Al-Si alloy like A319 alloy. In this study, it was tried to clad hyper-eutectic Al-Si alloy on the surface of A319 alloy. In the experiments, Al-36%Si alloy powder was mixed with organic binder to make a fluidic paste. The paste was screen-printed on the A319 alloy surface, melted by pulsed Nd:YAG laser and alloyed with the A319 base alloy. As experimental parameters, the average laser power was changed to 111 W, 202 W and 280 W. With increasing the average laser power, the melting depth was changed to $142{\mu}m$, $205{\mu}m$ and $245{\mu}m$, and the dilution rate to 67.2 %, 72.4 % and 75.7 %, and the Si content in the cladding layer to 16.2 %, 14.6 % and 13.7 %, respectively. The cross-section of the cladding layer showed very fine eutectic microstructure even though it was hyper-eutectic Al-Si alloy. This seems to be due to the rapid solidification of the melted spot by single laser pulse. The average hardness for the three cladding layers was HV175, which was much higher than HV96 of A319 base alloy. From the block-on-roll wear tests, A319 alloy had a wear loss of 5.8 mg, but the three cladding layers had an average wear loss of 3.5 mg, which meant that an increase of 40 % in wear resistance was obtained by laser cladding.

해사를 사용한 초기재령 콘크리트의 일축 구속 거동 해석 (Analysis of Axial Restrained Behavior of Early-Age Concrete Using Sea-Sand)

  • 박상순;송하원;조호진;변근주
    • 콘크리트학회논문집
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    • 제14권3호
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    • pp.331-340
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    • 2002
  • 본 연구에서는 해사를 사용한 초기재령 콘크리트의 자기 및 건조 수축의 구속에 의한 균열발생을 재현하기 위해 유한요소 해석을 실시하였다. 이를 위해 미시역학적 관점에서 열역학적 평형관계를 토대로 해사를 사용한 초기재령 콘크리트의 수화발열 모델, 수분이동 모델 및 건조수축 예측 모델 등의 재료 모델을 정립하여 해석알고리즘을 제안하였고 초기재령에서 해사를 사용 한 콘크리트의 자기 및 건조수축의 구속에 의해서 발생하는 구속응력의 경시변화와 그에 따른 균열발생 및 시기에 관한 균열평가를 목적으로 염분 함유량을 변화시킨 콘크리트의 시편에 대하여 일축 방향 변형구속 실험을 실시하였다. 실험결과 초기재령 콘크리트내 염분 함유량의 증가가 강도발현에 큰 영향을 미치지 못하는 반면 건조수축량을 증가시키므로 일축 방향 변형 구속시 동일 재령에서 높은 구속인장력이 발생하고 그로 인해 균열발생시기를 앞당기는 것을 밝혔다. 또한 구속시험과 동일한 조건으로 해사를 사용한 콘크리트 시편에 대한 응력해석을 실시하여 부재내부에 도입된 건조수축 응력 및 균열 발생의 시간 의존적 변화를 재현하여 그 타당성을 실험결과와 비교를 통해 검증하였다.