• Journal of the Korean institute of surface engineering
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• v.43 no.5
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• pp.224-229
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• 2010

$Ni-Si_3N_4$ nano-composite coatings were prepared by pulse current (PC) electrodeposition and direct current (DC) electrodeposition techniques. The micro-structure of the coatings was characterized by scanning electron microscopy (SEM), vickers microhardness, X-Ray Diffraction (XRD) and wear-friction tests. The results showed that the micro-structure and wear performance of the coatings were affected by the electrodeposition techniques. Pulse current electrodeposited $Ni-Si_3N_4$ composite coatings exhibited higher microhardness, smooth surface, and better wear resistance properties as compared to coatings prepared under DC condition. The $Ni-Si_3N_4$ composite coatings prepared at 50 Hz pulse frequency with 10% duty cycles has shown higher codeposition of nano-particles. Consequently, increased microhardness and less plastic deformations occurred in coatings during sliding wear test. The XRD patterns revealed that the increased pulse frequencies changed the preferred (100) nickel crystallite orientations into mixed (111) and (100) orientations.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2004.04a
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• pp.67-70
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• 2004

An investigation was performed to study the impact damage of the laminated composite plates caused by a low- velocity foreign object with multi-scale modeling based on the concepts of Direct Numerical Simulation (DNS)[4]. In the micro-scale part, we discretize the composite plates through separate modeling of fiber and matrix for the local microscopic analysis. A micro-scalemodel was developed for predicting the initiation of the damage and the extent of the final damage as a function of material properties, laminate configuration and the impactor's mass, etc. Anda macro-scale model was developed for description of global dynamic behavior. The connection betweenmicroscopic and macroscopic is implemented by the tied interface constraints of LS-DYNA contact card. A transient dynamic finite element analysis was adopted for calculating the contact force history and the stresses and strains inside the composites during impact resulting from a point-nose impactor. The low-velocity impact events such as contact force, deformation, etc. are simulated in the macroscopic sense and the impact damages, fiber-breakage, matrix cracking and delamination etc. are examined in the microscopic sense.

• Advances in nano research
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• v.5 no.4
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• pp.337-357
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• 2017

Knowledge of thin films mechanical properties is strongly associated to the reliability and the performances of Nano Electro Mechanical Systems (NEMS). In the literature, there are several methods for micro materials characterization. Bulge test is an established nondestructive technique for studying the mechanical properties of thin films. This study improve the performances of NEMS by investigating the mechanical behavior of Nano rectangular thin film (NRTF) made of new material embedded in Nano Electro Mechanical Systems (NEMS) by developing the bulge test technique. The NRTF built from adhesively-bonded layers of basalt fiber reinforced polymer (BFRP) laminate composite materials in Nano size at room temperature and were used for plane-strain bulging. The NRTF is first pre-stressed to ensure that is no initial deflection before applied the loads on NRTF and then clamped between two plates. A differential pressure is applying to a deformation of the laminated composite NRTF. This makes the plane-strain bulge test idea for studying the mechanical behavior of laminated composite NRTF in both the elastic and plastic regimes. An exact solution of governing equations for symmetric cross-ply BFRP laminated composite NRTF was established with taking in-to account the effect of the residual strength from pre-stressed loading. The stress-strain relationship of the BFRP laminated composite NRTF was determined by hydraulic bulging test. The NRTF thickness gradation in different points of hemisphere formed in bulge test was analysed.

• Advances in nano research
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• v.14 no.5
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• pp.443-450
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• 2023

Carbon nanotubes (CNTs) have received increased interest in reinforcing research for polymer matrix composites due to their exceptional mechanical characteristics. Its high surface area/volume ratio and aspect ratio enable polymer-based composites to make the most of its features. This study focuses on the experimental tensile testing and fabrication of carbon nanotube reinforced composite (CNTRC) beams, exploring various micromechanical models. By examining the performance of these models alongside experimental results, the research aims to better understand and optimize the mechanical properties of CNTRC materials. Tensile properties of neat epoxy and 0.3%; 0.4% and 0.5% by CNT reinforced laminated single layer (0°/90°) carbon fiber composite beams were investigated. The composite plates were produced in accordance with ASTM D7264 standard. The tensile test was performed in order to see the mechanical properties of the composite beams. The results showed that the optimum amount of CNT was 0.3% based on the tensile capacity. The capacity was significantly reduced when 0.4% CNT was utilized. Moreover, the experimental results are compared with Finite Element Models using ABAQUS. Hashin Failure Criteria was utilized to predict the tensile capacity. Good conformance was observed between experimental and numerical models. More importantly is that Young' Moduli of the specimens is compared with the prediction Halpin-Tsai and Mixture-Rule. Although Halpin-Tsai can accurately predict the Young's Moduli of the specimens, the accuracy of Mixture-Rule was significantly low.

• Transactions on Electrical and Electronic Materials
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• v.13 no.5
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• pp.248-251
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• 2012

In order to develop a high voltage insulation material, epoxy/micro-silica composites (EMC) and epoxy/micro-silica/nano-silica composites (EMNC) with three different particle sizes in ${\mu}m$ and one particle size in nm were prepared and their tensile and flexural tests were carried out and the data was estimated by Weibull statistical analysis. The tensile strength of the neat epoxy was 82.8 MPa and those of the EMCs were larger than that of the neat epoxy, and they were much more advanced by the addition of 10 nm sized nano-silica to the EMCs. Flexural strength showed the same tendency of the tensile strength. As the micro-particle size decreased, tensile and flexural strength increased.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2003.10a
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• pp.99-102
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• 2003

This paper aims to observe the micro-mechanical behaviour of tow geometry during deformation of dry woven carbon-fiber fabric. With the increment of shear angle fabric experiences 'lock-up'phenomenon. In this paper, deformation of micro-mechanical parameters such as tow interval, change in tow amplitude and wavelength are investigated. To observe the micro-deformation of the fabric structure, appropriate specimens from bias extension and biaxial tests are sectioned and observed under the microscope. It was found that different loading conditions cause geometric deferences in the tow architecture.

• Korean Journal of Materials Research
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• v.29 no.4
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• pp.221-227
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• 2019

This study examines the role of the nano- and micro-particle ratio in dispersion stability and mechanical properties of composite resins for SLA(stereolithography) 3D printing technology. VTES(vinyltriethoxysilane)-coated $ZrO_2$ ceramic particles with different nano- and micro-particle ratios are prepared by a hydrolysis and condensation reaction and then dispersed in commercial photopolymer (High-temp) based on interpenetrating networks(IPNs). The coating characteristics of VTES-coated $ZrO_2$ particles are observed by FE-TEM and FT-IR. The rheological properties of VTES-coated $ZrO_2/High-temp$ composite solution with different particle ratios are investigated by rheometer, and the dispersion properties of the composite solution are confirmed by relaxation NMR and Turbiscan. The mechanical properties of 3D-printed objects are measured by a tensile test and nanoindenter. To investigate the aggregation and dispersion properties of VTES-coated $ZrO_2$ ceramic particles with different particle ratios, we observe the cross-sectional images of 3D printed objects using FE-SEM. The 3D printed objects of the composite solution with nano-particles of 80 % demonstrate improved mechanical characteristics.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2002.10a
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• pp.689-692
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• 2002

Composite materials, when damaged under thermal or mechanical loadings, show property changes. Among many mechanical properties of composite materials. the stiffness tend to be reduced due to micro-cracking, debonding, or delamination caused by external loadings. This research presents results regarding the detecting technique of internal damages within composite that experienced low-velocity impacts. Post-damage evaluations were made experimentally using flexural and compression loadings. Preliminary finite element analysis was made and compared with analytical solutions. The experimental results to determine the degree of damage will be compared with finite element results.

• Journal of the Korean institute of surface engineering
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• v.30 no.5
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• pp.347-354
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• 1997

Composite plating is a method of co-depositing fine particles of metallic, non-metallic compound or polymers in the plated layer to improve material properties such as were-resistance, lubrication, or corrosion resistance. Graded Ni-Sic composite coating were produced in this research. Prior to produce Graded Ni-SiC composite coatings, effects of particle size, particle content, pH of electrolyte, temperature, current density, stirring rate on the amount of SiC deposited in the Ni layer were investigated. By manipulating current density and plating time properties of these coating were evaluated by micro-indentation hardness test.

• Proceedings of the Korea Concrete Institute Conference
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• 2003.11a
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• pp.244-247
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• 2003

Recently, construction materials have been quickly advancing. Especially, the rate of development of cement based construction materials is much quicker than steel or composite materials. In order to optimize the ductility and strength of cement based materials, Micro-Mechanics based fiber concrete called Engineered Cement Composite (ECC) has been developed and studied extensively by many researchers in the field due to ECC's remarkable flexural strain and strength capacities, many leading nation (i.e., US, Japan and European countries have reached the point of being able to use ECC in actual constructions. But, due to the belated interest in the field, Korea is lagging behind the leading countries. ECC's ability to use its short fibers to bridge micro-cracks (50-80㎛ in width) allows great ductility and strength. In this study, it is confirmed excellency of ECC through the test of tensile strength.