• Title/Summary/Keyword: Metal bond

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A STUDY ON THE BOND STRENGTH BETWEEN REUSED DENTAL ALLOYS AND PORCELAIN (치과 도재용 금속의 재사용에 따른 금속과 도재간의 결합 강도에 관한 연구)

  • Kim, In;Yang, Hong-So
    • The Journal of Korean Academy of Prosthodontics
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    • v.31 no.2
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    • pp.181-190
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    • 1993
  • The purpose of this study was to evaluate the effect of shear bond strength between various percentage of reused dental ceramic alloys and porcelain. One hundred specimens were made of one semiprecious alloy and three nonprecious alloys. Each alloy group was subdevided into five groups according to the additional precentage of new alloy. Group I specimens were made of 100% new alloy and served as the control of the investigation. Group II specimens were made of once-cast alloy with 75% new alloy. Group III specimens were made of once-cast alloy with 50% new alloy. Group IV specimens were made of once-cast alloy with 25% new alloy. Group V specimens were made of 100% recast alloy. Five specimens were made for each group of the alloy combinations. The test specimens were prepared by firing porcelain doughnuts on the alloy rod surface, and invested in dental stone. Bond strengths were measured by Instron universal testing machine at a crosshead speed of 0.5mm/min. The fractured surface of metal specimens were examined under the scanning electron microscope. The obtained results were as follows : 1. The shear bond strength of Albabond showed no significant difference between control group and reused alloy group. 2. The shear bond strength of reused alloy groups of nonprecious alloys were lower than that of control groups. 3. The shear bond strength between porcelain and metal in semiprecious alloy was higher than in nonprecious alloys 4. In nonprecious alloys. Rexillium III showed the highest bond strength value and Excelalloy showed the lowest shear bond strength value. 5. Regardless of the type of alloys and additional proportion of new alloys, scanning electron microscope photographs of the fracture surface between alloy and porcelain revealed simillar semiprecious alloy and nonprecious alloys.

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Computer-Aided Alloy Design of Insert Metal for Transient Liquid Phase Bonding of High Aluminum Ni-base Superalloys

  • Nishimotd, Kazutoshi;Saida, Kazuyoshi
    • Proceedings of the KWS Conference
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    • 2002.10a
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    • pp.803-808
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    • 2002
  • A computer-aided alloy-designing technique to develop the insert metal for transient liquid phase (TLP) bonding was applied to high aluminum Ni-base superalloys. The main procedure of a mathematical programming method was to obtain the optimal chemical composition through rationally compromising the plural objective performances of insert metal by a grid-search which involved data estimation from the limited experimental data using interpolation method. The objective function Z which was introduced as an index of bonding performance of insert metal involved the melting point, hardness (strength), formability of brittle phases and void ratio (bonding defects) in bond layer as the evaluating factors. The contour maps of objective function Z were also obtained applying the interpolation method. The compositions of Ni-3.0%Cr-4.0%B-0.5%Ce (for ${\gamma}$/${\gamma}$/${\beta}$ type alloy) and Ni3.5%Cr-3.5%B-3%Ti (for ${\gamma}$/${\gamma}$ type alloy) which optimized the objective function were determined as insert metal. SEM observations revealed that the microstructure in bond layers using the newly developed insert metals indicated quite sound morphologies without forming microconstituents and voids. The creep rupture properties of both joints were much improved compared to a commercial insert metal of MBF-80 (Ni-15.5%Cr-3.7%B), and were fairly comparable to those of base metals.

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The effect of the gold based bonding agents on the bond between Ni-Cr alloys and ceramic restorations (Ni-Cr합금과 도재간의 결합력에 gold-based bonding agent가 미치는 영향)

  • Lee, Jung-Hwan;Joo, Kyu-Ji
    • Journal of Technologic Dentistry
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    • v.29 no.2
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    • pp.213-223
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    • 2007
  • The success of a porcelain fused to metal (PFM) restoration depends upon the quality of the porcelain-metal bond. The adhesion between metal substructure and dental porcelain is related to the diffusion of oxygen to the reaction layer formed on cast-metal surface during firing. The purposed of this investigation was to study the effects of gold based bonding agent on Ni-Cr alloy-ceramic adhesion between porcelain matrix, gold based bonding agent and metal substructure interface. gold based bonding agent have been applied as an intermediate layer between a metal substructure and a ceramic coating. gold based bonding agent(Aurofilm NP, Metalor, Swiss) was applied on Ni-Cr alloy surface by four method. Surfaces only air abraded with 110${\beta}\neq$ Al2O3 particles were used as control. metal ceramic adhesion was evaluated by a biaxial flexure test(N=5) and volume fraction of adherent porcelain was determined by SEM/EDS analysis. Result of this study suggest that the layering sequence of gold based bonding agent is very important and can improve porcelain adherence to PFM.

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AN EXPERIMENTAL STUDY ON THE RESIDUAL STRESS AND BOND STRENGTH OF CERAMO-METAL SYSTEM (치과도재용(齒科陶材用) 합금(合金)과 도재간(陶材間)의 잔류응력(殘溜應力) 및 결합강도(結合强度)에 관(關)한 실험적(實驗的) 연구(硏究))

  • Kim, Gi-Jin;Bae, Tae-Seong;Song, Kwang-Yeob;Park, Charn-Woon
    • The Journal of Korean Academy of Prosthodontics
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    • v.29 no.2
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    • pp.67-84
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    • 1991
  • This study was carried out to investiagate the residual stress caused by the mismatch of thermal expansion and the bond failure resistance of alloy-porcelain specimens. The thermal expansions of alloys and porcelains were measured by using a straight push-rod dilatometer. Porcelain glass transition temperatures, thermal expansion coefficients, and thermal compatibility indices were derived from length-versus-temperature curves. Strain gauges were used to experimentally determine the Young's moduli of porcelains, the residual stresses of porcelain surface, and tensile bond strengths of the specimens of simulated porcelain metal crown. The obtained results were as follows: 1. The coefficients of thermal expansion for alloys were the minimum of $13.53\mu/^{\circ}C$ and the maximum of $20.11\mu/^{\circ}C$ in the range of $100\sim600^{\circ}C$ and those for porcelains were the minimum of $7.72\mu/^{\circ}C$ and the maximum of $31.24\mu/^{\circ}C$ in the range of $100\sim500^{\circ}C$. 2. The glass transition temperature of porcelains exhibited the same value without my relation to the healing rate, and the thermal disharmony of porcelain and alloy was more affected by porcelains than by the alloys. 3. The Young's moduli of body porcelains were larger than those of opaque porcelains(P<0.01) 4. It seemed that the residual stresses of porcelain surfaces in the porcelainalloy systems were more affected by porcelains than by alleys. 5. The bond strengths of the procelain-base metal alloy systems were larger than those of the porcelain-precious metal alloy systems. The fracture strengths of porcelain surfaces showed significant difference between porcelains (P<0.05).

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The Bonding Strength Characteristic of the Filler Metal Powder on the TLP Bonded Region of Superalloy GTD-111DS (일방향 초내열합금 GTD-111DS에서 삽입금속 분말에 따른 천이액상확산접합부의 접합강도 특성)

  • Oh, In-Seok;Kim, Gil-Moo;Moon, Byeong-Shik
    • Journal of Welding and Joining
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    • v.25 no.5
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    • pp.45-50
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    • 2007
  • The Ni-base superalloy GTD111 DS is used in the first stage blade of high power land-based gas turbines. Advanced repair technologies of the blade have been introduced to the gas turbine industry over recent years. The effect of the filler metal powder on Transient Liquid Phase bonding phenomenon and tensile mechanical properties was investigated on the GTD111 DS superalloy. At the filler metal powder N series, the base metal powders fully melted at the initial time and a large amount of the base metal near the bonded interlayer was dissolved by liquid inter metal. Liquid filler metal powder was eliminated by isothermal solidification which was controlled by the diffusion of B into the base metal. The solids in the bonded interlayer grew from the base metal near the bonded interlayer inward the insert metal during the isothermal solidification. The bond strength of N series filler metal powder was over 1000 MPa. and ${\gamma}'$ phase size of N series TLP bonded region was similar with base metal by influence of Ti, Al elements. At the insert metal powder M series, the Si element fluidity of the filler metal was good but microstructure irregularity on bonded region because of excessive Si element. Nuclear of solids formed not only from the base metal near the bonded interlayer but also from the remained filler metal powder in the bonded interlayer. When the isothermal solidification was finished, the content of the elements in the boned interlayer was approximately equal to that of the base metal. But boride and silicide formed in the base metal near the bonded interlayer. And these boride decreased with the increasing of holding time. The bond strength of M series filler metal powder was about 400 MPa.

Characteristics of Ni-based Alloy Bond in Diamond Tool Using Vacuum Brazing Method

  • An, Sang-Jae;Song, Min-Seok;Jee, Won-Ho
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.1130-1131
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    • 2006
  • We found that the """interface reaction between Ni-based alloy bond, diamond, and steel core is very critical in bond strength of diamond tool. None element from metal bond diffuses into the steel core but the Fe element of steel core was easily diffused into the bond. This diffusion depth of Fe has a great effect on the bonding strength. The Cr in steel core accelerated the Fe diffusion and improved the bond strength, on the other hand, carbon decreased the strength. Ni-based alloy bond including Cr was chemically bonded with diamond by forming Cr carbide. However, the Cr and Fe in STS304 were largely interdiffused, the strength was very low. The Cr passivity layer formed at surface of STS304 made worse strength at commissure in brazing process.

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Study on the Bonding Pad Lift Failure in Wire Bonding (와이어 본딩시 본딩 패드 리프트 불량에 관한 연구)

  • 김경섭;장의구;신영의
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.11 no.12
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    • pp.1079-1083
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    • 1998
  • In this study, ultrasonic power of Aluminum wire bonder, bond time and bond force are investigated and valued in order to minimize failure of bonding pad lift. We also tried to control those 3 factors properly. We got the conclusion that if we turn down the ability of ultrasonic power or bond time, we can get a pad lift from a boundary between bond pad ad wire because pad metal and wire joining is unstable, but it is best condition when it ultrasonic power is 100∼130unit, bond time is 15∼20msec and bond force is 4∼6gf.

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Study about shear bond strength of zirconia core used in dental prosthesis (치과 보철물에 사용되는 지르코니아 코어의 전단결합강도에 관한 연구)

  • Sim, Ji-Young;Kim, Jae-Hong;Kim, Woong-Chul;Kim, Hae-Young;Kim, Ji-Hwan
    • Journal of Technologic Dentistry
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    • v.33 no.4
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    • pp.299-306
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    • 2011
  • Purpose: This study aimed to investigate the shear bond strength by manufacturing the veneering porcelain on the IPS e.max $ZirCAD^{(R)}$ zirconia core, using the layering technique and heat-pressing technique, and to evaluate the clinical stability by comparing to the conventional metal ceramic system. Methods: The Schmitz-Schulmeyer test method was used to evaluate the core-veneer shear bond strength of zirconia core ceramic(IPS e.max $ZirCAD^{(R)}$) and their manufacture recommended two veneering ceramic systems(IPS e.max $ceram^{(R)}$, IPS e. max $ZirPress^{(R)}$). A metal ceramic system(Bellabond $plus^{(R)}$, VITA $VM13^{(R)}$) was used as a control group for the two all ceramic system test groups. The maximum loading and shear bond strength was measured. The average shear strength(MPa) was analyzed with the one-way ANOVA and the Tukey's test(${\alpha}$=.05). The fracture specimens were examined using Microscope to determine the failure pattern. Results: The mean shear bond strengths(SD) in MPa were MBSB control 43.62(2.13); ZBSB 18.65(1.76); ZPSB 18.89(1.54). The shear strengths of the zirconia cores were not significantly different(P>.05). Microscope examination showed that zirconia specimens presented mixed failure, and base metal alloy specimens showed adhesive failure. Conclusion: There was no siginificant different between the layering technique and the heat pressing technique in the veneering methods on the zirconia cores. None of the zirconia core and veneering ceramics could attain the high bond strength values of the metal ceramic combination.

Bond Strength between Co-Cr Alloy Metal and Ceramic (Co-Cr 합금의 금속-도재 결합 강도)

  • Kim, Min-Jeong;Park, Gwang-Sig
    • The Journal of the Korea Contents Association
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    • v.21 no.3
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    • pp.602-608
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    • 2021
  • For the comparison of bond strength between the Co-Cr alloy and ceramic, which are clinically used, test samples made with a traditional casting method as a control group), and Milling and SLM(3d printing group) samples were made as an experimental group. The metal-ceramic bond strength was measured with a universal testing machine. For the measurement, a three-point bending test was conducted. After the bond strength was measured, metal-ceramic interface was observed. According to the test result, casting group had 53.59 MPa, milling group had 45.90 MPa, and 3d printing group had 58.34 MPa. There was no statistical significance. With regard to failure pattern, most of the samples in two groups, showed mixed failure. This study showed a clinically applicable value when measuring the bond strength of alloy-ceramic material with an alloy produced by 3D printing.

Shear bond strength of luting cements to fixed superstructure metal surfaces under various seating forces

  • Ozer, Fusun;Pak-Tunc, Elif;Dagli, Nesrin Esen;Ramachandran, Deepika;Sen, Deniz;Blatz, Markus Bernhard
    • The Journal of Advanced Prosthodontics
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    • v.10 no.5
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    • pp.340-346
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    • 2018
  • PURPOSE. In this study, the shear bond strengths (SBS) of luting cements to fixed superstructure metal surfaces under various seating forces were investigated. MATERIALS AND METHODS. Seven different cements [Polycarboxylate (PCC), Glass-Ionomer (GIC), Zinc phospahate (ZPC), Self-adhesive resin (RXU), Resin (C&B), and Temporary cements ((RXT) and (TCS))] were bonded to a total number of 224 square blocks ($5{\times}5{\times}3mm$) made of one pure metal [Titanium (CP Ti) and two metal alloys [Gold-Platinum (Au-Pt) and Cobalt-Chrome (Co-Cr)] under 10 N and 50 N seating forces. SBS values were determined and data were analyzed with 3-way ANOVA. Pairwise comparisons and interactions among groups were analyzed with Tukey's simultaneous confidence intervals. RESULTS. Overall mean scores indicated that Co-Cr showed the highest SBS values ($1.96{\pm}0.4$) (P<.00), while Au-Pt showed the lowest among all metals tested ($1.57{\pm}0.4$) (P<.00). Except for PCC/CP Ti, RXU/CP Ti, and GIC/Au-Pt factor level combinations (P<.00), the cements tested under 10 N seating force showed no significantly higher SBS values when compared to the values of those tested under 50 N seating force (P>.05). The PCC cement showed the highest mean SBS score ($3.59{\pm}0.07$) among all cements tested (P<.00), while the resin-based temporary luting cement RXT showed the lowest ($0.39{\pm}0.07$) (P<.00). CONCLUSION. Polycarboxylate cement provides reliable bonding performance to metal surfaces. Resin-based temporary luting cements can be used when retrievability is needed. GIC is not suitable for permanent cementation of fixed dental prostheses consisting of CP Ti or Au-Pt substructures.