• Title/Summary/Keyword: Melting point

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Study on the Reduction of Molten EAF Slag (용융 전기로 슬래그의 환원반응에 관한 연구)

  • Joo, Seong-Woong;Shin, Jong-Dae;Shin, Dong-Kyung;Hong, Seong-Hun;Ki, Jun-Sung;Hwang, Jin-Il;You, Byung-Don
    • Korean Journal of Metals and Materials
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    • v.50 no.10
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    • pp.753-761
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    • 2012
  • The reduction behavior of low level oxides such as (T.Fe), (MnO) and ($P_2O_5$) in molten EAF slag was investigated using commercial reductants. In an air atmosphere, the slag volume increased and the reduction rate of the slag was very low due to the oxidation loss of reductants by oxygen in the air. The reduction rate of the slag was also low when a commercial reductant was used alone in an Ar gas atmosphere. The reason is probably because the material transfer through the interface between the slag and reductant is difficult due to the formation of high melting point oxide. When reductants were mixed with burnt lime in order to form low melting point reaction products, the reduction rate of the slag increased up to the range of 45-70%. By using the mixtures of reductants and burnt lime so as to form a low melting point slag at the reaction end, the reduction rate of the slag was improved up to 60-85%.

The scientific analysis of glass beads excavated from Naesanri in Gosung (고대 유리구슬의 재질분석 연구-고성 내산리 출토 유리구슬을 중심으로)

  • Moon, Whan-Suk;Hwang, Jin-Ju;Cho, Nam-Chul;Hong, Jong-Ouk
    • 보존과학연구
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    • s.21
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    • pp.57-75
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    • 2000
  • We performed the scientific analysis through composition analysis, micro-structure investigation, melting point and hardness test to the glass beads excavated at Naesanri in Gosung. Through this investigation, we could examine closely the characterization of raw materials and manufacture technique As a result of micro-structure investigation of glass beads, it appeared that the bubbles in glass beads have remained. Coloring agents of yellow glass bead was remained to the shape of inclusion. And on observing the transparent solid particle, we can know that these do not melt the raw materials because of low melting temperature of a crucible. The result of composition analysis of all glass beads using ICP, these were classified as $Na_2O_2$-$SiO_2$ type of glass. Also, these added to $AI_2O_3$ to improve the durability. The value of Vickers hardness of glass beads appeared the HV 490-530. The HV 1,440 of the transparent solid particle was much more than that of inner glass bead. This means that raw materials do not melt because of a low melting temperature of a crucible. The result of melting temperature analysis of glass beads using DSC/TGA, it was measured about $1,250^{\circ}C$.

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A Study on the Properties and Methods of Electrode System for Tapping of Melts (출탕유도전극을 이용한 용융물의 출탕방법 및 특성에 대한 연구)

  • Moon, Young-Pyo;Choi, Jang-Young
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.65 no.3
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    • pp.499-503
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    • 2016
  • For safety and economy reasons, hazardous waste including radioactive waste is desired to be converted into stable waste forms with a maximum volume reduction. High temperature melting technology using a plasma torch system can effectively treat even the non-flammable waste as desired. By far, one of the most difficult process for melting the non-flammable waste is a tapping of melts because the melting point of a residual slag in the tapping hole is high and because the viscosity of the melt increases sharply when tapping out. In case of a stationary furnace with a slant tapping port on the side of furnace, a certain amount of melts is left in the tapping hole after tapping out. Because of this, at every end of a melting cycle, the tapping hole needs to be opened by tapping device. The developed tapping device of melts based on both a guide electrode and auxiliary electrode is adequate for the application to discharge of melts except that the consumption of the guide electrode is somewhat faster than expected. Melt is collected in the water cooled vessel.

A Study on Snow Melting System for the Anti-freezing Testing Road (시험선로 결빙방지를 위한 융설시스템에 관한 연구)

  • Han, K.I.;Lee, A.H.;Cho, D.H.
    • Journal of Power System Engineering
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    • v.10 no.1
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    • pp.34-40
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    • 2006
  • The snow melting system by electric heating wires which is adopted in this study is a part of road facilities to keep surface temperature of the road higher than freezing point of water for melting the snow accumulated on it. The system is designed to increase traffic safety and capacity. The electric heating wires are buried under paved road at a certain depth and operated automatically and manually. Design theory, amount of heating, and installation standard vary according to economic situation, weather condition, and installation place where the system applies. It is tried to figure out that the appropriate range of required heat capacity and installation depth and intervals for solving snowdrifts and freezing problems with the minimum electric power consumption. The most important factors to design the system are calculation of heating capacity depending on weather condition and depth and interval of the electric heating wires depending on air condition respectively. The study were performed under the range of the air temperatures($-2^{\circ}C,\;-5^{\circ}C,\;-8^{\circ}C$), the intervals of the electric heating wires(70mm, 100mm, 125mm), and the installation depths(50mm, 70mm, 100mm). The ready made commercial program package was used to verify the experimental results.

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A study on the characteristics of Pb free Sn-2%Ag-x%Bi solder alloys (Pb Free Sn-2%Ag-x%Bi계 Solder의 특성에 관한 연구)

  • 흥순국;박일경;강정윤
    • Journal of Welding and Joining
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    • v.16 no.3
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    • pp.148-156
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    • 1998
  • The purpose of this study is to investigate the characteristics of Pb-Free Sn-2%Ag-Bi solder alloys. The solder alloys used in this study is Sn-2%Ag-(3,5,7,9%) Bi It is examined that their properties such as melting range, wettability, microstructure, microhardness, and tensile property. The addition of Bi(3,5,7,9%) lowered the melting point of the solder and the melting range was 196~203$^{\circ}C$. The wettability of the solder as equal to that of Sn-37% Pb solder. The morphology of structure did not change largely by addition of Bi. But the structure of cellular dendrite of linear type displayed. The tensile strength of the solder was superior to that of Sn-37%Pb solder. But the elongation was inferior to that of Sn-37%Pb solder. The hardness of Sn-2%Ag solder was tow times and that of Sn-2%Ag-Bi solder was three times of that in Sn-37%Pb solder. But the effect of increment of Bi content did not change largely.

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The Wetting Properties of UBM-coated Si-wafer to the Lead-free Solders in Si-wafer/Bumps/Glass Flip-Chip Bonding System

  • Hong, Soon-Min;Park, Jae-Yong;Park, Chang-Bae;Jung, Jae-Pil;Kang, Choon-Sik
    • Proceedings of the International Microelectronics And Packaging Society Conference
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    • 2000.04a
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    • pp.74-79
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    • 2000
  • In an attempt to estimate the wetting properties of wettable metal layers by wetting balance method, an analysis of wetting curves of the coating layer was performed. Based on the analysis, wetting properties of UBM-coated Si-plate were estimated by the new wettability indices. The wetting curves of the one and both sides-coated UBM layers have the similar shape and show the similar tendency to the temperature. So the wetting property estimation of one side coating is possible with wetting balance method. For UBM of Si-chip, Cr/Cu/Au UBM is better than Ti/Ni/Au in the point of wetting time. At general reflow temperature, the wettability of high melting point solders(Sn-Sb, Sn-Ag) is better than that of few melting point ones(Sn-Bi, Sn-In).The contact angle of the one side coated plate to the solder can be calculated from the farce balance equation by measuring the static state force and the tilt angle.

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Evaluation of Self-deicing Function of Snow-melting Asphalt (자체 용설 아스팔트 혼합물의 용빙특성 분석)

  • Kim, Kwang-Woo;Lee, Gi-Ho;Hong, Sang-Ki;Jin, Jo-Ill;Doh, Young-Soo
    • International Journal of Highway Engineering
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    • v.5 no.2 s.16
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    • pp.1-14
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    • 2003
  • This study is a fundamental research for developing self-deicing function of snow-melting asphalt concrete for roadway pavement. The objective of this study is to develop technology of making self-snow-melting asphalt pavement and evaluate properties of the asphalt concrete containing deicers. Asphalt concrete with deicers and CRM was produced by dry process. The $\alpha$-deicer, CRM and F-deicer were used for sand asphalt mixtures of thin-layer pavement on the existing pavement. The $\alpha$-deicer, $\beta$-deicer, CRM A, CRM B and C were used for 13mm dense-graded mixtures on surface course. Penetration grade of 60-80 asphalt was used for asphalt mixtures. Marshall mix-design, indirect tensile strength, freezing and thawing test, analysis of extracted water were carried out to evaluate performance of self deicing function of asphalt mixtures. The study result showed that snow-melting asphalt mixtures had not only good mechanical characteristics and good snow-melting function, but also chemically safe in environmental point of view.

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Evaluation on Spalling Properties of Ultra High Strength Concrete with Melting and Vaporization of Fiber (유기섬유의 용융 및 기화에 따른 초고강도 콘크리트의 폭렬 특성 평가)

  • Kim, Gyu-Yong;Choe, Gyeong-Cheol;Lee, Joo-Ha;Lee, Seung-Hoon;Lee, Tae-Gyu
    • Journal of the Korea Concrete Institute
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    • v.24 no.2
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    • pp.173-183
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    • 2012
  • Recently, experimental studies to prevent explosive spalling based on spalling mechanism and addition of Polypropylene fiber in high strength concrete (HSC) are performed actively. However, with respect to ultra high strength concrete (UHSC), its compact internal structure is more difficult release vapor pressure at rapid rising temperature compared to HSC. Therefore, in this study, an experiment was conducted to evaluate spalling properties of UHSC using ${\Box}$ $100mm{\times}100{\times}H200mm$ rectangular specimen according to ISO-834 standard fire curve. With respect melting point of fiber, three fiber types of Polyethylene, Polypropylene, and Nylon fibers with melting temperature of $110^{\circ}C$, $165^{\circ}C$, and $225^{\circ}C$, respectively, were considered. Mixed fiber of 0.15% and 0.25% of concrete volume was used to consider spalling properties based on water vapor pressure release. Then, TGDTA test on fiber and FEM analysis were performed. The results showed that it is difficult to prevent initial spalling without loss of fiber mass even if fiber melting temperature is low. Also, in preventing thermal spalling, fiber that melts to rapidly create porosity within 10 minutes of fire is more effective than that of low melting temperature property of fiber.

A study on the growth mechanism of rutile single crystal by skull melting method and conditions of RF generator (스컬용융법에 의한 루틸 단결정 성장메커니즘과 RE generator 조건에 관한 연구)

  • Seok jeong-Won;Choi Jong-Koen
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.15 no.5
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    • pp.175-181
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    • 2005
  • Ingots of rutile single crystals were grown by the skull melting method, and their characteristics were compared in terms of melt-dwelling time for each melt. The method is based on direct inductive heating of an electrically conducted melt by an alternating RF field, and the heating is performed by absorption of RF energy. $TiO_2$ is an insulator at room temperature but its electric conductivity increases elevated temperature. Therefore, titanium metal ring(outside diameter : 6cm, inside diameter : 4cm, thickness 0.2cm) was embedded into $TiO_2$, powder (anatase phase, CERAC, 3N) for initial RF induction heating. Important factors of the skull melting method are electric resistivity of materials at their melting point, working frequency of RF generator and cold crucible size. In this study, electric resitivity of $TiO_2$, $(10^{-2}\~10^{-1}\;{\Omega}{\cdot}m)$ at its melting point was estimated by compairing the electric resitivities of alumina and zirconia. Inner diameter and height of the cold crucible was 11 and 14cm, respectively, which were determined by considering of the Penetration depth $(0.36\~1.13cm)$ and the frequency of RF generator.

Characterization of PVDF-DBP Materials for Thermally Induced Phase Separation (열유도상분리법 적용을 위한 PVDF-DBP 소재의 특성평가)

  • Kim, Se Jong;Lee, Jeong Woo;Nam, Sang Yong
    • Membrane Journal
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    • v.26 no.6
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    • pp.449-457
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    • 2016
  • In this study, polyvinylidene fluoride (PVDF) membrane with excellent mechanical properties and chemical resistance was prepared and characterized for the application of water treatment. Dibutyl-phthalate (DBP) was used as a diluent for making a membranes through temperature induced phase separation (TIPS) method, and the crystallization temperature, melting point, cloud point and SEM image were observed with different ratio of diluent in polymer/diluent mixture. The crystallization temperature and melting point increased proportionally with the content of polymer, while the cloud point temperature decreased. Finally, it was confirmed that stable membrane could be manufactured at a polymer content of 62 wt% and a temperature $125^{\circ}C$ using the phase diagram of PVDF/DBP mixtures with temperatures.