• Title/Summary/Keyword: Mean grain size

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Properties of ZnO:Ga Thin Films Deposited by RF Magnetron Sputtering with Ar Gas Flows (RF 마그네트론 스퍼터링법으로 제조한 GZO 박막의 Ar 유량에 따른 특성)

  • Kim, Deok Kyu
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.33 no.6
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    • pp.450-453
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    • 2020
  • In this study, ZnO:Ga thin films were fabricated on a glass substrate using various Ar flows by an RF magnetron sputter system at room temperature. The dependencies of Ar flow on different properties were investigated. An appropriate control over the Ar flow led to the formation of a high-quality thin film. The ZnO:Ga films were formed as a hexagonal wurtzite structure with high (002) preferential orientation. The films exhibited a typical columnar microstructure and a smooth top face. The average transmittance was 85~89% within the visible area. By decreasing the Ar flow, the sheet resistance was decreased due to an increase in the grain size and a decrease in the root mean square roughness. The lowest sheet resistance of 86 Ω/□ was obtained at room temperature for the 40 sccm Ar flow.

Microstructure of alumina-dispersed Ce-TZP ceramics (알루미나가 분산된 세리아 안정화 지르코니아 세라믹스의 미세구조)

  • 김민정;이종국
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.10 no.2
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    • pp.122-127
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    • 2000
  • Microstructural evolutions in ceria-stabilized zirconia (Ce-TZP) and alumina-dispersed Ce-TZP ceramics were investigated as functions of doping and annealing conditions. All of sintered specimens showed the relative density over 99 %. Sintered specimens had linear grain boundaries and normal grain shapes, but ceria-doped specimens had irregular grain shapes and nonlinear grain boundaries due to the diffusion-induced grain boundary migration during annealing at $1650^{\circ}C$ for 2 h. Mean grain boundary length of Ce-TZP with irregular grain shapes was higher than that of normal grain shapes, and was a value of 23pm at the maximum. Alumina particles dispersed in Ce-TZP inhibited the grain growth of zirconia particles. $Al_2O_3$Ce-TZP doped with ceria and annealed at $1650^{\circ}C$ for 2 h showed irregular grain shapes as well as small grain size. Added alumina particles showed the grain growth during sintering or annealing, and they changed the position from grain boundary to inside of the grains during the annealing. The specimens with normal grain shapes showed an intergranular fracture mode, whereas the specimens with irregular grain shapes showed a transgranular fracture mode during the crack propagation.

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Analysis of Paleo Sedimentary Environment of Gochang Coast Using Grain Size Distribution Characteristics (입도분포 특성을 기반으로 한 고창 연안의 과거 퇴적환경 분석)

  • Han, Min;Yang, Dong-Yoon;Park, Chanhyeok
    • Journal of The Geomorphological Association of Korea
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    • v.25 no.3
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    • pp.43-55
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    • 2018
  • This study aimed to identify different sedimentary environments of Gochang coast according to geomorphic conditions of each bore hole. To achieve the aim, this study utilized the classification of sedimentary environmental conditions of surface sediment, which was based on grain size distribution characteristics.In other words, three sedimentary environmental conditions ofsandy flat + sand beach, coastal sand dune and weathered bedrock soil, which were distinguished based on grain size distribution characteristics of mean-sorting for surface sediments, were applied to the sediments of bore holes. Four sedimentary environments could be identified in Gochang coast. First, the lake sedimentary environment originated from terrestrial sediments seems to have been dominated by weathered bedrock soil that the surface flow has deposited in a coastal wetland or a boundary, which is affected by the sea. Second, the lake sedimentary environment that is little affected by coastal sand dunes is located at the center of a valley, which is connected to the land, and the dune slack of Saban-ri. The surface flow of weather bedrock soil is the main source of deposits. However, there seems to have been a temporary influence of the sea. Third, the lake sedimentary environment that is strongly affected by coastal sand dunes is located at the dune slack of Yeongjeong-ri. This environment shows traces of a change from a coastal sand dune into the dune slack. Finally, the coastalsand dune sedimentary environment, which wasinvestigated by boring the current coastal sand dune, shows a temporary influence of the land but seems to have maintained the overall stability. Consequently, this study demonstrated that the grain size distribution characteristics of the present surface sediments could be effectively applied to identify the sedimentary environments of the paleo bore hole sediments. In addition, the paleo change of sedimentary environment could also be identified in many places of Gochang coast. If the results of this study are combined with the age dating and geochemical analysis in future works, the paleo environmental change in Gochang coast will be restored more precisely.

The Relationship between Microstructure and Property of Rapidly Solidified Al-Mg-X(X=Cr, Zr or Mn) Asloys (급속응고 Al-Mg-X(X=Cr, Zr or Mn) 합금의 미세구조와 특성간의 관계)

  • 맹덕영
    • Journal of Powder Materials
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    • v.3 no.4
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    • pp.271-278
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    • 1996
  • In this study, the effect of the transition elements on the microstructure and mechanical properties of rapidly solidified Al-Mg-X alloys was investigated. As a result of the rapid solidification processing, fine equiaxed grains with a mean diameter of 2 $\mu$m were observed in these alloys. Many fine particles were found to be distributed rather homogeneously throughout the matrix with relatively large particles occasionally at grain boundaries. The ultimate tensile strengths of Al-Mg-X alloys were found to decrease rather remarkably at 150 $^{\circ}C$ without the gain of the ductility at 150 $^{\circ}C$, which may result from segregation of $\beta$ ($Al_{3}Mg_{2}$) precipitates. Fine dimples were observed on the fracture surfaces for all alloy systems and the variation of the size and shape of dimples was not observed upon alloy systems. The ductility at 530 $^{\circ}C$ was found to be ~100%, suggesting that grain boundary sliding did not contribute to ductiliy despite he grain size stabilization. The absence of superplastic behavior may be associated with low boundary misorientation in rapidly solidified Al-Mg-X alloys.

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A Study on Dynamic and Static Recrystallization Behaviors and Microstructure Evolution Prediction of a Die Steel (금형강의 동적 및 정적 재결정 거동과 미세조직 변화 예측에 관한 연구)

  • 정호승;조종래;차도진;배원병
    • Transactions of Materials Processing
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    • v.10 no.4
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    • pp.338-346
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    • 2001
  • Evaluation of microstructural changes is important for process control during open die forging of heavy ingots. The control of forging parameters, such as shape of the dies, reduction, temperature and sequence of passes, is to maximize the forging effects and to minimize inhomogeneities of mechanical properties. The hot working die steel is produced by using the multistage open die forging. The structure is altered during forging by subsequent Precesses of plastic deformation, recrystallization and grain growth. A numerical analysis using an rigid visco-plastic finite element model was performed to predict microstructural evolution of hot working die steel.

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A Study on Dynamic and Static Recrystallization Behaviors and Microstructure Evolution Prediction of Die Steels (금형강의 동적 및 정적 재결정 거동과 미세조직 변화 예측에 관한 연구)

  • Jeong H. S.;Cho J. R.;Cha D. J.;Bae Y. B.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2001.05a
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    • pp.131-135
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    • 2001
  • Evaluation of microstructural changes during open die forging of heavy ingots is important for process control. The objective of the control of forging parameters, such as shape of the dies, reduction, temperature and sequence of passes, is to maximize the forging effects md to minimize inhomogeneities of mechanical properties. The hot working die steel is produced by using the multistage open die forging. The structure is altered during forging by subsequent processes of plastic deformation, recrystallization and grain growth. A numerical analysis using an rigid visco-plastic finite element model was performed to predict microstructural evolution of hot working die steel.

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Prediction of Hydraulic Conductivity from Gran-size Distribution Parameters (입도분포를 이용한 투수계수의 예측)

  • Song, Young-Woo;Lee, In-Koo
    • Journal of the Korean Geotechnical Society
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    • v.18 no.3
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    • pp.5-12
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    • 2002
  • Hydraulic conductivity k is one of the most important engineering properties of soil. However, both field and laboratory procedures fur the determination of k are often tedious and expensive. This paper presents new models to predict k using statistical parameters from grain size distribution. A number of permeability tests far 36 types of sands mixed based on statistics were conducted to develop the regression-based models. Parameters used to estimate k are both the geometric mean and geometric standard deviation of the soil samples, or the particle-size distribution curve parameters such as D_{10},D_{50},D_{60}. Hydraulic conductivity predicted by this model is in good agreement with the laboratory measurements fir the soil samples obtained at 20 locations within the Korean Peninsula. The performances of the proposed models were also compared with those of existing models including Hazen's.

Estimation Error Analysis on the Sediment Grain Size Information in the Coastal Zone (연안해역 퇴적물 입도정보 추정오차 분석)

  • Cho, Hong-Yeon;Kim, Chang-Il;Oh, Young-Min
    • Journal of Korean Society of Coastal and Ocean Engineers
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    • v.18 no.2
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    • pp.124-136
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    • 2006
  • The change pattern of the sediment grain size distribution information (median grain size(D50)) due to some gridding method and sampling density is analyzed with reference to the grid information estimated by the 90 sediment samples which was collected in the coastal water off the Baengnyeongdo Island, in June 2004. The standard deviation of absolute deviation (AD) estimated the selected gridding method shows 8.0 ${\mu}m$ at June, 2004 and 10 ${\mu}m$ November, 2004. The estimated statistical information of absolute deviation in comparison with the grid information of reference and changed sampling density shows that the AD mean error trends increase as the number of samples decrease. The AD mean error is below 10% in the case of the information estimation using 50-sample with reference to the 90-sample information. In this case, the sampling density is suggested as about 9 sediment samples per $km^2$, at coastal zone in Yoggipo port in the condition of the study area is 5.9 $km^2$.

Effect of stress-strain curve changing with equal channel angular pressing on ultimate strength of ship hull stiffened panels

  • Sekban, Dursun Murat;Olmez, Hasan
    • Structural Engineering and Mechanics
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    • v.78 no.4
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    • pp.473-484
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    • 2021
  • Similar to other structures, ultimate strength values showing the maximum load that the structure can resist without damaging has great importance on ships. Therefore, increasing the ultimate strength values will be an important benefit for the structure. Low carbon steels used in ships due to their low cost and good weldability. Improving the ultimate strength values without interfering with the chemical composition to prevent of the weldability properties of these steels would be very beneficial for ships. Grain refinement via severe plastic deformation (SPD) is an essential strengthening mechanism without changing the chemical composition of metallic materials. Among SPD methods, equal channel angular pressing (ECAP) is one of the most commonly used one due to its capacity for achieving bulk ultrafine-grained (UFG) materials. When the literature is examined, it is seen that there is no study about ultimate strength calculation in ships after ECAP. Therefore, the mean purpose of this study is to apply ECAP to a shipbuilding low carbon steel to be able to achieve mechanical properties and investigate the alteration of ship hull girder grillage system's ultimate strength via finite element analysis approach. A fine-grained (FG) microstructure with a mean grain size of 6 ㎛ (initial grain size was 25 ㎛) was after ECAP. This microstructural evolution brought about a considerable increase in strength values. Both yield and tensile strength values increased from 280 MPa and 425 MPa to about 420 MPa and 785 MPa, respectively. This improvement in the strength values reflected a finite element method to determine the ultimate strength of ship hull girder grillage system. As a result of calculations, it was reached significantly higher ultimate strength values (237,876 MPa) compared the non-processed situation (192,986 MPa) on ship hull girder grillage system.

A Study on the Characteristics and Burial Ages of Sediment Deposits at Jiduri, Daecheong Island (대청도 지두리 해안의 모래 퇴적층의 특성과 매몰연대에 대한 연구)

  • Kim, Jong Yeon
    • Journal of The Geomorphological Association of Korea
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    • v.25 no.1
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    • pp.1-17
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    • 2018
  • The characteristics and burial ages of sand sediments on the Jiduri coast in Daechung-myeon, Ongjin-gun, Incheon were investigated. Daecheong Island is the area where the characteristics of the rocky coast and sand coast are shown. Various studies have been conducted on the Okjukdong sand dune that appears in the north of the island. However, there has been no study on the sandy sedimentary topography of the Jiduri and Moraewul area in the south. The sandy sedimentary terrain of Jiduri is divided into sandy beaches, sand dunes and sand deposits along the slope including climbing dune. Overall, the depth of sandy sediments in Jiduri is not deep. The characteristics of sandy sediments and burial ages were investigated at an elevation of about 23 m above sea level at the back of Jiduli Beach and 46 m above sea level at the ridge line between Jiduri and Moraewol. From the Jiduri coast to the hillside behind, the average grain size decreases and the sorting becomes better as it moves from the intertidal zone to the beach and the foredune. This indicates the selective sand transport by the wind and can be judged by the terrain formed under the current sedimentation environment. The average grain size at the upper part of the section of JD-1 (elevation of about 23m MSL) was $1.6918{\varphi}$ of medium sand. The sorting was $0.4584{\varphi}$, skewness was -1.0491 and kurtosis was -1.2411, respectively. Particularly, the average particle size of the crosssection issomewhat uniform, but the color of the constituent material changes from brown to black. In the case of JD-2 (about 46 m MSL), the mean grain size of the section was $1.7943{\varphi}$, the sorting was 0.4931, the skewness was -1.1163, and the kurtosis was 1.2133. On the other hand, the brown and black layers of JD-1 exhibited a burial age of $0.1{\pm}0.0ka$ and the JD-2 had a burial age of $0.7{\pm}0.0ka$.