• Title/Summary/Keyword: Mg 입자

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자기연마를 이용한 Al평판 연마의 특성

  • Yeo, Woo-Seok;Park, Won-Kyu;Kim, Yul-Tae;Choi, Hwan;Lee, Jong-Chan;Jung, Sun-Hwan
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2003.10a
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    • pp.82-82
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    • 2003
  • 산업이 발전함에 따라 연마 후의 요구 정밀도도 더욱 높아지고 있다. 하지만 일반적인 기계 가공으로는 연마하기 힘든 부위가 아직 너무 많은 것이 현실이다. 곡관부, 관내부, 가공물 사이에 있는 틈새부 등이 그 예이다. 따라서 본 연구에서는 일반적인 기계 가공으로 연마하기 어려운 틈새부의 연마를 하기 위한 기본적인 자기 연마 특성을 관찰 하고자 하는 것이다. 본 연구에서 사용하는 Al은 Al-Mg합금으로 비열처리 5xxx계열이다. 이 합금은 고강도를 가지고 있으면서, 해수에 대한 내식성이 우수하여 널리 이용되는 금속이다. 본 연구에서 사용되는 실험 장치는 두개의 극(N-S) 사이에 연마 입자를 투입하여 브릿지를 형성한다. 이 브릿지 사이를 Al합금이 두개의 서버 모터에 의해 상대적인 운동을 하게 한다. 연마는 이러한 상대 운동을 이용하는 원리이다. 본 연구에서 이루어지는 실험은 연마 입자의 성분비와 양, 그리고 가공시간 등의 변수를 이용하여 가장 우수한 연마 조건을 선택하고자 한다. 차후 연구 과제는 본 연구에서 얻어지는 연마 특성을 이용하여 두 개의 평판 혹은 어려 개의 Al평판의 틈 즉, 일반적인 기계 가공으로 연마하기 힘든 부위의 연마에 적용하여 그 특성을 알아보고, 일선 산업 현장에 응용 가치를 알아보고자 한다.

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Development of Aerosol-LIBS (Laser Induced Breakdown Spectroscopy) for Real-time Monitoring of Process-induced Particles (공정 중 발생 오염입자 실시간 모니터링을 위한 에어로졸-레이저 유도 플라즈마 분광분석 시스템 개발)

  • Kim, Gibaek;Kim, Kyoungtae;Maeng, Hyunok;Lee, Hae Bum;Park, Kihong
    • Particle and aerosol research
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    • v.12 no.3
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    • pp.57-63
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    • 2016
  • The laser-induced breakdown spectroscopy (LIBS) has been used for rapid detection of elemental compositions of various materials in multi-media (solid, liquid, gas, and aerosols). In this study, the aerosol-LIBS has been developed for real-time monitoring of process-induced particles produced during the semiconductor manufacturing. The developed aerosol-LIBS mainly consists of laser, optics, spectrometer, and aerosol chamber. A new aerosol chamber was constructed for the aerosol-LIBS to be applied for various semiconductor manufacturing process, including exhaust tubes, and low pressure and high temperature chamber. The aerosol-LIBS was evaluated by using laboratory generated aerosols for detection of various elements. As a result, P, Fe, Mg, Cu, Co, Ni, Ca, Na, and K emission lines were successfully detected by the aerosol-LIBS. Further evaluation of the aerosol-LIBS is being conducted.

An Experimental Study on Flocculation and Settling of Fine-grained Suspended Sediments (부유물질의 응접작용 및 침전특성에 관한 실험적 연구)

  • Chu, Yong-Shik;Park, Yong-Ahn;Lee, Hee-Jun;Park, Kwang-Soon;Kweon, Su-Jae
    • The Sea:JOURNAL OF THE KOREAN SOCIETY OF OCEANOGRAPHY
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    • v.4 no.1
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    • pp.40-49
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    • 1999
  • A laboratory flume experiment, using turbulence-generating acryl tank and natural sediments, was conducted to investigate the effects of salinity, concentration of suspended sediment, turbulence and clay minerals on the flocculation and settling of fine-grained suspended sediments. While experiments were run, a sequence of water samples were taken near the bottom of the tank to analyze the variations of size distribution and relative contents of clay minerals. The results of the salinity experiment indicate that median settling velocity ($W_{50}$) increases linearly with salinity. Different settling processes of suspended sediments under variable concentrations appear to be predictable, depending upon the range of the suspension concentration. At concentrations less than 200 mg/l, $W_{50}$ is rarely varied with concentration probably because of the individual--grain settling mode. In the range of 200 to 13,000 mg/l show $W_{50}$ and concentration a good relationship following an empirical formula: $W_{50}=0.45C^{0.44}$. This relationship, however, no longer holds in concentrations exceeding 13,000 mg/l; instead, a more or less reverse one is shown. This result suggests an effect of hindered settling. The turbulence effect is somewhat different from that of concentration. Turbulence accelerates the flocculation and settling susepended sediments at low concentration (200 mg/l), whereas at high concentration turbulence breaks floes down and impedes the settling. Size distribution of suspended sediments sampled near the bottom of the tank tend to be more negatively skewed and leptokurtic in turbulent conditions compared to those in static conditions. The clay mineral analysis from the sequential water samples shows that over time the content of smectite decreases most rapidly with illite remaining concentrated in suspension. This means that smectite, among other clay minerals, plays the most effective role in the flocculation of fine-grained sediment in saline water.

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Investigations on High Temperature Filtration System for Particle Removal using Ceramic Candle Filter in the Pilot Scale Vitrification Plant (유리화 공정에서의 세라믹 캔들 필터를 이용한 분진 제거목적의 고온 여과 시스템에 관한 연구)

  • 류보현;박승철;황태원;하종현
    • Proceedings of the Korea Air Pollution Research Association Conference
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    • 2003.05b
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    • pp.391-392
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    • 2003
  • 한전 원자력 환경기술원에서는 중ㆍ저준위 방사성폐기물 유리화 기술의 상용화 가능성을 입증하기 위한 유리화 실증설비를 건설하여 시험 중에 있으며 이 유리화 기술은 유도 가열식 저온로(Cold Crucible Melter, CCM)에 폐기물을 투입하는 기술로서 폐기물의 부피 축소 효과와 더불어 최종 고화물로 생성되는 폐기물의 침출율이 매우 낮은 장점을 지닌다. 이와 같은 유리화 공정은 기존의 소각처리에서와 같이 폐기물의 열적 산화과정에 의해 유해오염가스와 입자성 물질이 발생된다. 따라서 이를 처리하기 위해배기체 처리공정(Off Gas Treatment System, OGTS)을 설치하여 환경 배출기준(SO$_2$300ppm, NO$_2$ 200ppm, CO 600ppm, HCI 50ppm, 분진 100mg/Nm$^3$ 등)을 만족하도록 하였고 특히 입자성 물질은 후단 OGTS나 배관내 침적으로 인한 방사성 오염을 막기 위해 CCM 후단에서 효율적으로 제거되어야만 한다. (중략)

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Design of 1 Ton/Day bench scaled- Particulate Removal Process for IGCC at High Temperature High Pressure (1T/D Bench급 석탄가스화 복합 발전용 고온.고압 집진 공정 설계)

  • 최주홍;박영철;정진도;김종영
    • Proceedings of the Korea Society for Energy Engineering kosee Conference
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    • 1995.05a
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    • pp.146-149
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    • 1995
  • 석탄 가스화 복합발전 시스템(IGCC)에서 집진은 가스 터빈의 입자에 의한 마모와 침식으로부터의 보호와 분진 배출의 환경 규제를 만족하기 위한 필수 공정이다. 특히 고온고압에서 집진이 수행되면 시스템의 열효율 향상은 물론 가스정제 시스템을 간단히 함으로써 건설비와 운전비의 절감에도 큰 효과를 거둘 수 있다. 석탄 가스화 공정에서 평균 입경이 2 - 3$\mu\textrm{m}$의 입자가 10g/m이상으로 발생되는 농도를 10mg/m이하로 처리하기 위하여 많은 집진 시스템이 제안되고 있지만 IGCC에 도입하기 위한 집진시스템으로서 세라믹 캔들 필터가 제일 타당하다. 세라믹 캔들 필터로 절데 집진 일경이 5$\mu\textrm{m}$이하이고 전체 집진 효율을 99.6% 이상 수행할 수 있다. 세라믹 필터를 이용한 상용화 개발 현황은 현재 세계적으로 bench급, pilot급, 그리고 상용화급 IGCC공정에 도입되어 그 성능이 검정되고 있으며 본 시스템의 내구성과 안정성이 상용화에 충족한 것으로 판명되고 있다. 본 연구에서는 고온고압용 세라믹 필터 집진시스템을 개발하기 위하여 제작된 bench급 집진 공정 및 세라믹 필터설계의 기술적 문제점을 소개하였다.

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제주시 대기부유분진 중 수용성 이온성분의 입경별 분포특성

  • 송정화;박용이;허철구
    • Proceedings of the Korean Environmental Sciences Society Conference
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    • 2004.11a
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    • pp.115-117
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    • 2004
  • 제주시 지역 대기부유분진의 입경별 조성특성을 살펴보기 위하여 제주시청 별관 옥상에서 다단계 분진 포집기(8-stage non viable cascade impactor)를 사용하여 대기부유분진을 채취하여 분진의 질량농도 및 수용성 이온성분의 입경분포를 조사하였다. 조사결과 제주시 지역의 대기부유분진은 0.9, 5, $9.5{\mu}m$부근에서 peak를 보이는 삼산형분포(tri-modal distribution)를 나타내었고 $Na^+,\;Ca^{2+},\;Mg^{2+}$$Cl^-$와 같이 주로 해염에 기인하는 이온 성분들은 $2.1{\mu}m$이상의 조대입자 영역에 존재하고 있었으며 주로 $4{\mu}m$$9.5{\mu}m$부근에서 peak를 보였다. $NH_4^+,\;K^+,\;SO_4^{2-}$$2.1{\mu}m$이하의 미세입자 영역에 존재하고 있으며 $NO_3^-$의 경우는 계절에 따라 약간의 차이가 있긴 하지만 주로 0.9, 4, $9.5{\mu}m$에서 peak를 나타내고 있다.

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Effect of Coagulants on the Behavior of Ultra Fine Dust in a Coal Firing Boiler (석탄 화력 보일러에서의 응집제 이용에 따른 초미세먼지 거동)

  • Ryu, Hwanwoo;Song, Byungho
    • Applied Chemistry for Engineering
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    • v.31 no.1
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    • pp.84-89
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    • 2020
  • Particulate matters of PM2.5, particularly focusing on 0.1~1 ㎛ decrease the efficiency of dust-collector due to the brownian-motion. This study is to verify the effect of coagulant on the particle size distributions of potassium and PM2.5. The activated coagulant was spayed to the coal fired fluidized bed combustion boiler by the weight ratio of 1,200 : 1 = coal : coagulant, and the size distributions of captured particles at both the cyclone (FP) and electrostatic precipitator (EP) were measured. As the result of XRP analysis, the potassium content of FP increased to 13.33% (averagely from 1.65% to 1.87%) and, in EP at 17.68% (averagely from 1.65% to 2.03%). And it was confirmed by the particle size distribution analyzer and SEM image analysis that the distribution rates of PM2.5 decreased at 89.53% on average in FP, and at 88.57% in EP. The total dust concentration (mg/㎥) confirmed by tele-monitering system (TMS) decreased during the primary test from 2.6 to 1.7~1.9 and also the secondary test from 2.9 to 1.7~1.9.

Selective Removal of Arsenic Compounds from the Contaminated Paddy Soil in China Using Froth Flotation Technique (포말부선 기술을 이용한 중국 오염농경지내 비소화합물의 선택적 제거)

  • Lee, Seungwoo;Jeon, Chilsung;Lee, Eunseong;Yoo, Kyungmin;Choi, Junhyun;Kim, Hyunjung
    • Journal of Korean Society of Environmental Engineers
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    • v.38 no.7
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    • pp.343-352
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    • 2016
  • Effects of grinding time and chemicals dosage in arsenic removal from contaminated paddy soil in China were investigated using lab scale attrition and froth flotation combining process. Arsenic concentration in the field soil was 76.51 mg/kg, exceeding Korean and Chinese standards, and predominant arsenic compounds fraction in sequential extraction was "residual" (over 80%). After wet sieving, soil with >2 mm and < 0.038 mm showed concentration lower than 'Warning Level' in Korea. Soil with 0.038-0.075 mm, showing the highest concentration, was discarded since it occupied minor weight fraction (10.1%). Thus soil between 0.075 and 2 mm was only used in the combining process. The highest Arsenic concentration in progeny fragments smaller than 0.038 mm reached up to 981.66 mg/kg after 5 min of attrition. Optimal dosage of collector ($C_5H_{11}OCS_2K$) and modifier ($Na_2S$ and $CuSO_4$) in froth flotation process for the selective separation of the chipped progeny particles from the parent fragments were determined both as 200 g/ton. Arsenic removal efficiency in froth flotation process was 38.47% and it was increased to 72.74% in additional flotation process, scavenging. Average arsenic concentration after overall process - wet sieving, attrition and froth flotation - was estimated to 16.45 mg/kg.

A Study on the Mill Scale Pretreatment and Magnetite Production for Phosphate Adsorption (인 흡착을 위한 Mill Scale 전처리 및 Magnetite 제조 연구)

  • Chun, Hyuncheol;Choi, Younggyun
    • Journal of Korean Society of Environmental Engineers
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    • v.37 no.4
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    • pp.246-252
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    • 2015
  • In steel factory, hot roller cleaning process produces a lot of iron oxide particles called as mill scale. Major components of these particles are wustite (FeO), magnetite ($Fe_3O_4$), and hematite ($Fe_2O_3$). In this study, we tried to produce pure magnetite from the mill scale because of the largest phosphate adsorption capacity of the magnetite. The mill scale was treated with acid (HCl+$H_2O_2$), base (NaOH), and acid-base ($H_2SO_4$+NaOH). Batch adsorption tests showed the acid and/or base treatment could increase the phosphate adsorption capacity of the iron oxides from 0.28 to over 3.11 mgP/g. Magnetite, which could be obtained by acid and base treatment of the mill scale, showed the best adsorption capacity. From the kinetic analysis, both Freundlich and Langmuir isotherm well described the phosphate adsorption behavior of the magnetite. In Langmuir model, maximum phosphate adsorption capacity was found to be 5.1 mgP/g at $20^{\circ}C$.

Densification and Grain Growth Behavior of MgO and TiO2-doped Alumina (MgO 및 TiO2가 첨가된 알루미나의 치밀화와 입성장 거동)

  • Lee, Jung-A;Kim, Jeong-Joo
    • Journal of the Korean Ceramic Society
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    • v.39 no.11
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    • pp.1083-1089
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    • 2002
  • Densification and grain growth behavior of MgO and -doped alumina ceramics were investigated. MgO was found to inhibit grain growth and to promote densification, but acted to promote grain growth more than densification. The density which showed the maximum shrinkage rate was investigated in the plot of shrinkage rate versus density. The data suggests that the maximum shrinkage rate separates the two kinetic regimes, below the density of maximum shrinkage, the regime associated with densification and above the maxima, the regime associated with the grain growth. The plot exhibits a maximum which shifts to higher temperatures with MgO doping and to lower with doping.