• Title/Summary/Keyword: Mass measurement

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Development of a Mushroom Powder Certified Reference Material for Element Analysis

  • Betru, Tegegn Gizachew;Yim, Yong-Hyeon;Lee, Kyoung-Seok
    • Mass Spectrometry Letters
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    • v.11 no.4
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    • pp.108-112
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    • 2020
  • A certified reference material (CRM) for the analysis of nutrient elements in an edible mushroom (Ganoderma lyceum) powder has been developed (KRISS CRM 108-10-011). The mass fractions of calcium (Ca), iron (Fe), and zinc (Zn) were measured by isotope dilution inductively coupled plasma mass spectrometry (ID ICP/MS). To dissolve the fungi cell wall of mushroom consisted of chitin fibers, sample preparation method by single reaction chamber type microwave-assisted acid digestion with acid mixtures was optimized. The mean measurement results obtained from 12 sample bottles were used to assign as the certified values for the CRM and the between-bottle homogeneities were evaluated from the relative standard deviations. The certified values were metrologically traceable to the definition of the kilogram in the International System of Units (SI). This CRM is expected to be used for validation of analytical methods or quality control of measurement results in analytical laboratories when they determine the mass fractions of elements in mushroom or other similar samples.

Measurements of Heat (Mass) Transfer Coefficient on the Surface of a Turbine Blade with n High Turning Angle Using Naphthalene Sublimation Technique (큰 회전각을 가지는 터빈 블레이드 표면에서 나프탈렌승화법을 이용한 열(물질)전달계수 측정)

  • Gwon, Hyeon-Gu;Lee, Sang-U;Park, Byeong-Gyu
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.26 no.8
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    • pp.1077-1087
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    • 2002
  • The heat (mass) transfer characteristics on the blade surface of a high-turning first-stage turbine rotor for power generation has been investigated by employing the naphthalene sublimation technique. A four-axis profile measurement system is developed successfully for the measurements of local sublimation depth on the curved surface In the leading edge region, there is a good agreement between the present heat (mass) transfer data and the previous result on a turbine blade with a moderate turning angle, but some discrepancies are found in the mid-chord heat (mass) transfer between the two results. The local heat (mass) transfer on the present suction surface is greatly enhanced due to an earlier boundary transition, compared with that on a turbine blade with a moderate turning angle, meanwhile there is only a slight change in the pressure-side heat (mass) transfer between the two different turbine rotors. In general, the heat (mass) transfer augmentation by the endwall vortices is found much higher on the suction surface than on the pressure surface.

Large Scale Mass Flow Measurement Using Bellmouth and Rake (벨마우스와 레이크를 이용한 대용량 유량 계측)

  • Kim, Jeong-Woo
    • Journal of the Korean Society of Propulsion Engineers
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    • v.16 no.4
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    • pp.70-79
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    • 2012
  • For an aerodynamic test facility, it is very important to get the precise measurement data of pressure, temperature and mass flow rate at the upstream to the test article. Hence, a new measurement method using a bellmouth and rakes was studied for the large scale system of which the corrected mass flow is between 5 kg/s and 8 kg/s. The bellmouth was designed by ISO standard for 0.5% accuracy, and the rakes were designed by using the equal area method. From the results of 9 test trials, it is found that the Reynolds number of rakes and the mass flow rate ratio can be simply formulated by an one-dimensional equation. The mass flow rate of rakes was calibrated by this equation. By the result of calibration, The maximum error rate was -0.507%, and the average error rate was -0.000274%.

Comparison of Lipid Profiles in Head and Brain Samples of Drosophila Melanogaster Using Electrospray Ionization Mass Spectrometry (ESI-MS)

  • Jang, Hyun Jun;Park, Jeong Hyang;Lee, Ga Seul;Lee, Sung Bae;Moon, Jeong Hee;Choi, Joon Sig;Lee, Tae Geol;Yoon, Sohee
    • Mass Spectrometry Letters
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    • v.10 no.1
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    • pp.11-17
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    • 2019
  • Drosophila melanogaster (fruits fly) is a representative model system widely used in biological studies because its brain function and basic cellular processes are similar to human beings. The whole head of the fly is often used to obtain the key function in brain-related diseases like degenerative brain diseases; however the biomolecular distribution of the head may be slightly different from that of a brain. Herein, lipid profiles of the head and dissected brain samples of Drosophila were studied using electrospray ionization-mass spectrometry (ESI-MS). According to the sample types, the detection of phospholipid ions was suppressed by triacylglycerol (TAG), or the specific phospholipid signals that are absent in the mass spectrum were measured. The lipid distribution was found to be different in the wild-type and the microRNA-14 deficiency model ($miR-14{\Delta}^1$) with abnormal lipid metabolism. A few phospholipids were also profiled by comparison of the head and the brain in two fly model systems. The mass spectra showed that the phospholipid distributions in the $miR-14{\Delta}^1$ model and the wild-type were different, and principal component analysis revealed a correlation between some phospholipids (phosphatidylethanolamine (PE), phosphatidylinositol (PI), and phosphatidylserine (PS)) in $miR-14{\Delta}^1$. The overall results suggested that brain-related lipids should be profiled using fly samples after dissection for more accurate analysis.

A Study on the Gravity Anomaly of Okcheon Group based on the Gravity Measurement around Chung Lake (충주호 주변의 중력 측정에 의한 옥천계의 중력이상 연구)

  • Park, Jong-Oh;Song, Moo-Young
    • Journal of the Korean earth science society
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    • v.32 no.1
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    • pp.12-20
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    • 2011
  • The gravity measurement was conducted at 256 stations around Chungju Lake to study subsurface geological distributions and subterranean mass discontinuities by the results of gravity anomaly in Metamorphic Complex, Okcheon Group, Great Limestone Group of Choson Supergroup, and Cretaceous biotite granites. Okcheon Group showed a high Bouguer gravity anomaly while Great Limestone Group of Choson Supergroup relatively a low anomaly. The mean depth of subterranean mass discontinuities is about 2.0 km and downward along the Suchangri Formation from the Hwanggangri and Moonjuri formations. In general, Okcheon Group appeared shallower than the depth of Great Limestone Group of Choson Supergroup when imaging the subterranean mass discontinuities from the Bouguer gravity anomaly.

A Technique to Minimize Impurity Signal from Blank Rhenium Filaments for Highly Accurate TIMS Measurements of Uranium in Ultra-Trace Levels

  • Park, Jong-Ho;Choi, In-Hee;Song, Kyu-Seok
    • Mass Spectrometry Letters
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    • v.1 no.1
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    • pp.17-20
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    • 2010
  • As background significantly affects measurement accuracy and a detection limit in determination of the trace amounts of uranium, it is necessary to minimize the impurities in the filaments used for thermal ionization mass spectrometry (TIMS). We have varied the degassing condition such as the heating currents and duration times to reduce the backgrounds from the filaments prepared with zone-refined rhenium tape. The most efficient degassing condition of the heating current and the duration time was determined as 3.5 A and 60 min, respectively. The TIMS measurement combined with the isotope dilution mass spectrometry (IDMS) technique showed that the uranium backgrounds were determined to be in a few fg level from blank rhenium filaments. The background minimized filaments were utilized to measure the uranium isotope ratios of a U030 (NIST) standard sample. The excellent agreement of the measurement with the certified isotope ratios showed that the degassing procedure optimized in this study efficiently reduced the impurity signals of uranium from blank rhenium filaments to a negligible level.

Analysis of Women's Tailored Jacket Pattern Making Drafting to Suggest Implication for Apparel Mass Customization Process (의류 대량맞춤 공정 시사점 제안을 위한 여성용 테일러드 재킷 제도법 분석)

  • Hyunjung Han;Hyunsook Han
    • Journal of the Korea Fashion and Costume Design Association
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    • v.25 no.4
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    • pp.45-57
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    • 2023
  • This research compared and analyzed a representative jacket pattern making method to suggest implications for the mass customization process of clothing. Four types of pattern making methods were selected according to the degree of reflection of human body measurements. Patterns were analyzed according to the size of middle-aged women. The results of this study are as follows. First, it identified and compared the difference in human body measurement and drafting processes required for pattern drafting. Next, as a result of analyzing the manuals and institutional figures presented in the pattern drafting manuals, problems such as B.P. location and compartment of the chest circumference, which are not appropriate, were found and the human body measurement method is different for each pattern making method. Through the above analysis, the advantages and disadvantages of the pattern making methods were identified and proposed improvements and implications for the application to the apaarel mass customization process were presented.

A Study on Liquified Petroleum Gas(LPG) Fuel Quantitative Method using Coriolis Mass Flowmeter (코리올리 질량유량계를 이용한 액화석유가스(LPG) 정량 측정 방법 연구)

  • Park, Tae-Seong;Seong, Sang-Rae;Yim, Eui-Soon;Lee, Joung-Min;Lee, Myung-Sig;Kang, Hyung-Kyu
    • Journal of the Korean Institute of Gas
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    • v.22 no.6
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    • pp.109-122
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    • 2018
  • Domestic LPG meters are being tested for LPG quantification in accordance with the "Measures Act". The LPG meter is re-tested every three years in accordance with the "Enforcement Decree of the Measures Act". The maximum permissible error within the test is within ${\pm}1.0%$, and the tolerance is within ${\pm}1.5%$. For the quantitative measurement of LPG, a hydrometer for LPG, a balance, and a pressure vessel are used. The volume of LPG varies in depending on the temperature and pressure. The current quantitative measurement method of LPG requires the measurement of temperature, pressure and density in order to determine the volume of LPG, respectively, and some equipments are needed accordingly. Coriolis mass flowmeter, on the other hand, measure the mass flow, density and temperature at the same time, and can be converted and calculated to the required values using a computer program, also it is widely applied in the industrial field. In this study, the volume of LPG was measured using a Coriolis mass flowmeter as a basic study of LPG quantitative measurement. In addition, it is shown that it is possible to apply for the LPG quantitative measurement using the Coriolis mass flowmeter by comparing it with the conventional LPG quantitative measurement method.

Analysis of Measurement Error for PM-10 Mass Concentration by Inter-Comparison Study (비교 측정을 통한 PM-10 질량농도의 오차 분석)

  • Jung, Chang-Hoon;Cho, Yang-Sung;Hwang, S.M.;Jung, Y.G.;Ryu, J.C.;Shin, D.S.
    • Journal of Korean Society for Atmospheric Environment
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    • v.23 no.6
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    • pp.689-698
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    • 2007
  • Particular attention is paid to the validity of PM-10 measurement using beta attenuation method. In this study, the inter-comparison studies were undertaken for PM-10 sampler with different measuring methods. The three beta attenuation monitoring instruments (BAM1020, FH C-14, and DIGS-150) and filter based gravitational method using High Volume Air Sampler were collocated and mass concentrations were compared from August to November, 2006. The results of the investigation show that beta attenuation monitoring instruments are comparable with gravitational method within 10% of measurement error. For specific conditions under high humidity and high concentrations, the inter-comparison results also showed a relatively good agreement and this can be explained as the effect of inlet heating of beta attenuation instrument. Subsequently, this study shows that beta attenuation monitoring instruments can be equivalently used with reasonable validity when compared gravimetric method.

Measurement of Absolute Magnitude and Position of HDD Unbalance based on Mobility (모빌리티 측정을 통한 하드디스크의 Unbalance 검출 및 보정방법)

  • Choi, Hyun;Kim, In-Woong;Lee, Jae-Won;Jeong, Yong-Koo;Choi, Jung-Hun
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2002.11b
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    • pp.358-362
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    • 2002
  • The HDD unbalance, with higher rotational speed, is directly influenced by the mechanical assembly allowance between clamping disk and platter disk. The low frequency structural vibration induced by the unbalance force finally gives rise to the structure borne noise of the personal computer. To meet the noise and vibration requirements, the absolute unbalance mass of HDD needs to be measured and adjusted in the disk assembling stage. This study introduces the measurement methods of the absolute magnitude and position of the unbalance mass of HDD based on the mobility and acceleration orbit. The absolute unbalance mass can be obtained by the acceleration responses and the mobility of the mechanical part, while the position of the unbalance mass ran be obtained by the rotation acceleration orbit.

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