• Title/Summary/Keyword: Melting Range

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Manganese in Seawaters of the Amundsen Sea, Antarctic (남극 아문젠해에서 해수 중 Mn의 분포 특성)

  • Jang, Dongjun;Choi, Mansik;Park, Jongkyu;Park, Kyungkyu;Hong, Jinsol;Lee, Sanghoon;Jung, Jinyoung
    • Ocean and Polar Research
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    • v.41 no.2
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    • pp.63-77
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    • 2019
  • In order to investigate the behavior and seasonal variability of Mn as one of the bio-essential metals in the Amundsen sea, which is known as the most biologically productive coastal area around the Antartica, seawaters were collected using a clean sampling system for 10 stations (96 ea) in 2014 (ANA04B) and for 12 stations (139 ea) in 2016 (ANA06B) surveys of RV ARAON. Dissolved and particulate Mn concentration varied in the range of 0.15-4.43 nmol/kg and <0.01 to 2.42 nM in 2014 and in the range of 0.25-4.15 nmol/kg and 0.01-2.64 nM in 2016, respectively. From the sectional distribution of dissolved and particulate Mn, it might be suggested that dissolved/particulate Mn was provided from iceberg melting and diffusion/resuspension from sediments, respectively. Although this sea is highly productive, there was little evidence regarding the biological origin of dissolved Mn, but particulate Mn only in sea ice and offshore areas could be explained as originating from organic matters, e.g. phytoplanktons. And it could be suggested that the subsurface maximum of dissolved Mn was formed by isopycnal transport of melting materials from ice wall to offshore. Compared to early (2014) summer, temperature, salinity, biomass, dissolved and particulate Mn in late (2016) summer indicated that temporal variations might be resulted from the reduction of ice melting and mCDW flow, which induced a reduction in resuspension. In addition, in the late summer, particles including biomass were reduced, which brought about a reduction in the removal rate of dissolved Mn.

Improved Thermal Bonding Behaviour of Polypropylene Non-wovens by Blending Different Molecular Weights of PP

  • Deopura, B.L.;Mattu, Ankush;Jain, Anurag;Alagirusamy, R.
    • Fibers and Polymers
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    • v.3 no.1
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    • pp.38-42
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    • 2002
  • Polypropylene filaments were spun from a mixture of PP chips of two different Melt Flow Index (MFI) (3 MFI and 35 MFI). A significant difference was observed in the melting characteristics of the resultant filaments from either of the individual components as observed from the DSC. The main difference being in the degree of melting achieved at any temperature in the initial stages of the melting range, which was found to be higher in case of the filaments spun from the b]end. These filaments were then thermally bonded using silicon oil bath and heated roller method. Subsequently the bond strength of the filaments was measured on the Instron Tensile Tester using the loop technique. The values of the world strengths obtained from the blend were compared with those made from the individual component. It was found that the bond strength of the bonds obtained from the blended filament at a given temperature was higher than that of the bonds made from the filaments of either of the individual components, which is also suggested by the DSC curves. The difference in the bond strength was found to be as high as 25% in case of the blend with 60:40 composition ratios of the 3 MFI and 35 MFI components respectively.

A study on the optimum condition of electric snow melting and deicing system for the anti-freezing testing road (시험 선로 결빙 방지를 위한 전기 가열식 융설 및 융빙 시스템의 최적 조건에 관한 연구)

  • Han, Kyu-Il
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.44 no.4
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    • pp.362-369
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    • 2008
  • The snow melting system by electric heating wires which is adopted in this research is a part of road facilities to keep surface temperature of the road higher than freezing point of water for melting the snow accumulated on it. The electric heating wires are buried under paved road at a certain depth and operated automatically and manually. Design theory, amount of heating, and installation standard vary according to economic situation, weather condition, installation place and each country applying the system. A main purpose of this study is figuring out the appropriate range of required heat capacity and installation depth and pitch for solving snowdrifts and freezing problems with minimum electric power consumption. This study was performed under the ambient air temperature($-2^{\circ}C$, $-5^{\circ}C$), the pitches of the electric heating wires(200 mm, 300 mm), heating value($250\;W/m^2$, $300\;W/m^2$, $350\;W/m^2$).

Thermoelectric Properties of Binary Skutterudite CoSb3 Prepared by Encapsulated Induction Melting (밀폐유도용해로 제조된 2원계 Skutterudite CoSb3의 열전특성)

  • You, Sin-Wook;Jung, Jae-Yong;Ur, Soon-Chul;Kim, Il-Ho
    • Korean Journal of Materials Research
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    • v.16 no.5
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    • pp.312-317
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    • 2006
  • Binary skutterudite $CoSb_3$ compounds were prepared by the encapsulated induction melting (EIM) process, and their thermoelectric, microstructural and mechanical properties were examined. Single-phase ${\delta}-CoSb_3$ was successfully produced by the EIM and subsequent heat treatment at 773 K-873 K for 24 hours in vacuum. Seebeck coefficient increased with increasing heat treatment temperature up to 673 K, showing the positive signs in the range of measuring temperature. However, the samples heat-treated at 773 K-873 K showed negative Seebeck coefficient from room temperature to 400 K, while it showed positive signs above 400 K. Electrical resistivity decreased with increasing temperature, showing typical semiconducting conductivity. Thermal conductivity decreased drastically with increasing heat-treatment temperature. This is closely related with the phase transition to ${\delta}-CoSb_3$.

Forging of 1.9wt%C Ultrahigh Carbon Workroll : Part I - Analysis on Void Formation and Microstructure (1.9wt%C 초고탄소 워크롤 단조 공정 : Part I - 기공생성 및 미세조직 분석)

  • Lim, H.C.;Lee, H.;Kim, B.M.;Kang, S.H.
    • Transactions of Materials Processing
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    • v.22 no.8
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    • pp.456-462
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    • 2013
  • Compression tests were conducted at the various temperatures and strain rates to investigate void formation and microstructures behavior of a 1.9wt%C ultrahigh carbon steel used in forged workrolls. The microstructure, grain size and volume fraction of cementite were determined using specimens deformed in the temperature range from 800 to $1150^{\circ}C$ and strain rates from 0.01 to 10/s. It was found from the microstructural analysis that the grain size is larger at higher temperatures and lower strain rate deformation conditions. In addition, a higher volume fraction of cementite was measured at lower temperatures. The brittle blocky cementite was fractured at $800^{\circ}C$ and $900^{\circ}C$ regardless of strain rate. As a result, numerous new micro voids were formed in the fragmented blocky cementite. It was also found that local melting can occur at temperatures of more than $1130^{\circ}C$. Therefore, the forging temperature should be controlled between $900^{\circ}C$ and $1120^{\circ}C$. The temperature rise, which depends on the anvil stroke and velocity, was estimated through cogging simulation to find the appropriate forging temperature and to prevent local melting due to plastic work.

Microstructure and Mechanical Properties of CoCrFeMnNi-type High-entropy Alloy Fabricated by Selective Laser Melting: A Review (선택적 레이저 용융법으로 제조된 CoCrFeMnNi계 고엔트로피합금의 미세조직 및 기계적 물성 연구 동향)

  • Park, Jeong Min
    • Journal of Powder Materials
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    • v.29 no.2
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    • pp.132-151
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    • 2022
  • The CoCrFeMnNi high-entropy alloy (HEA), which is the most widely known HEA with a single face-centered cubic structure, has attracted significant academic attention over the past decade owing to its outstanding multifunctional performance. Recent studies have suggested that CoCrFeMnNi-type HEAs exhibit excellent printability for selective laser melting (SLM) under a wide range of process conditions. Moreover, it has been suggested that SLM can not only provide great topological freedom of design but also exhibit excellent mechanical properties by overcoming the strength-ductility trade-off via producing a hierarchical heterogeneous microstructure. In this regard, the SLM-processed CoCrFeMnNi HEA has been extensively studied to comprehensively understand the mechanisms of microstructural evolution and resulting changes in mechanical properties. In this review, recent studies on CoCrFeMnNi-type HEAs produced using SLM are discussed with respect to process-induced microstructural evolution and the relationship between hierarchical heterogeneous microstructure and mechanical properties.

Correlation of morphological changes of rice starch granules with rheological properties during heating In excess water (가열 조리시 쌀 전분 입자들의 형태학적 변화와 리올로지 특성과의 관계)

  • Lee, Young-Eun;Osman, Elizabeth M.
    • Applied Biological Chemistry
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    • v.34 no.4
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    • pp.379-385
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    • 1991
  • Morphological changes of starch granules from 12 different varieties of rice were examined by scanning electron microscopy during heating at 2.5% (w/v) concentration. Rice starch granules proceeded through a similar pattern of progressive morphological changes daring heating, regardless of variety. Rice starch granules began to swell radially in the initial stage of gelatinization and then undergo radial contraction and random tangential expansion to form complex structures in the latter stage of gelatinization temperature range. At higher temperatures, starch granules softened and melted into thin flat discs, and then stretched into thin filaments to form three-dimensional networks. These progressive morphological changes were reflected in the changes of swelling power, solubility and amylograph viscosity of starch. During the transition of melting or softening, swelling power, solubility and amylograph viscosity increased rapidly. The time of loss of granular structure of starch depended on gelatinization temperature range. The ratio of amylose to amylopectin was largely responsible fur the rate of melting or softening and the fineness of a three-dimensional filamentous network above the gelatinization temperature range. Therefore, both the gelatinization temperature range and amylose content of starch affect the rate of cooking, and amylose content of starch affects the final texture of cooked starch paste.

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Effect of heat setting on physical properties of dyeable polypropylene(DPP) fabric (가염형 폴리프로필렌직물의 열처리에 따른 물성변화)

  • Lee, Sin-Hui;Kim, Eun-Mi
    • Proceedings of the Korean Society of Dyers and Finishers Conference
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    • 2008.04a
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    • pp.37-39
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    • 2008
  • The purpose of this study is to improve the defects of DPP fabric by heat setting and to describe the change of physical properties of DPP fabrics. The thermosetting was carried out in autoclave from 100 to 140$^{\circ}C$ temperature range for 10min.. In this study, we investigated the effect of the thermosetting temperatures on the structural, thermal, mechanical properties and dyeability of DPP fabrics. The melting peak of multi peak changed to single peak with an increased thermosetting temperatures. The melting energy(J/g), the tensile strength and elongation were found to increase with increasing temperature of heat setting. The diffraction peak at Bragg angle(2${\theta}$) about 13.8$^{\circ}$ were very strong, and diffraction intensity, d-spacing and half-width decreased with increasing thermosetting temperatures. On the other hand, the dyeability(K/S) and crease recovery decreased with an increasing thermosetting temperatures.

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Measuring Nano-Width of Wave Fronts in Combustion: a Numerical Approach (연소시 발생하는 파면의 나노 사이즈 두께 측정: 수치적 접근)

  • Yoh, Jai-Ick
    • 한국연소학회:학술대회논문집
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    • 2005.10a
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    • pp.20-27
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    • 2005
  • I consider the structure of steady wave system which is admitted by the continuum equations for materials that undergo phase transformations with exothermic chemical reaction. In particular, the dynamic phase front structures between liquid and gas phases, and solid and liquid phases are computationally investigated. Based on the one-dimensional continuum shock structure analysis, the present approach can estimate the nano-width of waves that are present in combustion. For illustration purpose, n-heptane is used in the evaporation and condensation analysis and HMX is used in the melting and freezing analysis of energetic materials of interest. On-going effort includes extension of this idea to include broad range of liquid and solid fuels, such as rocket propellants.

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A Study on the Characteristics of Sn-Ag-X Solder Joint (Sn-Ag-X계 무연솔더 접합부의 미세조직 및 전단강도에 관한 연구)

  • 김문일;문준권;정재필
    • Journal of Welding and Joining
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    • v.20 no.2
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    • pp.77-81
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    • 2002
  • Many kinds of Pb-free solder have been investigated because of the environmental concerns. Sn-Ag-Cu system is well blown as most competitive Pb-free solder. However, since Sn-Ag-Cu system has relatively high melting point compared to Sn-Pb eutectic, it may a limitation, the some application. In this study, Bi and In contained solder of $Sn_3Ag_8Bi_5In$ which has relatively lower melting point, $188~204^{\circ}C$, was investigated. $Sn_3Ag_8Bi_5In$ solder ball of $500\mu\textrm{m}$ diameter was set on the Ni/Cu/Cr-UBM and reflow soldered in the range of $220~240^{\circ}C$ for 5~15s. The maximum shear strength of the solder ball was around 170mN by reflowing at $240^{\circ}C$ for 10s. Intermetallic compound formed on the UBM of Si-wafer was analysed by SEM(scanning electron microscope) and XRD(X-ray diffractometer).