• Title/Summary/Keyword: Material property test

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Physical and Mechanical Properties of Magnesium Oxide Matrix depending on Addition Ratio of Magnesium Chloride (염화마그네슘 첨가율에 따른 산화마그네슘 경화체의 물리 및 역학적 특성)

  • Kim, Heon-Tae;Jung, Byeong-Yeol;Lee, Sang-Soo;Song, Ha-Young
    • Journal of the Korea Institute of Building Construction
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    • v.14 no.4
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    • pp.308-313
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    • 2014
  • Recently, for longevity of resident building, the main trend is that the change of the inside space organization of resident building from wall construction to rhamen construction, which resulted in increase in use of lightweight composite panel. Thus, in this study, authors analyzed the engineering property of oxide of magnesium depending on the magnesium chloride addition ratio. The results of this research is expected to contribute on providing a fundamental material for the surface materials of lightweight composite panel. As the result of the experiment, as fluidity increased, air content decreased and initial set and final set as the magnesium chloride addition ratio increase. In the aspect of flexural strength and compressive strength, the test specimen showed the highest strength at 40% of the magnesium chloride addition ratio. At 20% of the magnesium chloride addition ratio, the test specimen showed the lowest water absorption rate. As the magnesium chloride addition ratio increases, the expansibility tends to increase as well in the aspect of shrinkage strain. After observing microstructure, we can see hydration products in the form of needle. It appeared high flexural strength because the hydration products have mineral fibrous tissue shape, which also contribute to the cause of the expansibility.

The Study on the Physical Property of Provisional Prosthesis using Modified Temporary Abutment (변형된 임플란트 임시 지대주의 물성에 대한 연구)

  • Yang, Byung-Duk;Yoon, Tae-Ho;Choi, Un-Jae;Park, Ju-Mi
    • Journal of Dental Rehabilitation and Applied Science
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    • v.22 no.4
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    • pp.329-340
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    • 2006
  • Statement of problem: Damping of the peak force transmitted to implants has been reported by in vitro studies using impact forces on resin-veneered superstructures. Theoretical assumptions suggest that use of acrylic resin for the occlusal surfaces of a prosthesis would protect the connection between implant and bone. Therefore, the relationship between prosthesis materials and the force transmitted through the implant system also needs to be investigated under conditions that resemble the intraoral mechanical environment. Purpose: The purpose of this study was to analyze the fracture strength and modes of temporary prosthesis when a flange or occlusally extended structure were connected on the top of the abutment. Material and method: Modified abutments of winged and bulk design were made by casting the desired wax pattern which is made on the UCLA type plastic cylinder. Temporary crowns were made using templates on the modified abutments, and its fracture toughness and strain were compared to the traditional temporary prosthesis. To evaluate the effect of aging, 5.000 times of thermocycling were performed, and their result was compared to the 24hours specimen result. Results: The following conclusions were drawn from this study: 1. In the fracture toughness test, temporary crown's fracture line located next to the screw hole while modified designs with metal support showed fracture line on the metal and its propagation along the metal-resin interface. 2. Wing and bulk structure didn't show significant difference in the fracture toughness (p>0.05), but wing structure showed stress concentration on the screw hole area compared to bulk structure which showed even stress distribution. 3. In the fracture toughness test after thermocycling, wing and bulk structure showed increased or similar results in metal supported area while off-metal area and temporary crown showed decreased results. 4. In the strain measurement after thermocycling, its value increased in the temporary and bulk structure. However, wing structure showed decreased value in the loading point while increased value in the screw hole area. Conclusion: Wing type design showed compatible result to the bulk type that its application with composite resin prosthesis to the implant dentistry is considered promising.

Study of the Nondestructive Test Method for the Embrittlement Evaluation of Nuclear Reactor Vessel Material by $M{\ddot{o}}ssbauer$ Spectroscopy ($M{\ddot{o}}ssbauer$ 분광법에 의한 원자로 용기재료의 비파괴적 중성자 조사평가에 대한 연구)

  • Jung, M.M.;Jang, K.S.;Yoo, K.B.;Kim, G.M.;Yoon, I.S;Hong, C.Y.
    • Journal of the Korean Society for Nondestructive Testing
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    • v.20 no.3
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    • pp.183-190
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    • 2000
  • The purpose of this study is to evaluate the magnetic property change of the nuclear reactor vessel steel irradiated by fast neutrons using $M{\ddot{o}}ssbauer$ spectroscopy, and the effects of the defects produced by neutron irradiation on the changes using X-ray diffraction. The specimens, fabricated with the dimension of $23mm{\times}18mm{\times}70{\mu}m$, were irradiated by neutron fluence from $10^{12}n/cm^2\;to\;10^{18}n/cm^2$ at 343K. Throughout the experiments, it is understood that (1) the X-ray diffraction measurement shows that the change of crystal nature is started at the irradiation of $10^{16}n/cm^2$ and a crystal structure has been severely damaged at the irradiation over $10^{17}n/cm^2$, (2) the analysis of the $M{\ddot{o}}ssbauer$ spectra has shown that magnetic transition phenomena occur at the irradiation over $10^{17}n/cm^2$ and (3) both methods can be utilized as nondestructive test methods for the embrittlement evaluation of materials irradiated by fast neutrons.

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The Shear Strength Characteristics of Weathered Granite Soil in Unsaturated State (불포화(不飽和) 화강암질풍화토(花崗岩質風化土)의 전단강도(剪斷强度) 특성(特性))

  • Cho, Seong Seup;Kang, Yea Mook;Chee, In Taeg
    • Korean Journal of Agricultural Science
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    • v.12 no.1
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    • pp.86-100
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    • 1985
  • In order to investigate the strength characteristics of weathered granite soils in unsaturated state, the five physically different weathered granite soils and the common soil (sandy loam) were examined. The disturbed and the undisturbed material were prepared for triaxial compression test. The following conclusions were drawn from the study; 1. Dry density of the undisturbed soil samples was lower than maximum dry density determined from the compaction test and it showed the higher value at the well graded soil. 2. The failure strength of the samples decreased with the increase of moisture content of the soil and these results were highly pronounced at the common soil sample having a good cohesive property. 3. On weathered granite soils, the cohesion was lower measured and the internal friction angle highly, the decrease rate at internal friction angle with increase of moisture content of the soil was more significant than that of cohesion 4. The modulus of deformation of the samples decreased with increase of moisture content of the soil and these phenomena were highly pronounced at the weathered granite soils than common soil. 5. The failure strength of the samples increased with in crease of confining pressure and effect of confining pressure on failure strength was highly significant at the lower moisture content of the soil.

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Carbonation Characteristics of Alkali Activated Blast-Furnace Slag Mortar (알칼리활성 고로슬래그 모르타르의 탄산화 특성)

  • Song, Keum-Il;Yang, Keun-Hyeok;Lee, Bang-Yeon;Song, Jin-Kyu
    • Journal of the Korea Concrete Institute
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    • v.24 no.3
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    • pp.315-322
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    • 2012
  • Alkali-activated slag (AAS) is the most obvious alternative materials that can replace OPC. But, AAS industrial usage as a structural material should be evaluated for its durability. Carbonation resistance is one of the most important factors in durability evaluation. Test results for 18 slag-based mortars activated by sodium silicate and 6 OPC mortars were obtained in this study to verify the carbonation property. Main variables considered in the study were flow, compressive strength before and after carbonation, and carbonation depth. Mineralogical and micro-structural analysis of OPC and AAS specimens prior to and after carbonation was conducted using XRD, TGA, FTIR FE-SEM. Test results showed that CHS was major hydration products of AAS and, unlike OPC, no other hydration products were found. After carbonation, CSH of hydration product in AAS turned into an amorphous silica gel, and alumina compounds was not detected. From the analysis of the results, it was estimated that the micro-structures of CSH in AAS easily collapsed during carbonation. Also, the results showed that this collapse of chemical chain of CSH lowered the compressive strength of concrete after carbonation. By increasing the dosage of activators, carbonation resistance and compressive strength were effectively improved.

Evaluation of mechanical properties of KURT granite under simulated coupled condition of a geological repository (복합 처분환경 모사조건에서의 KURT 화강암의 역학적 물성 변화 평가)

  • Park, Seunghun;Kim, Jin-Seop;Kim, Geon Young;Kwon, Sangki
    • Journal of Korean Tunnelling and Underground Space Association
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    • v.21 no.4
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    • pp.501-518
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    • 2019
  • The rock properties measured under in-situ geological condition can be used to increase the reliability in numerical simulations with regard to the long-term performance of a high-level waste repository. In this study, the change in mechanical properties of KURT (Korea atomic energy research institute Underground Research Tunnel) granite was evaluated under the simulated THM (Thermo-Hydro-Mechanical) coupled condition due to a deep geological formation in the disposal repository. The rock properties such as uniaxial compression strength, indirect tensile strength, elastic modulus and Poisson's ratio were measured under the coupled test conditions (M, HM, TM, THM). It was found that the mechanical properties of KURT granite is more susceptible to the change in saturation rather than temperature within the test condition of this study. The changes in uniaxial compression strength and indirect tensile strength from the rock samples of dried or saturated conditions showed the maximum relative error of about 20% and 13% respectively under the constant temperature condition. Therefore, it is necessary to use the material properties of rock measured under the coupled THM condition as input parameters for the numerical simulation of long-term performance assessment of a disposal repository

Estimation of the Mechanical Properties of the Concrete Tunnel Lining by Drilling Resistance Test (천공저항시험에 의한 콘크리트 터널라이닝의 역학적 특성 추정)

  • Choi, Soon-Wook;Sung, Yun-Chang;Cheong, Ho-Seop;Chang, Soo-Ho
    • Journal of the Korean Geotechnical Society
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    • v.23 no.11
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    • pp.87-98
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    • 2007
  • For the quick rehabilitation of a fire-damaged tunnel structure, it is the most important procedure to investigate the fire-induced damaged zone rapidly. This study aims to propose a new drilling resistance testing method by which mechanical properties of tunnel concrete lining altered by high temperature can be estimated easily and continuously. Especially, it alms to derive the relationships to estimate mechanical properties of mortar and concrete materials from drilling parameters. To obtain the optimum testing condition, a series of drilling resistance tests were carried out for mortar specimens. When the rotation per minute of drill bit, tile penetration rate and the bit diameter were 1,300 rpm, 1.40 mm/sec, and 10 mm respectively, the deviation of measured drilling resistance forces was minimal. Under the optimum testing condition, the relationships between drilling resistance and mechanical properties of mortar specimens were shown to be very favorable. The concept of replacing a mean value of resistance farces measured during drilling with the resistance energy was proposed to consider the effects of randomly distributed aggregates inside a concrete material on drilling resistance. When the concept was applied to concrete materials, a favorable relationship between actual compressive strength and drilling resistance energy was also successfully derived.

Effects of chromium chloride addition on coloration and mechanical properties of 3Y-TZP (크롬염화물 첨가에 따른 지르코니아 색상 및 물리적 성질 변화에 관한 연구)

  • Oh, Gye-Jeong;Seo, Yoon-Jeong;Yun, Kwi-Dug;Lim, Hyun-Pil;Park, Sang-Won;Lee, Kyung-Ku;Lim, Tae-Kwan;Lee, Doh-Jae
    • The Journal of Korean Academy of Prosthodontics
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    • v.49 no.2
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    • pp.120-127
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    • 2011
  • Purpose: The purpose of this study was to examine the effects of chromium chloride addition on coloration, mechanical property and microstructure of 3Y-TZP. Materials and methods: Chromium chloride was weighed as 0.06, 0.12, and 0.25 wt% and each measured amount was dissolved in alcohol. $ZrO_2$ powder was mixed with each of the individual slurry to prepare chromium doped zirconia specimen. The color, physical properties and microstructure were observed after the zirconia specimen were sintered at $1450^{\circ}C$. In order to evaluate the color, spectrophotometer was used to analyze the value of $L^*$, $C^*$, $a^*$ and $b^*$, after placing the specimen on a white plate, and measured according to the International Commission on Illumination (CIE) standard, Illuminant D65 and SCE system. The density was measured in the Archimedes method, while microstructures were evaluated by using the scanning electron microscopy (SEM) and XRD. Fracture toughness was calculated Vickers indentation method and indentation size was measured by using the optical microscope. The data were analyzed with 1-way ANOVA test (${\alpha}$ = 0.05). The Tukey multiple comparison test was used for post hocanalysis. Results: 1. Chromium chloride rendered zirconia a brownish color. While chromium chloride content was increased, the color of zirconia was changed from brownish to brownish-red. 2. Chromium chloride content was increased; density of the specimen was decreased. 3. More chromium chloride in the ratio showed increase size of grains. 4. But the addition of chromium chloride did not affect the crystal phase of zirconia, and all specimens showed tetragonal phase. 5. The chromium chloride in zirconia did not showed statistically significant difference in fracture toughness, but addition of 0.25 wt% showed a statistically significant difference (P<.05). Conclusion: Based on the above results, this study suggests that chromium chlorides can make colored zirconia while adding in a liquid form. The new colored zirconia showed a slight difference in color to that of the natural tooth, nevertheless this material can be used as an all ceramic core material.

A Study on the Material Characteristics and Functionality Evaluation of a Size Layer of a Canvas (캔버스 차단층(Size Layer)의 재료특성 및 기능평가 연구)

  • Kim, Hwan Ju;Lee, Hwa Soo;Chung, Yong Jae
    • Journal of Conservation Science
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    • v.32 no.2
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    • pp.167-178
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    • 2016
  • Despite the size layer is an important part for conserving the artworks in the configuration of oil painting, the conservation scientific approaches of that have not been made yet. Therefore, this study produced standard samples on the basis of the analysis results of oil painting works, and carried out the evaluation of functions of the size layer materials. As a result of literature material, traditionally, animal glue was used for the size layer, whereas synthetic resin have been used in combination with animal glue since the modern age, in particular, it was identified that Polyvinyl Acetate(PVAc) was in general use. As a result of analysis of oil painting works, size layer was detected on the support and it was identified as animal glue. As a result of analysis based on Funaoka canvas for ground, it showed that the lead oxide and the titanium dioxide were the main constituents. On the basis of these results, standard samples were produced. As a result of evaluation on the functions of the size layer materials, in the case of the animal glue, stable result was observed in the shrinkag expansion rate, whereas slight weakness was observed in moisture proofing, color, and tensile strength, and dense cracks were found on surface. As for PVAc(A), moisture proofing, color, and the tensile strength exhibited stable results. Higher shrinkage rate was observed and the cracks with wide gaps were found on surface. As for PVAc(B), tensile strength, shrinkage expansion rate, and surface observation showed stable results, whereas moisture proofing property showed poor results. Different aspects were observed in each experiment, and this phenomena were considered to be due to the density and the adhesion properties between the hydrophilic and hydrophobic molecules in the size layer materials. The results are expected to be used as materials for the oil painting work conservation henceforth.

Brittle rock property and damage index assessment for predicting brittle failure in underground opening (지하공동의 취성파괴 예측을 위한 암석물성 및 손상지수 평가)

  • Lee, Kang-Hyun;Bang, Joon-Ho;Kim, Jin-Ha;Kim, Sang-Ho;Lee, In-Mo
    • Journal of Korean Tunnelling and Underground Space Association
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    • v.11 no.4
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    • pp.327-351
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    • 2009
  • Laboratory tests are performed in this paper to investigate the brittle failure characteristics of over-stressed rocks taken in deep depth. Also, numerical simulation performed using that the so-called CWFS(Cohesion Weakening Frictional Strengthening) model is known to predict brittle failure phenomenon reasonably well. The most typical rock types of Korean peninsula - granite and gneiss - were used for testing. Results of uniaxial compression tests showed that the crack initiation stress was about 41 % to 42% of the uniaxial compressive strength regardless of rock types, where as, the crack damage stress of granite was about 75%, and that of gneiss was about 97%. Through the damage-controlled test, strength parameters of each rock were obtained as a function of damage degree. After the peak, the crack damage stress and the maximum stress were decreased, The cohesion was decreased and the friction angle was increased with increase of rock damage. Before reaching the peak, the elastic modulus was slightly increased, while decreased after the peak. Poisson's ratio was increased as the damage of rock proceeds. Comparison of uniaxial compression tests and damage-controlled tests shows the crack initiation stress estimated from the damage-controlled test fluctuated within the range of crack initiation stress obtained from the uniaxial compression test; the crack damage stress was less than that estimated from the uniaxial compression test. In order to predict the critical depth that brittle failure occurs, numerical simulations using the CWFS model were performed for an example site. Material parameters obtained from the laboratory tests mentioned above were used for CWFS simulation. Comparison between the critical depth predicted from the numerical simulation using the CWFS model and that predicted by using the damage index proposed by Martin et al.(l999), showed that critical depth cannot be reasonably predicted by the currently used damage index except for circular tunnels. A modified damage index was proposed by the author which takes the shape of tunnels other than circular into account.