• 제목/요약/키워드: Material Measurements

검색결과 1,586건 처리시간 0.045초

Equo-Tip 경도값에 미치는 실험변수의 영향 (The Effect of Test Variables on the Accuracy of Equo-Tip Hardness)

  • 남승훈;전승범;김종집
    • 열처리공학회지
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    • 제3권2호
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    • pp.32-36
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    • 1990
  • For the accurate measurements of hardness in a material, it is necessary to have a thorough understanding of the effects of test variables on the accuracy of hardness value. For the rebound hardness test, major test variables are the radius of hammer ball tip, type of backing materials, size and roughness of the specimen. In this study, effects of these variables on Equo-Tip hardness value were investigated. Hardness measurements were carried out using WC balls with various sizes of worn-ot zone. The sample materials chosen for the experiments were commercial standard hardness blocks and SM45C steel bars subjected to either normalization or quench and temper treatments. As backing materials, aluminum, steel and rubber plates were used in all the experiments. Experimental results show that for the accurate measurements of Equo-tip hardness, it is necessary to use the hammer ball with a worn-out zone parameter of less than 0.23, and the recommended minimum thickness and width of the specimen are 25mm and 70mm, respectively. Further for the surface preparation, the specimens need to be polished with an emery paper of No. 400 or finer, and for the backing matrials, it is recommended to use steels or rubbers.

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접촉 공진 힘 현미경 기술을 이용한 플립 칩 범프 재료의 국부 탄성계수 측정 (Measurement of Local Elastic Properties of Flip-chip Bump Materials using Contact Resonance Force Microscopy)

  • 김대현;안효석;한준희
    • Tribology and Lubricants
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    • 제28권4호
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    • pp.173-177
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    • 2012
  • We used contact resonance force microscopy (CRFM) technique to determine the quantitative elastic properties of multiple materials integrated on the sub micrometer scale. The CRFM approach measures the frequencies of an AFM cantilever's first two flexural resonances while in contact with a material. The plain strain modulus of an unknown or test material can be obtained by comparing the resonant spectrum of the test material to that of a reference material. In this study we examined the following bumping materials for flip chip by using copper electrode as a reference material: NiP, Solder (Sn-Au-Cu alloy) and under filled epoxy. Data were analyzed by conventional beam dynamics and contact dynamics. The results showed a good agreement (~15% difference) with corresponding values determined by nanoindentaion. These results provide insight into the use of CRFM methods to attain reliable and accurate measurements of elastic properties of materials on the nanoscale.

Impact Echo Test for the Dynamic Characteristics of a Vibration-Mitigated Concrete Structure

  • Chung, Young-Soo;Park, Young-Goo
    • KCI Concrete Journal
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    • 제14권1호
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    • pp.23-29
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    • 2002
  • Recent construction activities have given rise to civil petitions associated with vibration-induced damages or nuisances. To mitigate unfavorable effects of construction activities, the measures to reduce or isolate from vibration need to be adopted. In this research, a vibration-mitigated concrete, which is one of the active measures for reducing vibration in concrete structures, was investigated. Concrete was mixed with vibration-reducing materials (i.e. latex, rubber power, plastic resin, and polystyrofoam) to reduce vibration and tested to evaluate dynamic material properties and structural characteristics. Normal and high strength concrete specimens with a certain level of damage were also tested for comparisons. In addition, recycling tires and plastic materials were added to produce a vibration-reducing concrete. A total of 32 concrete bars and eight concrete beams were tested to investigate the dynamic material properties and structural characteristics. Wave measurements on concrete bars showed that vibration-mitigated concrete has larger material damping ratio than normal or high strength concrete. Styrofoam turned out to be the most effective vibration-reducing mixture. Flexural vibration tests on eight flexural concrete beams also revealed that material damping ratio of the concrete beams is much smaller than structural damping ratio for all the cases.

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$LiV_3O_8$/Li 이차전지의 복합양극의 조성에 따른 영향 (Effects of Cathode Composition for $LiV_3O_8$/Li Secondary Battery)

  • 박수길;김종진;이홍기;엄재석;전세호
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1998년도 추계학술대회 논문집
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    • pp.29-32
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    • 1998
  • A new treatment of LiV$_3$O$_{8}$ has beer proposed for improving its electrochemical behavior as a cathode material secondary lithium batteries. Early in its development, the preparation method of LiV$_3$O$_{8}$ strongly influenced its electrochemical properties, such as discharge capacity, rate capability and cycling efficiency. In the present experiment, a new synthesis route has been applied to obtain LiV$_3$O$_{8}$ . Instead of the conventional high temperature technique leading to the crystalline form, a solution technique producing the amorphous form has been used. This material, after dehydration, shows an electrochemical performance exceeding that of the crystalline one. These measurements showed that the ultrasonic treatment process of crystalline LiV$_3$O$_{8}$ causes a decrease in crystallinity and considerable increases in specific surface area and interlayer spacing. So the ultrasonic method provides a convenient means for improving the electrochemical behavior of LiV$_3$O$_{8}$ as a cathode material for secondary lithium batteries.batteries.

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SiC single crystal grown on a seed with an inserted epitaxial layer for the power device application

  • 안준호;김정곤;서정두;김정규;견명옥;이원재;김일수;신병철;구갑렬
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2006년도 추계학술대회 논문집 Vol.19
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    • pp.232-232
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    • 2006
  • SiC single crystal Ingots were prepared onto different seed material using sublimation PVT techniques and then their crystal quality was systematically compared. In this study, the conventional SiC seed material and the new SiC seed material with an inserted SiC epitaxial layer on a seed surface were used as a seed for SiC bulk growth. The inserted epitaxial layer was grown by a sublimation epitaxy method called the CST with a low growth rate of $2{\mu}m/h$ N-type 2"-SIC single crystals exhibiting the polytype of 6H-SiC were successfully fabricated and carrier concentration levels of below $10^{17}/cm^3$ were determined from the absorption spectrum and Hall measurements. The slightly higher growth rate and carrier concentration were obtained in SiC single crystal Ingot grown on new SiC Seed materials with the inserted epitaxial layer on the seed surface, maintaining the high quality.

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시효조건에 다른 $Fe_{78}B_{13}Si_9$ 비정질 합금의 결정화 연구 (The Effects of Aging Conditions on the Crystallization of $Fe_{78}B_{13}Si_9$ Metallic Glass)

  • 이원재;김기욱;민복기;송재성;홍진완;강원구;김윤동
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1989년도 하계종합학술대회 논문집
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    • pp.291-294
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    • 1989
  • The effect of isothermal aging on the crystallization of $Fe_{78}B_{13}Si_9$ metallic glass has been investigated by electrical resistivity, X-ray measurements, bending test, thermal analysis and transmission electron microscpy. Amouphous $Fe_{78}B_{13}Si_9$ alloy was annealed isothermally for 5 to 1200 min. between $300^{\circ}C$ and $540^{\circ}C$. It has been found that close relation between relative resistivity and X-ray diffraction pattern showed. The crystalline peaks of ${\alpha}$-(Fe, Si) and $Fe_2B$ are detected by X-ray experiment. The crystalline phases observed by TEH show ${\alpha}$-(Fe, Si) and $Fe_2B$ with dendritic and cylindrical morphology, respectively. It has been also found that the embrittleness of aged samples rapidly increased with the crystallization and was shown before the crystallization.

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A Comparative Study on Arrhenius-Type Constitutive Models with Regression Methods

  • Lee, Kyunghoon;Murugesan, Mohanraj;Lee, Seung-Min;Kang, Beom-Soo
    • 소성∙가공
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    • 제26권1호
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    • pp.18-27
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    • 2017
  • A comparative study was performed on strain-compensated Arrhenius-type constitutive models established with two regression methods: polynomial regression and regression Kriging. For measurements at high temperatures, experimental data of 70Cr3Mo steel were adopted from previous research. An Arrhenius-type constitutive model necessitates strain compensation for material constants to account for strain effect. To associate the material constants with strain, we first evaluated them at a set of discrete strains, then capitalized on surrogate modeling to represent the material constants as a function of strain. As a result, disparate flow stress models were formed via the two different regression methods. The constructed constitutive models were examined systematically against measured flow stresses by validation methods. The predicted material constants were found to be quite accurate compared to the actual material constants. However, notable mismatches between measured and predicted flow stresses were revealed by the proposed validation techniques, which carry out validation with not the entire, but a single tensile test case.

다층구조 수중 방음재의 디커플링성능 측정방법에 대한 고찰 (Measurement of decoupling performance of an multi-layered underwater decoupling material)

  • 김상렬;김재승;김재호;함일배;전재진
    • 한국소음진동공학회:학술대회논문집
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    • 한국소음진동공학회 2012년도 추계학술대회 논문집
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    • pp.437-444
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    • 2012
  • In this paper, the measurement method of the decoupling performance of a underwater decoupling material is studied. First, the simple vibro-acoustic coupled model of a multi-layered underwater decoupling material attached to a plate is analytically derived using impedance transfer matrix. Two test methods are introduced using the theoretical expression of the simple model. One is based on the ratio of the plate vibration and the radiated pressure under impact excitation of the plate. The other is based on the reciprocity theorem and uses the ratio of the incident pressure and the plate vibration under projector excitation in water. Some measurements are carried out according to the test methods using a pulse tube. The test results show the advantages and disadvantages of two methods. It is also shown that the combination of impact and projector excitation methods may be a useful tool to evaluate the performance of a underwater decoupling material.

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Evaluation of nuclear material accountability by the probability of detection for loss of Pu (LOPu) scenarios in pyroprocessing

  • Woo, Seung Min;Chirayath, Sunil S.
    • Nuclear Engineering and Technology
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    • 제51권1호
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    • pp.198-206
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    • 2019
  • A new methodology to analyze the nuclear material accountability for pyroprocessing system is developed. The $Pu-to-^{244}Cm$ ratio quantification is one of the methods for Pu accountancy in pyroprocessing. However, an uncertainty in the $Pu-to-^{244}Cm$ ratio due to the non-uniform composition in used fuel assemblies can affect the accountancy of Pu. A random variable, LOPu, is developed to analyze the probability of detection for Pu diversion of hypothetical scenarios at a pyroprocessing facility considering the uncertainty in $Pu-to-^{244}Cm$ ratio estimation. The analysis is carried out by the hypothesis testing and the event tree method. The probability of detection for diversion of 8 kg Pu is found to be less than 95% if a large size granule consisting of small size particles gets sampled for measurements. To increase the probability of detection more than 95%, first, a new Material Balance Area (MBA) structure consisting of more number of Key Measurement Points (KMPs) is designed. This multiple KMP-measurement for the MBA shows the probability of detection for 8 kg Pu diversion is greater than 96%. Increasing the granule sample number from one to ten also shows the probability of detection is greater than 95% in the most ranges for granule and powder sizes.

Restoration Modeling Analysis for Abandoned Channels of the Mangyeong River

  • Kim, Jae-Hoon;Julien, Pierre Y.;Ji, Un;Kang, Joon-Gu
    • 한국환경과학회지
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    • 제20권5호
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    • pp.555-564
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    • 2011
  • This study examines the potential restoration of abandoned channels of the Mangyeong River in South Korea. To analyze the morphological changes and equilibrium conditions, a flow duration analysis was performed to obtain the discharge of 255 m3/s with a recurrence interval of 1.5 year. It is a gravel-bed stream with a median bed diameter of 36 mm. The reach-averaged results using HEC-RAS showed that the top width is 244 m, the mean flow depth is 1.11 m, the width/depth ratio is very high at 277, the channel velocity is 1.18 m/s, and the Froude number is also high at 0.42. The hydraulic parameters vary in the vicinity of the three sills which control the bed elevation. The total sediment load is 6,500 tons per day and the equivalent sediment concentration is 240 mg/l. The Engelund-Hansen method was closer to the field measurements than any other method. The bed material coarser than 33 mm will not move. The methods of Julien-Wargadalam and Lacey gave an equilibrium channel width of 83 m and 77 m respectively, which demonstrates that the Mangyeong River is currently very wide and shallow. The planform geometry for the Mangyeong River is definitely straight with a sinuosity as low as 1.03. The thalweg and mean bed elevation profiles were analyzed using field measurements in 1976, 1993 and 2009. The measured profiles indicated that the channel has degraded about 2 m since 1976. The coarse gravel material and large width-depth ratio increase the stability of the bed material in this reach.