• 제목/요약/키워드: Melt-spun

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Co-Fe-B 자왜변환기를 이용한 간섭계형 광섬유 자계센서의 동작특성

  • 이경식
    • 한국광학회지
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    • 제4권4호
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    • pp.474-479
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    • 1993
  • Melt-spun법에 의해서 자왜특성을 갖는 Co-Fe-B ribbon을 제작한 후 광섬유 Mach-Zehnder 간섭계의 sensing-arm에 부착하여 간섭형 자계센서를 구성하였다. Co-Fe-B 자왜변환기로 구성된 자계센서의 동작실험 결과 ac 자왜 응답이 최대가 되는 dc 바이어스 자계는 출력이 0인 바이어스 지점으로부터 0.970e 정도 떨어져 있었으며, 최소 감지자장은 3kHz에서 3.9${\times}10^{-5}$ Oe(rms)/${\sqrt{Hz}}$였다. 응답이 최대가 되는 지점에 바이어스를 고정시켰을 때 ac 자계셈서의 출력이 포화되기 시작하는 입력 자계신호는 1 Oe(rms) 근처였다. Co-Fe-B 자왜변환기의 주파수 특성곡선에서 응답이 피크가 되는 주파수는 ~500Hz였다.

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Steam Activation Behaviors of Oxidatively Stabilized Petroleum-based Pitch Fibers Spun by Melt-blown Method

  • Kim, Chan;Kim, Young-Min;Yang, Kap-Seung
    • Carbon letters
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    • 제3권2호
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    • pp.93-98
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    • 2002
  • Short pitch fibers were prepared from petroleum based isotropic precursor pitch by melt-blown technology. The pitch fibers were stabilized in oxidizing condition, followed by steam activations at various conditions. The fiber surface and pore structures of the activated carbon fibers (ACFs) were respectively characterized by using SEM and applying BET theory from nitrogen adsorption at 77 K. The weight loss of the oxidized fiber was proportional to activation temperature and activation time, independently. The adsorption isotherms of the nitrogen on the ACFs were constructed and analyzed to be as Type I consisting of micropores mainly. The specific surface area of the ACFs proportionally increased with the weight loss at a given activation temperature. The specific surface area was ranged 850~1900 $m^2/g$ with pores of narrow distribution in sizes. The average pore size was ranged 5.8~14.1 ${\AA}$ with the larger value from the more severe activation condition.

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Spinning of Petroleum based Isotropic Pitch by Melt-blown Method

  • Kim, Chan;Lee, Su-Hyun;Kim, Young-Min;Yang, Kap-Seung
    • Carbon letters
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    • 제3권1호
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    • pp.33-38
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    • 2002
  • Petroleum based isotropic pitch was spun into short fiber by melt-blown spinning technology. The processing parameters chosen were air velocity, die temperature, and throughput rate of the pitch within the ranges of experimental tolerances. The fiber diameter was reduced to $6{\mu}m$ by increases of hot air velocity, and spin die temperature. Also, the fiber diameter was strongly dependent on the throughput rate of the pitch and jet speed of hot air through the spinnerets. Even fibers with $10{\mu}m$ diameter were produced at throughput rate of $0.17g/min{\cdot}hole$ and at die temperature of $290^{\circ}C$.

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Preparation of Partial Mesophase Pitch-based Carbon Fiber from FCC-DO

  • Park, Sang-Hee;Yang, Kap-Seung;Soh, Soon-Young
    • Carbon letters
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    • 제2권2호
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    • pp.99-104
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    • 2001
  • Partial mesophase (PM) pitch precursor was prepared from fluidized catalytic cracking-decant oils (FCC-DO) by chemical reaction in the presence of $Br_2$. The PM pitch heated-treatment at $420^{\circ}C$ for 9 h exhibited the softening point of $297^{\circ}C$ with 23% yield, and 55% anisotropic content. The PM pitch precursor was melt-spun through circular nozzle by pressurized $N_2$, stabilized at $310^{\circ}C$, carbonized at $700^{\circ}C$, $1000^{\circ}C$, and $1200^{\circ}C$. The enough stabilization introduced 16.4% of the oxygen approximately. The stacking height ($L_{c002}$) and interlayer spacing ($d_{002}$) of the as-spun fibers were 4.58 nm and $3.45{\AA}$ and the value became minimum and maximum at $700^{\circ}C$ respectively in the carbonization procedure. The tensile strength increased with an increase in the heat treatment temperature exhibiting highest value of 750 MPa at $1200^{\circ}C$ carbonization.

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