• Title/Summary/Keyword: Materials characterization

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Characterization of Fe Nanocapsules synthesized by Plasma Arc Discharge Process (플라즈마 아크방전(PAD)법으로 제조된 Fe Nanocapsules의 특성)

  • Park Woo-Young;Youn Cheol-Su;Yu Ji-Hun;Oh Young-Woo;Choi Chul-Jin
    • Journal of Powder Materials
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    • v.11 no.6 s.47
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    • pp.510-514
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    • 2004
  • Iron-carbon nanocapsules were synthesized by plasma arc discharge (PAD) process under various atmosphere of methane, argon and hydrogen gas. Characterization and surface properties were investigated by means of HRTEM, XRD, XPS and Mossbauer spectroscopy. Fe nanocapsules synthesized were composed of three phases $({\alpha}-Fe,\;Y-Fe\;and\;Fe_{3}C)$ with core/shell structures. The surface of nanocapsules was covered by the shell of graphite phase in the thickness of $4{\~}5$nm.

Fabrication of caterpillar mixer and its surface characterization (캐터필러형 믹서의 제작 및 표면 특성 연구)

  • Han Chang-Soo;Park June-Ki;Yoon Yeo-Hwan
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2006.05a
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    • pp.541-542
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    • 2006
  • A micro-size caterpillar mixer has been recently used fur desktop chemical factory and so attractive due to small investment fund for arranging the factory and high efficiency by mixing in sub micro-level region. We report the fabrication of caterpillar mixer and its surface treatment for enhancement of mixing performance. We used the

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Ultrasonic Nondestructive Evaluation(NDE) of Cornposite Materials - A Review -

  • Lee, Ouk-Sub
    • Journal of the Korean Society for Nondestructive Testing
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    • v.9 no.2
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    • pp.25-36
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    • 1989
  • This essay is a general review of the application of ultrasonic NDE techniques to the performance assessment and characterization of composite materials. A brief review of ultrasonic input-output characterization of a composite plate by shear waves is presented. A theoretical development of ultrasonic wave propagation in isotropic and anisotropic media excited, respectively, by a circular transducer and an oscillatory point source is summarized. Some experimental results are described in which ultrasonic velocity and attenuation measurements give insight into material degradation of fatigued composite laminates. Ultrasonic determination of the elastic constants of a composite plate and an experimental attempt at ultrasonic testing of an isotropic plate containing a crack are also included. A recent effort for the characterization of viscoelastic materials using the ultrasonic NDE technique is outlined. Finally, the reliability of ultrasonic NDE is briefly touched upon.

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Surface Characterization and Morphology in Ar-Plasma-Treated Polypropylene Blend

  • Weon, Jong-Il;Choi, Kil-Yeong
    • Macromolecular Research
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    • v.17 no.11
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    • pp.886-893
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    • 2009
  • Surface modifications using a radio frequency Ar-plasma treatment were performed on a polypropylene (PP) blend used for automotive bumper fascia. The surface characterization and morphology were examined. With increasing aging time, there was an increase in wettability, oxygen containing polar functional groups (i.e., C-O, C=O and O-C=O) due to oxidation, the amount of tale, and bearing depth and roughness on the PP surface, while there was a decrease in the number of hydrocarbon groups (i.e., C-C and C-H). AFM indicated that the Ar-plasma-treatment on a PP blend surface transforms the wholly annular surface into a locally dimpled surface, leading to an improvement in wettability. SEM showed that the PP layer observed in the non-plasma-treated sample was removed after the Ar-plasma treatment and the rubber particles were exposed to the surface. The observed surface characterization and morphologies are responsible for the improved wettability and interfacial adhesion between the PP blend substrate and bumper coating layers.

Structural Characterization and EDLC-Electrode Performance of Coal-Tar-Pitch Activated Carbon Using K2CO3 Treatment (K2CO3 처리된 Coal Tar Pitch 활성탄 전극의 결정성 및 EDLC 성능)

  • Choi, Poo Reum;Jung, Ji Chul;Lim, Yun-Soo;Kim, Myung-Soo
    • Korean Journal of Materials Research
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    • v.26 no.9
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    • pp.460-467
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    • 2016
  • Activated carbons (ACs) have been used as EDLC (electric double-layer capacitor) electrode materials due to their high specific area, stability, and ecological advantages. In order to prepare ACs with high density and crystallinity, coal tar pitch (CTP) was activated by $K_2CO_3$ and the textural and electrochemical properties of the obtained ACs were investigated. Although the CTP ACs formed by $K_2CO_3$ activation had much smaller specific surface area and pore volume than did the CTP ACs formed by KOH activation, their volumetric specific capacitance (F/cc) levels as electrode materials for EDLC were comparable due to their higher density and micro-crystallinity. Structural characterization and EDLC-electrode performance were studied with different activation conditions of $CTP/K_2CO_3$ ratio, activation temperature, and activation period.

CHARACTERIZATION OF MONOLITHIC RS-SiC AND RS-$SiC_f/SiC$ COMPOSITE MATERIALS (반응소결 SiC 재료와 $SiC_f/SiC$ 복합재료의 특성)

  • Jin, Joon-Ok;Lee, Sang-Pill;Lee, Jin-Kyung;Yoon, Han-Ki;Khoyama, Akira
    • Proceedings of the KSME Conference
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    • 2003.04a
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    • pp.376-380
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    • 2003
  • The microstructure and the mechanical properties of RS-SiC and RS-$SiC_f/SiC$ materials have been investigated in conjunction with the content of residual silicon and porosity. The mechanical properties of RS-SiC materials suffered from the thermal exposure were also examined. RS-SiC based materials bave been fabricated using the complex matrix slurry with different composition ratios of SiC and C panicles. The characterization of RS-SiC based materials was investigated by means of SEM, EDS ~d three point bending test. Based on the mechanical property-microstructure correlation, the high temperature applicability of RS-SiC based materials was discussed.

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