• Title/Summary/Keyword: Mechanical pretreatment

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Chromate Conversion Coating on 3D Printed Aluminum Alloys (3D 프린팅으로 제조한 알루미늄 합금의 크로메이트 코팅)

  • Shin, Hong-Shik;Kim, Hyo-Tae;Kim, Ki-Seung;Choi, Hye-Yoon
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.21 no.2
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    • pp.109-115
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    • 2022
  • The demand for metal 3D printing technology is increasing in various industries. The materials commonly used for metal 3D printing include aluminum alloys, titanium alloys, and stainless steel. In particular, for applications in the aviation and defense industry, aluminum alloy 3D printing parts are being produced. To improve the corrosion resistance in the 3D printed aluminum alloy outputs, a post-treatment process, such as chromate coating, should be applied. However, powdered materials, such as AlSi7Mg and AlSi10Mg, used for 3D printing, have a high silicon content; therefore, a suitable pretreatment is required for chromate coating. In the desmut step of the pretreatment process, the chromate coating can be formed only when a smut composed of silicon compounds or oxides is effectively removed. In this study, suitable desmut solutions for 3D printed AlSi7Mg and AlSi10Mg materials with high silicon contents were presented, and the chromate coating properties were studied accordingly. The smut removal effect was confirmed using an aqueous desmut solution composed of sulfuric, nitric, and hydrofluoric acids. Thus, a chromate coating was successfully formed. The surfaces of the aluminum alloys after desmut and chromate coating were analyzed using SEM and EDS.

AN AUTORADIOGRAPHIC STUDY OF THE MICROLEAKAGE AROUND A PIT AND FIGURE SEALANT (치면열구 전쇄재의 미세누출에 관한 자가방사법적 연구)

  • Sohn, Jang-Sook;Lee, Jong-Gap
    • Journal of the korean academy of Pediatric Dentistry
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    • v.10 no.1
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    • pp.77-83
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    • 1983
  • The purpose of this study was to observe the microleakage of a pit and fissure sealant at the tooth-restoration interface. One hundred and sixty-seven extracted permanent and deciduous teeth were used and some simple mechanical pretreatment were done before etching. The degree of microleakage was assessed by $Ca^{45}$ after 24 hours, and 2 months. The results were as follows: 1. Among total 167 teeth, 53 teeth (32%) were demonstrated the microleakage. 2. After 2 months the leakage was increased from 22 percent to 35 percent in permanent teeth, and from 32 percent to 43 percent in primary teeth. 3. The group treated by fluoride paste was demonstrated the largest leakage, 50 percent in primary teeth and 33 percent in permanent teeth. There are more leakage in primary teeth (38%) than permanent teeth (28%).

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Development of Microfluidic Channel for Pretreatment of Extracellular ATP using DEP Force (DEP를 이용한 세포 외부 ATP 제거 전처리 미세 유로의 개발)

  • Lim, Hee-Taek;Jung, Hyo-Il
    • Proceedings of the KSME Conference
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    • 2008.11a
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    • pp.1687-1689
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    • 2008
  • In the detection of pathogenic microorganisms ATP-bioluminescence reaction is a fascinating method. ATP(adenosine triphosphate) is an energy source of all kinds of living organism and ATP-bioluminescence reaction uses this ATP. However, ATP exists not only in the cells but also outside the cells. Therefore ATP-bioluminescence reaction only with intracellular ATP is very important in pathogenic microorganism detection. Because of that reason we developed a microfluidic channel containing Dielectrophoretic zone which capture microorganisms and eliminating and washing extracellular ATP with ATP-degarading enzymes, adenosine phosphate deaminase and apyrase. Microorganisms are captured by pDEP force at the DEP electrode zone and only extracellular ATPs are washed and eliminated outside the zone.

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Dielectrophoretic separator for Airborne Microbes (전기 영동을 이용한 공기 중 미생물 분리)

  • Moon, Hui-Sung;Nam, Yun-Woo;Park, Jae-Chan;Jung, Hyo-Il
    • Proceedings of the KSME Conference
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    • 2008.11a
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    • pp.1683-1684
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    • 2008
  • For direct detection of microbes in air, samples have to be collected but environmental particles such as dust are also trapped in such samples. Therefore the isolation of target bacteria from non-biological materials of similar size is of great importance in the identification of such organisms. Dielectrophoresis is an emerging technique that can rapidly separate cells in microfluidics. In this paper we proposed a new method for the separation of airborne microbes using condensation and dielectrophoresis. This system could be used as a continuous flow through separation system for various particles and utilized as a pretreatment technique for microbe detection.

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Characteristics of direct transesterification using ultrasound on oil extracted from spent coffee grounds

  • Kim, Yeong Su;Woo, Duk Gam;Kim, Tae Han
    • Environmental Engineering Research
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    • v.25 no.4
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    • pp.470-478
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    • 2020
  • Spent coffee grounds (SCG), the residue after brewing coffee beverage, is a promising biodiesel feedstock due to its high oil contents (15-20%). However, SCG should be pretreated to reduce the high free fatty acid content, which hampers transesterification reaction. To overcome this, we explored a direct transesterification reaction of SCG using ultrasound irradiation and identified the optimal sonication parameters. A high fatty acid methyl ester (FAME) content, up to 97.2%, could be achieved with ultrasound amplitude of 99.2 ㎛, irradiation time of 10 min, and methanol to oil ratio of 7:1 in the presence of potassium hydroxide concentration of 1.25 wt.%. In addition, we demonstrated that ultrasound irradiation is an efficient method to produce biodiesel from untreated SCG in a short time with less energy than the conventional mechanical stirring method. The physical and chemical properties of the SCG biodiesel met the requirements for an alternative fuel to the current commercial biodiesel.

Selective Concentration and Determination of Phenol and Chlorophenols by Solid Phase Extraction

  • Jung, Min-Woo;Lee, Dai Woon;Paeng, Ki-Jung
    • Analytical Science and Technology
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    • v.8 no.4
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    • pp.535-538
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    • 1995
  • This study employs the variety of mixtures of XAD resin and active carbons as concentration base for solid phase extraction (SPE) which has been widely used to preconcentrate and purify phenol and chlorophenols in determination of environmental water samples. In this study, we employed variety of mixtures of copolymer based XAD-4 resin with active carbons. This cartridges shows advantages of both materials, such as better affinity to phenol by active carbon and better mechanical stabilities from XAD resin. The better enrichment factor, pretreatment time, recoveries and limit of detection (LOD) were achieved by the attempts to pack precolumns with both meterials for preconcentration.

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Effect of Gas Nitriding Characteristics on the Mechanical Properties after Pre-Heat Treatment of Stainless Steels (스테인리스강의 기계적 성질에 미치는 예비처리 후 가스질화조건의 영향)

  • Kim, Y.H.;Kim, H.G.
    • Journal of the Korean Society for Heat Treatment
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    • v.23 no.3
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    • pp.142-149
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    • 2010
  • Austenitic stainless steel is more or less difficult with conventional gas nitriding treatment, but it can be nitrided after appropriate pre-heat treatment. The pretreatment was more effective upon nitriding for austenitic stainless steel than martensitic stainless steel. Both thickness and microhardness measurements indicated that effect of the nitriding treatment was more sensitive in austenitic stainless steel than martensitic stainless steel with nitriding time. Fatigue strength was most increased with SACM 645 steel among three steels.

The Development of 125kW Molten Carbonate Fuel cell System (125kW 용융탄산염 연료전지 시스템 개발)

  • Kim, Beom-Joo
    • Journal of the Korean Professional Engineers Association
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    • v.44 no.1
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    • pp.48-52
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    • 2011
  • The KEPCO Research Institute has developed Molten Carbonate Fuel Cell(MCFC) since 1993. Recently, an 125-kW MCFC system was operated at Boryeong thermal power plant, Korea from December, 2009 to March, 2010, This system is composed of an 125-kW stack, mechanical balance of plant (MBOP), and Power Conditioning System. The stack has 200 unit cells of which effective area is 10,000 cm2. Especially, MBOP is mainly made up of ejector and catalytic combustor which help this system to be supplied with cathode inlet gas using anode tail gas and fresh air. After the pretreatment of this system was performed for about 20 days, initial load operation was performed at January. 2010. Moreover, this system had been operated for 3,270 hours.

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Inhibitory Effect on Melanogenesis of Rhizoma Bletillae (白급이 멜라닌 형성 억제에 미치는 영향)

  • Yoon, Hwa-Jung;Yoon, Jung-Won;Yoon, So-Won;Ko, Woo-Shin;Woo, Won-Hong
    • The Journal of Korean Medicine Ophthalmology and Otolaryngology and Dermatology
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    • v.16 no.1
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    • pp.100-111
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    • 2003
  • Recently many efforts were focused to understand the mechanical insights of melanogenesis to develop the agents for hyper-pigmentation and hypo-pigmentation. In the melanin biosynthetic pathway, tyrosinase is the rate limiting enzyme, and ${\alpha}$-melanocyte stimulating hormone(MSH) or cAMP-elevating agents stimulate melanogenesis and enhance the melanin synthesis and the tyrosinase activity. The author has analyzed the effects of Rhizoma Bletillae on the basal melanogenic activities of B16 mouse melanoma cells. Rhizoma Bletillae alone markedly suppressed melanin content and tyrosinase activity in a dose-dependent manner. Pretreatment of the cells with Rhizoma Bletillae. The decrease in the tyrosinase activity was paralled by a decrease in the abundance of tyrosinase protein and tyrosinase promoter activity. These results suggest that Rhizoma Bletillae inhibits melanogenesis of B16 melanoma cells via suppression of tyrosinase activity.

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Clinical Comparison of Low-dose and High-dose Steroid in Pediatric Cardiac Surgery with Cardiopulmonary Bypass

  • Choi Seok-Cheol;Kim Song-Myung;Kim Yang-Weon
    • Biomedical Science Letters
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    • v.12 no.3
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    • pp.289-301
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    • 2006
  • Cardiopulmonary bypass (CPB) for cardiac surgery triggers the production and release of numerous chemotactic substances and cytokines, ensuing systemic inflammatory response that leads to postoperative major organ dysfunction. Traditionally, corticosteroids (steroid) have been administered to patients undergoing cardiac surgery to ward off these detrimental physiologic alterations. However, the majority of the studies have been performed on adult patients with high-dose steroid. We carried out a randomized, prospective, double-blind study to compare the efficacy of low-dose steroid with that of high-dose steroid and to determine the adequate dose of pretreated-steroid for prophylactic effects in pediatric cardiac surgery. Thirty pediatric patients scheduled for elective cardiac surgery were randomly assigned to two groups; fifteen patients received low-dose methylprednisolone (10mg/kg intravenously, n=15, low-dose group) and the others received high-dose methylprednisolone (30mg/kg intravenously, n=15, high-dose group) 1 hour prior to CPB. Arterial blood samples were taken before CPB (Pre-CPB), 10 minutes after start of CPB (CPB-10), and immediately after CPB-end (CPB-OFF) for measuring total leukocyte counts (T-WBC) and diff-counts, platelet counts, interleukin-6 (IL-6), myeloperoxidase (MPO), total antioxidant (TAO), neuron-specific enolase (NSE), troponin I (TNI), aspartate aminotransferase (AST), alanine aminotransferase (ALT), creatinine, and blood urea nitrogen (BUN) levels. Other parameters such as volumes of urine output, pulmonary index $(PI,\;PaO_2/FiO_2)$, mechanical ventilating period, intensive care unit (ICU)-staying period, postoperative complications (fever, wound problem), postoperative 24 hrs and total volumes in blood loss, and hospitalized days were also assessed. All parameters were compared between two groups. There were no significant differences in T-WBC counts, monocyte fraction, platelet counts, TA levels, NSE levels, creatinine levels, BUN levels, the volumes of total urine output, PI, the incidences of fever and wound problem, postoperative 24hrs- and total-blood loss volumes and ICU-staying period between two groups (P>0.05). At CPB-OFF, neutrophil fraction, MPO level, TNI level, and AST level were higher in the high-dose group than in the low-dose group (P<0.05). IL-6 level at CPB-10 was higher in the high dose-group than in the low-dose group (P<0.05). Furthermore, mechanical ventilating periods and hospitalized days of the high-dose group were significantly longer than those of low-dose group (P<0.05). The high-dose group had significantly low lymphocyte fi-action at CPB-OFF compared with the low-dose group (P<0.001). These findings suggest that pretreatment of high-dose steroid is not superior to that of low-dose steroid regrading its potential benefits in pediatric cardiac surgery. Therefore, the conventional strategy of steroid treatment, high-dose pretreatment, should be modified in the cardiac surgery with CPB. However, further studies must be performed on the larger number of patients in as much as small number of patients in this study.

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